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Yıl 2017, Cilt: 1 Sayı: 1, 11 - 19, 28.12.2017

Alper Çolak Murat Taş Gazi İrez Orhan Büyükgüngör Ferdağ Çolak Handan Günay

Öz

Kaynakça

  • Reference 1 W. H.Correa, S. Papadopoulos, P. Radnidge, B. A. Roberts, J. L. Scott, Green Chem. 2002, 4, 245-251. Reference 2 A. Göblöys, L. Lázár, F. Fülöp, Tetrahedron 2002, 58, 1011-1016. Reference 3 J. Sinkkonen, K. N. Zelenin, A. K. A. Potapov, I. V. Lagoda, V. V. Alekseyev, K. Pihlaja, Tetrahedron 2003, 59, 1939-1950. Reference 4 K. Tanaka, R. Shiraishi, Green Chem. 2000, 2, 272-273. Reference 5 A. T. Çolak, M. Taş, G. İrez, O. Z. Yeşilel, O. Büyükgüngör, Z. Anorg. Allg. Chem. 2007, 633, 504-508. Reference 6 National committee for clinical laboratory standards (NCCLS) Performance standards for antimicrobial disk susceptibility tests. Approved standard (M2-A4). National committee for clinical laboratory standards Villanova, PA. 1990a. Reference 7 National committee for clinical laboratory standards. Methods for dilution antimicrobial susceptibility test for bacteria that grow aerobically. Approved standard (M7-A2). National committee for clinical laboratory standards, Villanova, PA. 1990b. Reference 8 Stoe&Cie, X-Area (Version 1.18) and X-Red32 (Version 1.04), Stoe&Cie. Darmstadt, Germany, 2002. Reference 9 M.C. Burla, R. Caliandro, M. Camalli, B. Carrozzini, G. L. Cascarano, L. D. Caro, C. Giacovazzo, G. Polidori, R. Spagna, J. Appl. Crystallogr. 2005, 38, 381-388. Reference 10 Sheldrick G.M. SHELXL-97: Program for the Refinement of Crystal Structures. (Germany University of Göttingen), 1997. Reference 11 C.K. Johnson, M.N. Burnett, ORTEP-III (version 1.0.2), Rep. ORNL-6895, Oak Ridge National Laboratory, Oak Ridge, TN (USA) (1996). Windows version: Farrugia L.J., University of Glasgow, Glasgow, Scotland (U.K.), 1997. Reference 12 L. J. Farrugia, J. Appl. Crystallogr. 1999, 32, 837-838. Reference 13 Á. Somogyi, Medical applications of Mass Spectrometry, K. Vékey, A. Telekes and A. Vertes (editors) Elsevier B.V. 2008. Reference 14 L. Bajpai, M. Varshney, C. N. Seubert, S. M. J. Stevens, J. V. Johnson, R. A. Yost, D. M. Dennis, J. Am. Soc. Mass Spectrom. 2005, 16, 814-824. Reference 15 M. Taş, H. Batı, J. Chem. Res. 2006, 87-92. Reference 16 A. Zülfikaroğlu, M. Taş, H. Batı, B. Batı, Synth. React. Inorg.Met. Org. Chem. 2003, 33, 625-638. Reference 17 H. Batı, M. Taş, B. Batı, Synth. React. Inorg. Met. Org. Chem. 2001, 31, 541-548. Reference 18 H. Batı, M. Taş, M. Macit, Synth. React. Inorg. Met. Org.Chem. 1998, 28, 1371-1380. Reference 19 M. V. Barybin, P. L. Diaconescu, C. C. Cummins, Inorg. Chem. 2001, 40, 2892-2897. Reference 20 S. Sevagapandian, G. Rajagopal, K. Nehru, P. Athappan, Trans. Metal Chem. 2000, 25, 388-393. Reference 21 R. M. Srivastava, I. M. Brinn, J. O. Machura-Herrera, H. B. Faria, G. B. Carpenter, D. Andrade, C.G. Venkatesh, L. P. F. Morais, J. Mol. Struct. 1997, 406, 159-167. Reference 22 F. Karipçin, H. I. Uçan, I. Karataş, Trans. Metal Chem. 2002, 27, 813-817. Reference 23 M. Taş, H. Batı, J. Therm. Anal. Cal. 2006, 85, 295-299. Reference 24 B. K. Singh, U. K., Jetley, R. K., Sharma, B. S. Garg, Spectrochimica Acta Part A 2007, 68, 63-73. Reference 25 N. Tounsi, L. Dupont, A. Mohamadou, E. Guillon, M. Aplincourt, G. Rogez, Polyhedron 2008, 27, 674-3682. Reference 26 M. C. Fernández-Fernández, R. B. Calle, A. Macías, L. V. Matarranz, P. P. Lourido, Polyhedron 2008, 27, 2301-2308. Reference 27 F. Hamurcu, A. B. Gündüzalp, S. Çete S., B. Erk, Tran. Met. Chem. 2008, 33, 137-141.

Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-tetrahydroquinazoline and Its Nickel(II) Complexes

Yıl 2017, Cilt: 1 Sayı: 1, 11 - 19, 28.12.2017

Alper Çolak Murat Taş Gazi İrez Orhan Büyükgüngör Ferdağ Çolak Handan Günay

Öz

The
2-methyl-2-(1-hydroxyiminoethyl)-1,2,3,4-tetrahydroquinazoline (HL or 1) and its novel Ni(II) complexes, square-planar
[Ni(L)(LH)]·(NO3) (2) and
octahedral [NiCl2(LH)(H2O)2]·(H2O) (3), have been synthesized. The ligand and complexes
have been characterized by means of elemental, IR, UV-Vis. spectroscopic
studies, 1H-NMR, 13C-NMR, magnetic susceptibility,
thermal analysis, mass spectroscopy and X-ray diffraction technique. The HL
ligand crystallizes in the P21/c. Antimicrobial activity of ligand (1) and complexes (2 and 3) was evaluated by
the agar diffusion method. Complex 2 showed weak antimicrobial activity against
tested microorganism strains. Complex 3 exhibited moderate antimicrobial activity
against Staphylococcus epidermidis
and Candida albicans.

Anahtar Kelimeler

antimicrobial activity nickel complex oxime 1 2 3

Kaynakça

  • Reference 1 W. H.Correa, S. Papadopoulos, P. Radnidge, B. A. Roberts, J. L. Scott, Green Chem. 2002, 4, 245-251. Reference 2 A. Göblöys, L. Lázár, F. Fülöp, Tetrahedron 2002, 58, 1011-1016. Reference 3 J. Sinkkonen, K. N. Zelenin, A. K. A. Potapov, I. V. Lagoda, V. V. Alekseyev, K. Pihlaja, Tetrahedron 2003, 59, 1939-1950. Reference 4 K. Tanaka, R. Shiraishi, Green Chem. 2000, 2, 272-273. Reference 5 A. T. Çolak, M. Taş, G. İrez, O. Z. Yeşilel, O. Büyükgüngör, Z. Anorg. Allg. Chem. 2007, 633, 504-508. Reference 6 National committee for clinical laboratory standards (NCCLS) Performance standards for antimicrobial disk susceptibility tests. Approved standard (M2-A4). National committee for clinical laboratory standards Villanova, PA. 1990a. Reference 7 National committee for clinical laboratory standards. Methods for dilution antimicrobial susceptibility test for bacteria that grow aerobically. Approved standard (M7-A2). National committee for clinical laboratory standards, Villanova, PA. 1990b. Reference 8 Stoe&Cie, X-Area (Version 1.18) and X-Red32 (Version 1.04), Stoe&Cie. Darmstadt, Germany, 2002. Reference 9 M.C. Burla, R. Caliandro, M. Camalli, B. Carrozzini, G. L. Cascarano, L. D. Caro, C. Giacovazzo, G. Polidori, R. Spagna, J. Appl. Crystallogr. 2005, 38, 381-388. Reference 10 Sheldrick G.M. SHELXL-97: Program for the Refinement of Crystal Structures. (Germany University of Göttingen), 1997. Reference 11 C.K. Johnson, M.N. Burnett, ORTEP-III (version 1.0.2), Rep. ORNL-6895, Oak Ridge National Laboratory, Oak Ridge, TN (USA) (1996). Windows version: Farrugia L.J., University of Glasgow, Glasgow, Scotland (U.K.), 1997. Reference 12 L. J. Farrugia, J. Appl. Crystallogr. 1999, 32, 837-838. Reference 13 Á. Somogyi, Medical applications of Mass Spectrometry, K. Vékey, A. Telekes and A. Vertes (editors) Elsevier B.V. 2008. Reference 14 L. Bajpai, M. Varshney, C. N. Seubert, S. M. J. Stevens, J. V. Johnson, R. A. Yost, D. M. Dennis, J. Am. Soc. Mass Spectrom. 2005, 16, 814-824. Reference 15 M. Taş, H. Batı, J. Chem. Res. 2006, 87-92. Reference 16 A. Zülfikaroğlu, M. Taş, H. Batı, B. Batı, Synth. React. Inorg.Met. Org. Chem. 2003, 33, 625-638. Reference 17 H. Batı, M. Taş, B. Batı, Synth. React. Inorg. Met. Org. Chem. 2001, 31, 541-548. Reference 18 H. Batı, M. Taş, M. Macit, Synth. React. Inorg. Met. Org.Chem. 1998, 28, 1371-1380. Reference 19 M. V. Barybin, P. L. Diaconescu, C. C. Cummins, Inorg. Chem. 2001, 40, 2892-2897. Reference 20 S. Sevagapandian, G. Rajagopal, K. Nehru, P. Athappan, Trans. Metal Chem. 2000, 25, 388-393. Reference 21 R. M. Srivastava, I. M. Brinn, J. O. Machura-Herrera, H. B. Faria, G. B. Carpenter, D. Andrade, C.G. Venkatesh, L. P. F. Morais, J. Mol. Struct. 1997, 406, 159-167. Reference 22 F. Karipçin, H. I. Uçan, I. Karataş, Trans. Metal Chem. 2002, 27, 813-817. Reference 23 M. Taş, H. Batı, J. Therm. Anal. Cal. 2006, 85, 295-299. Reference 24 B. K. Singh, U. K., Jetley, R. K., Sharma, B. S. Garg, Spectrochimica Acta Part A 2007, 68, 63-73. Reference 25 N. Tounsi, L. Dupont, A. Mohamadou, E. Guillon, M. Aplincourt, G. Rogez, Polyhedron 2008, 27, 674-3682. Reference 26 M. C. Fernández-Fernández, R. B. Calle, A. Macías, L. V. Matarranz, P. P. Lourido, Polyhedron 2008, 27, 2301-2308. Reference 27 F. Hamurcu, A. B. Gündüzalp, S. Çete S., B. Erk, Tran. Met. Chem. 2008, 33, 137-141.
Toplam 1 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Kimya Mühendisliği
Bölüm Research Articles
Yazarlar

