TY  - JOUR
T1  - Tek Kapta Yeni Bir Yöntemle Alkollerden Potansiyel Biyolojik Aktif Azidosülfonil Bileşiklerinin Sentezi
TT  - The Novel Method and One-pot Synthesis of Potential Biological Active Azidosulfonyl Compounds from Alcohols
AU  - Atmaca, Ufuk
PY  - 2020
DA  - March
Y2  - 2019
DO  - 10.21597/jist.570545
JF  - Journal of the Institute of Science and Technology
JO  - J. Inst. Sci. and Tech.
PB  - Igdir University
WT  - DergiPark
SN  - 2536-4618
SP  - 345
EP  - 356
VL  - 10
IS  - 1
LA  - tr
AB  - Bu çalışmada, çeşitli alkoller ile klorosülfonil izosiyanat (CSI) ve sodyum azid varlığında tek kapta yeni bir yöntemle azidosülfonil bileşiklerinin sentezi gerçekleştirilmiştir. Reaksiyon verimin artırılması için kullanılan asit, baz ve çözücü parametreleri incelenmiş ve optimize reaksiyon şartlarında yüksek verimlerle azidosülfonil bileşiklerinin sentezi gerçekleştirilmiştir. Sentezleri gerçekleştirilen bileşiklerin yapı karakterizasyonları 1H NMR, 13C NMR, IR ve Elementel analiz sonuçları ile yapılmıştır.
KW  - Azidosulfonil
KW  - alkol
KW  - klorosulfonil izosiyanat
KW  - sodyum azit
N2  - In this study, the one-pot synthesis of azidosulphonyl compounds by a new method was carried out in the presence of chlorosulfonyl isocyanate (CSI) and sodium azide with various alcohols. The acid, base and solvent parameters used to increase the reaction yield were investigated and synthesis of azidosulfonyl compounds was carried out in high yields under optimized reaction conditions. The structure characterization of the synthesized molecules was performed with 1H NMR, 13C NMR, IR and Elemental analysis.
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UR  - https://doi.org/10.21597/jist.570545
L1  - https://dergipark.org.tr/en/download/article-file/969975
ER  -