Short Communication
PDF Mendeley EndNote BibTex Cite

Year 2022, Volume early view, Issue early view, 0 - 0, 23.11.2021
https://doi.org/10.19111/bulletinofmre.947703

Abstract

References

  • Alomary, A.A., Belhadj, S. 2007. Determination of heavy metals Cd, Cr, Cu, Fe, Ni, Pb, Zn by ICP-OES and their speciation in Algerian Mediterranean Sea sediments after a five-stage sequential extraction procedure. Environmental monitoring and assessment 135, 1-3, 265-280.
  • Chen, Z., Canil, D., Longerich, H.P. 2000. Automated in situ trace element analysis of silicate materials by laser ablation inductively coupled plasma mass spectrometry. Fresenius' journal of analytical chemistry 368, 73-78.
  • Dahlquist, R.L, Knoll, J.W. 1978. Inductively coupled plasma-atomic emission spectrometry: analysis of biological materials and soils for major, trace, and ultra-trace elements. Applied Spectroscopy 32, 1-30.
  • Eggins, S.M. 2003. Laser ablation ICP-MS analysis of geological materials prepared as lithium borate glasses. Geostandards Newsletter 27, 147-162.
  • Elburg, M. A., Andersen, T., Bons, P. D., Weisheit, A., Simonsen, S. L., Smet, I. 2012. Metasomatism and metallogeny of A-type granites of the Mt Painter–Mt Babbage Inliers, South Australia. Lithos 151, 83-104.
  • Fedorowich, J. S., Richards, J. P., Jain, J. C., Kerrich, R., Fan, J. 1993. A rapid method for REE and trace-element analysis using laser sampling ICP-MS on direct fusion whole-rock glasses. Chemical Geology 106, 3-4, 229-249.
  • Govindaraju, K. 1994. 1994 compilation of working values and sample description for 383 geostandards. Geostandards newsletter 18, 1-158.
  • Guillong, M., Meier, D. L., Allan, M. M., Heinrich, C. A., Yardley, B. W. 2008. Appendix A6: SILLS: A MATLAB-based program for the reduction of laser ablation ICP-MS data of homogeneous materials and inclusions. Mineralogical Association of Canada Short Course 40, 328-333.
  • Günther, D., Quadt, A. V., Wirz, R., Cousin, H., Dietrich, V. J. 2001. Elemental analyses using laser ablation-inductively coupled plasma-mass spectrometry LA-ICP-MS of geological samples fused with Li2B4O7 and calibrated without matrix-matched standards. Microchimica Acta 136, 3-4, 101-107.
  • Imai, N. 1990. Quantitative analysis of original and powdered rocks and mineral inclusions by laser ablation inductively coupled plasma mass spectrometry. Analytica Chimica Acta 235, 381-391.
  • Jarvis, I., Jarvis, K. E. 1992. Inductively coupled plasma-atomic emission spectrometry in exploration geochemistry. Journal of Geochemical Exploration 44, 1-3, 139-200.
  • Jenner, G. A., Longerich, H. P., Jackson, S. E., Fryer, B. J. 1990. ICP-MS—A powerful tool for high-precision trace-element analysis in Earth sciences: Evidence from analysis of selected USGS reference samples. Chemical Geology 83, 1-2, 133-148.
  • Jochum, K. P., Weis, U., Stoll, B., Kuzmin, D., Yang, Q., Raczek, I., Enzweiler, J. 2011. Determination of reference values for NIST SRM 610–617 glasses following ISO guidelines. Geostandards and Geoanalytical Research 35, 4, 397-429.
