TY  - JOUR
T1  - TiNb-esaslı β-Ti Alaşımlarının Kristal Yapı, Mikroyapı ve Dönüşüm Sıcaklıklarına Tantal Katkısının Etkileri
TT  - The Effects of Tantalum Additive on the Crystal Structure, Microstructure and Transformation Temperatures of TiNb-based β-Ti Alloys
AU  - Ercan, Ercan
AU  - Dağdelen, Fethi
PY  - 2020
DA  - December
Y2  - 2020
DO  - 10.17798/bitlisfen.775976
JF  - Bitlis Eren Üniversitesi Fen Bilimleri Dergisi
PB  - Bitlis Eren University
WT  - DergiPark
SN  - 2147-3129
SP  - 1545
EP  - 1553
VL  - 9
IS  - 4
LA  - tr
AB  - β-tipi Ti-esaslı alaşımlar yüksek sıcaklıktaki dayanıklılığı ve biyo-uyumluluğu sayesinde uzay sanayisi ve medikal alanlarda kullanımı yaygın olan materyallerdir. Nb ve Ta gibi düşük yoğunluklu, üstün korozyon direnci ve toksik olmayan özelliklere sahip elementler ile takviye edilmesi, β-tipi Ti-esaslı alaşımları daha da çekici hale getirmiştir. TiNb(24,5-x)Ta(x=0,1,2,3,4) (at. %) oranlarında hazırlanan alaşımların X-ışını, mikroyapı ve dönüşüm sıcaklıkları incelendi. DSC analizlerinden 5,5 oC to 41,1 oC aralığında sadece α→β ters dönüşümü gözlenmiştir. Oda sıcaklığında yapılan XRD analizleri ile DSC sonuçlarının uyumlu olduğu görülmüştür. Baskın β fazlarına karşın α fazlarının küçük miktarlar da olduğu tespit edilmiştir. β fazının baskın olması Ta ve Nb elementlerinin iyi bir β stabilizatörü olduğunu göstermiştir. Optik mikroskop görüntülerinden alaşımlardaki β fazı, taneler ve tane sınırlarının artan Ta ilavesiyle belirginleşmiştir. SEM-EDX görüntülerinden α fazının çökelti olduğu görülmüştür. Ayrıca EDX sonuçları ile Ta element konsatrasyonunun tane sınırlarında arttığı bulunmuştur. Alaşımların (ev⁄a) ve (cv ) oranları oda sıcaklığı altında dönüşüm sergileyen düşük değerli (ev⁄a
KW  - β-tipi Ti
KW  - kristal yapı
KW  - mikroyapı
KW  - ters dönüşümlü martensit
N2  - β-type Ti-based alloys are materials which widely used in the aerospace industry and medical fields because it has a sufficient biocompatibility and high temperature resistance. Reinforcement with low-density, high corrosion resistance and non-toxic elements, such as Nb and Ta alloying with β-type of Ti-based alloys even more attractive. X-ray, microstructure, and transformation temperatures of TiNb(24,5-x)Ta(x = 0,1,2,3,4) (at. %) alloys were investigated. The DSC analysis showed only α→β reverse transformation for the temperature range of 5,5 oC to 41,1 oC. DSC results were found to be compatible with X-ray analysis taken at room temperature. It was found that α phases were in small amounts despite dominant β phases. The dominance of the β phase has shown that the Ta and Nb elements are a good β stabilizer. It was determined from the optical microscope images that the β phase, grains, and grain boundaries in alloys increased with the addition of Ta. From SEM-EDX results, it was found that α phase is a precipitation. Additionally, the EDX results showed that Ta elements concentration increased in the grain boundaries. Valance electron concentration (ev⁄a) and concentration of valance electron (cv ) values indicated that the alloy with low values of (ev⁄a
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UR  - https://doi.org/10.17798/bitlisfen.775976
L1  - https://dergipark.org.tr/en/download/article-file/1223200
ER  -