Fe2O3 Nanoparçacıkların Yeşil Sentezi ve Karakterizasyonu

Year 2023, Volume: 28 Issue: 3, 1059 - 1067, 29.12.2023

Başak Doğru Mert

https://doi.org/10.53433/yyufbed.1276192

Abstract

Bu çalışmanın amacı geniş uygulama alanları nedeniyle demir III oksit (Fe2O3) nanoparçacıkları üretmektir. Birçok avantajı nedeniyle sentez yönteminde zerdeçalın etanolik ekstraktı kullanılmıştır. Bu avantajlar arasında ucuz olması, yaygın olarak erişilebilir olması, ekstaksiyonlarının basit olması ve kontaminasyona daha az eğilimli olması yer alır. Üretilen parçacıklar, taramalı elektron mikroskobu (SEM), enerji dağılımlı X-Ray analizi (EDX) ve geçirimli elektron mikroskobu (TEM) ile analiz edildi. Ayrıca Fe2O3 partiküllerinin zeta potansiyeli belirlendi, ultraviyole-görünür bölge spektroskopisi (UV) analizi ve fourier dönüşümlü kızılötesi spektroskopisi (FTIR) analizi yapıldı. Elde edilen sonuçlara göre tanecik boyutu 30 ile 80 nm arasında değişen granüler şekilli nanopartiküller sentezlendi ve yeterince kararlı oldukları tespit edildi.

Keywords

Demir (III) oksit, Nanopartikül, Yeşil sentez

Green Synthesis and Characterization of Fe2O3 Nanoparticles

Abstract

The aim of this study is to produce iron III oxide (Fe2O3) nanoparticles due to their wide application area. The ethanolic extract of curcuma was used in the synthesis method due to number of advantages. These benefits include being inexpensive, widely accessible, simple to extract, and less prone to contamination. The produced particles were analyzed via scanning electron microscope (SEM), energy dispersive analysis (EDX), and transmission electron microscope (TEM). Furthermore, the zeta potential of Fe2O3 particles was determined, ultraviolet–visible spectroscopy (UV) analysis and fourier transform infrared spectroscopy (FTIR) analysis were done. According to the results obtained, granular nanoparticles with particle sizes ranging from 30 to 80 nm were synthesized and it was determined that they were sufficiently stable.

Keywords

Green synthesis, Iron (III) oxide, Nanoparticle

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