RELEASE PROFILE OF MINT (MENTHA SPICATA AND MENTHA PIPERITA) ESSENTIAL OIL MICROENCAPSULATED BY SPRAY DRYER

Yıl 2017, Cilt: 42 Sayı: 2, 186 - 196, 15.04.2017

Bülent Başyiğit, Mustafa Çam

Öz

Maltodextrin-gam
arabic (62-38%)  combination and 100% gam
arabic as wall materials were used for microencapsulation of mint (Mentha spicata and Mentha piperita) essantial oil. Mint (Mentha spicata and Mentha
piperita) essential oil was microencapsulated by spray dryer. Reaction
kinetics of these microcapsules were evaluated with accelerated storage. For
this purpose, microcapsules were put in oven at 160, 180 and 200 °C and they
were taken out at specific times to determine amounts of essential oils by Gas
Chromatography- Flame Ionization Dedector (GC-FID). It was
determined that release profile of mint (Mentha
spicata and Mentha piperita)
essential oil was appropriate to zero-order reaction. The activation energy, z
and Q10 values of microcapsules were evaluted different each other.
Additionally, it was observed that half-life and decimal reduction time (D)
decreased when tempareture increased.

Anahtar Kelimeler

Mentha spicata, Mentha piperita, essential oils, microencapsulation, kinetic

PÜSKÜRTMELİ KURUCUTU İLE MİKROENKAPSÜLE EDİLMİŞ NANE (MENTHA PIPERITA VE MENTHA SPICATA) ESANSİYEL YAĞININ SALINIM PROFİLİ

Öz

Bu
çalışmada gam arabik-maltodekstrin (GA-MD) (%38-62) kombinasyonu ve %100 gam
arabik (GA) nane (Mentha piperita ve Mentha spicata) esansiyel yağının
mikroenkapsülasyonu için kaplama materyali olarak kullanılmıştır. 4 farklı nane
(Mentha piperita ve Mentha spicata) esansiyel yağı
püskürtmeli kurutucu ile toz haline getirilmiştir. Mikroenkapsüle haldeki
örnekler fanlı etüvlerde 160, 180 ve 200 °C’de belirli aralıklarla örnekleme
yapılarak hızlandırılmış depolamaya alınmıştır. Mikroenkapsüle örneklerde kalan
yağ miktarı Gaz kromotografisi-Alev iyonizasyon dedektörü (GC-FID) ile
belirlenerek örneklerin reaksiyon kinetikleri incelenmiştir. Nane (Mentha piperita ve Mentha spicata) esansiyel yağ salınımının 0. derece reaksiyon
kinetiğine uygun olduğu belirlenmiştir. Ayrıca mikroenkapsüle edilmiş
örneklerin aktivasyon enerjileri, z ve Q10 değerleri birbirinden farklı
bulunmuş ve sıcaklık arttıkça örneklerin yarılanma süresi ve desimal azalma
süresinin (D) azaldığı görülmüştür.

Anahtar Kelimeler

Mentha spicata, Mentha piperita, esansiyel yağ, mikroenkapsülasyon, kinetik

Kaynakça

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