Benzotiyazol ve ilgili benzil halojenürler kullanılarak iki yeni benzotiyazolyum tuzu N-(4-metoksibenzil)benzotiyazolyum klorür (1a) ve N-(4-tert-bütilbenzil)benzotiyazolyum bromür (1b) hazırlandı. Selenoüre N,S-heterosiklik bazlı türevler (2a ve 2b), tuzların KOBut bazı varlığında selenyum ile reaksiyonu sonucu elde edildi. Sentezlenen bileşiklerin karakterizasyonu için 1H NMR, 13C NMR ve elementel analiz kullanıldı.. Ayrıca, selenyum katılma ürünlerinin molekül ağırlıkları LC-MS/MS analizi ile doğrulandı.
BAP 2019/141
This work was supported by the Scientific Research Project Fund of Manisa Celal Bayar University under project number 2019-141.
Two novel benzothiazolium salts, N-(4-methoxybenzyl)benzothiazolium chloride (1a) and N-(4-tert-butylbenzyl)benzothiazolium bromide (1b), were prepared by using benzothiazole and related benzyl halides. Selenourea N,S-heterocyclic-based derivatives (2a and 2b) were obtained by the reaction of the salts with selenium in the presence of KOBut base. 1H NMR, 13C NMR and elemental analysis were used for characterization of the synthesized compounds. Also, molecular weights of the selenium adducts were validated by LC-MS/MS analysis.
BAP 2019/141
This work was supported by the Scientific Research Project Fund of Manisa Celal Bayar University under project number 2019-141.
Primary Language | English |
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Subjects | Inorganic Chemistry (Other) |
Journal Section | Articles |
Authors | |
Project Number | BAP 2019/141 |
Early Pub Date | July 23, 2024 |
Publication Date | August 20, 2024 |
Submission Date | January 31, 2024 |
Acceptance Date | June 13, 2024 |
Published in Issue | Year 2024 Volume: 24 Issue: 4 |