Alper Çolak

Murat Taş

Gazi İrez Bu kişi benim

Orhan Büyükgüngör

Ferdağ Çolak Bu kişi benim

Handan Günay

Yayımlanma Tarihi 28 Aralık 2017
Yayımlandığı Sayı Yıl 2017 Cilt: 1 Sayı: 1

Kaynak Göster

APA Çolak, A., Taş, M., İrez, G., Büyükgüngör, O., vd. (2017). Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-tetrahydroquinazoline and Its Nickel(II) Complexes. Acta Materialia Turcica, 1(1), 11-19.
AMA Çolak A, Taş M, İrez G, Büyükgüngör O, Çolak F, Günay H. Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-tetrahydroquinazoline and Its Nickel(II) Complexes. ACTAMAT. Aralık 2017;1(1):11-19.
Chicago Çolak, Alper, Murat Taş, Gazi İrez, Orhan Büyükgüngör, Ferdağ Çolak, ve Handan Günay. “Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-Tetrahydroquinazoline and Its Nickel(II) Complexes”. Acta Materialia Turcica 1, sy. 1 (Aralık 2017): 11-19.
EndNote Çolak A, Taş M, İrez G, Büyükgüngör O, Çolak F, Günay H (01 Aralık 2017) Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-tetrahydroquinazoline and Its Nickel(II) Complexes. Acta Materialia Turcica 1 1 11–19.
IEEE A. Çolak, M. Taş, G. İrez, O. Büyükgüngör, F. Çolak, ve H. Günay, “Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-tetrahydroquinazoline and Its Nickel(II) Complexes”, ACTAMAT, c. 1, sy. 1, ss. 11–19, 2017.
ISNAD Çolak, Alper vd. “Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-Tetrahydroquinazoline and Its Nickel(II) Complexes”. Acta Materialia Turcica 1/1 (Aralık 2017), 11-19.
JAMA Çolak A, Taş M, İrez G, Büyükgüngör O, Çolak F, Günay H. Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-tetrahydroquinazoline and Its Nickel(II) Complexes. ACTAMAT. 2017;1:11–19.
MLA Çolak, Alper vd. “Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-Tetrahydroquinazoline and Its Nickel(II) Complexes”. Acta Materialia Turcica, c. 1, sy. 1, 2017, ss. 11-19.
Vancouver Çolak A, Taş M, İrez G, Büyükgüngör O, Çolak F, Günay H. Synthesis, Characterization and Biological Activities of Novel a 1,2,3,4-tetrahydroquinazoline and Its Nickel(II) Complexes. ACTAMAT. 2017;1(1):11-9.
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