  • Jochum, K. P., Weis, U., Schwager, B., Stoll, B., Wilson, S. A., Haug, G. H., Enzweiler, J. 2016 . Reference values following ISO guidelines for frequently requested rock reference materials. Geostandards and Geoanalytical Research 40, 3, 333-350.
  • Kurosawa, M., Shima, K., Ishii, S., Sasa, K. 2006. Trace element analysis of fused whole‐rock glasses by laser ablation‐ICP‐MS and PIXE. Geostandards and Geoanalytical Research 30, 1, 17-30.
  • Liu, Y., Hu, Z., Zong, K., Gao, C., Gao, S., Xu, J., Chen, H. 2010. Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS. Chinese Science Bulletin 55, 15, 1535-1546.
  • Liu, Y., Hu, Z., Li, M., Gao, S. 2013. Applications of LA-ICP-MS in the elemental analyses of geological samples. Chinese Science Bulletin 58, 32, 3863-3878.
  • Longerich, H. P., Jackson, S. E., Günther, D. 1996. Inter-laboratory note. Laser ablation inductively coupled plasma mass spectrometric transient signal data acquisition and analyte concentration calculation. Journal of analytical atomic spectrometry 11, 9, 899-904.
  • Navarro, M. S., Ulbrich, H. H. G. J., Andrade, S., Janasi, V. A. 2002. Adaptation of ICP–OES routine determination techniques for the analysis of rare earth elements by chromatographic separation in geologic materials: tests with reference materials and granitic rocks. Journal of alloys and compounds 344, 1-2, 40-45.
  • Norman, M. D., Pearson, N. J., Sharma, A., Griffin, W. L. 1996. Quantitative analysis of trace elements in geological materials by laser ablation ICPMS: instrumental operating conditions and calibration values of NIST glasses. Geostandards Newsletter 20, 2, 247-261.
  • Pearce, J. A., Harris, N. B., Tindle, A. G. 1984. Trace element discrimination diagrams for the tectonic interpretation of granitic rocks. Journal of petrology 25, 4, 956-983.
  • Petrelli, M., Perugini, D., Alagna, K. E., Poli, G., Peccerillo, A. 2008. Spatially resolved and bulk trace element analysis by laser ablation-inductively coupled plasma-mass spectrometry LA-ICP-MS . Periodico di Mineralogia 77, 3, 3-21.
  • Potts, P. J., Webb, P. C. 1992. X-ray fluorescence spectrometry. Journal of Geochemical Exploration 44, 1-3, 251-296.
  • Shao, F., Niu, Y., Liu, Y., Chen, S., Kong, J., Duan, M. 2017. Petrogenesis of Triassic granitoids in the East Kunlun Orogenic Belt, northern Tibetan Plateau and their tectonic implications. Lithos 282, 33-44.
  • Tamura, A., Akizawa, N., Otsuka, R., Kanayama, K., Python, M., Morishita, T., Arai, S. 2015. Measurement of whole-rock trace-element composition by flux-free fused glass and LA-ICP-MS: evaluation of simple and rapid routine work. Geochemical Journal 49, 3, 243-258.
  • Wilson, S. 2017. USGS microanalytical reference materials MRMS development. Microscopy and Microanalysis 23, 492-493.
  • GEOREM database. http://georem.mpch-mainz.gwdg.de/start.asp?dataversion=current . February 27, 2021.
  • Mendeley Database for Tables. https://data.mendeley.com/datasets/tfxzf3v44s/draft?a=d0b2dfde-46dd-4c6b-b024-ea27310b85e1 . February 27, 2021.
  • Perkin Elmer Syngistix Software. https://www.perkinelmer.com/lab-solutions/resources/docs/PRD_Syngistix-Atomic-Spec-Software-Family_011968_01.pdf . February 27, 2021.

Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments

Year 2022, Volume early view, Issue early view, 0 - 0, 23.11.2021
https://doi.org/10.19111/bulletinofmre.947703

Abstract

ICP-OES and LA-ICP-MS instruments routinely used to assess the geochemical properties of the various natural and synthetic materials. In this contribution the analytical routines and method development procedures of the ICP-OES and LA-ICP-MS facilities installed at the Istanbul University-Cerrahpaşa Geological Engineering Department, Geochronology and Geochemistry Laboratory have been evaluated using well-known international rock standards. Sample preparation techniques, method development, experimental setup and measurement conditions for the both ICP-OES and LA-ICP-MS instruments discussed and specific analyze results of NIST SRM 614, BCR-2, AGV-2, BCR-2G and AGV-2G evaluated. Flux-free USGS glass standards produced by in-house techniques and flux-bearing glasses produced by fusion of sample with the mixture of ultra-pure lithium-tetraborate, lithium metaborate and lithiumbromide are evaluated and compared with the well-known reference values in the literature. Relative standard deviation (RSD) values for the major oxide measurements for standards given range of range of 0.0 wt. % to 1.5 wt. %. RSD values for the trace and rare-earth-elements values mainly lower than 10 wt. %. The results confirm that the both flux-bearing and flux-free glasses reasonably match with the world-wide inter-laboratory values for international standards samples. The combination of these two instruments can be used to conduct geochemistry of various solid earth materials.

References

  • Alomary, A.A., Belhadj, S. 2007. Determination of heavy metals Cd, Cr, Cu, Fe, Ni, Pb, Zn by ICP-OES and their speciation in Algerian Mediterranean Sea sediments after a five-stage sequential extraction procedure. Environmental monitoring and assessment 135, 1-3, 265-280.
  • Chen, Z., Canil, D., Longerich, H.P. 2000. Automated in situ trace element analysis of silicate materials by laser ablation inductively coupled plasma mass spectrometry. Fresenius' journal of analytical chemistry 368, 73-78.
  • Dahlquist, R.L, Knoll, J.W. 1978. Inductively coupled plasma-atomic emission spectrometry: analysis of biological materials and soils for major, trace, and ultra-trace elements. Applied Spectroscopy 32, 1-30.
  • Eggins, S.M. 2003. Laser ablation ICP-MS analysis of geological materials prepared as lithium borate glasses. Geostandards Newsletter 27, 147-162.
  • Elburg, M. A., Andersen, T., Bons, P. D., Weisheit, A., Simonsen, S. L., Smet, I. 2012. Metasomatism and metallogeny of A-type granites of the Mt Painter–Mt Babbage Inliers, South Australia. Lithos 151, 83-104.
  • Fedorowich, J. S., Richards, J. P., Jain, J. C., Kerrich, R., Fan, J. 1993. A rapid method for REE and trace-element analysis using laser sampling ICP-MS on direct fusion whole-rock glasses. Chemical Geology 106, 3-4, 229-249.
  • Govindaraju, K. 1994. 1994 compilation of working values and sample description for 383 geostandards. Geostandards newsletter 18, 1-158.
  • Guillong, M., Meier, D. L., Allan, M. M., Heinrich, C. A., Yardley, B. W. 2008. Appendix A6: SILLS: A MATLAB-based program for the reduction of laser ablation ICP-MS data of homogeneous materials and inclusions. Mineralogical Association of Canada Short Course 40, 328-333.
  • Günther, D., Quadt, A. V., Wirz, R., Cousin, H., Dietrich, V. J. 2001. Elemental analyses using laser ablation-inductively coupled plasma-mass spectrometry LA-ICP-MS of geological samples fused with Li2B4O7 and calibrated without matrix-matched standards. Microchimica Acta 136, 3-4, 101-107.
  • Imai, N. 1990. Quantitative analysis of original and powdered rocks and mineral inclusions by laser ablation inductively coupled plasma mass spectrometry. Analytica Chimica Acta 235, 381-391.
  • Jarvis, I., Jarvis, K. E. 1992. Inductively coupled plasma-atomic emission spectrometry in exploration geochemistry. Journal of Geochemical Exploration 44, 1-3, 139-200.
  • Jenner, G. A., Longerich, H. P., Jackson, S. E., Fryer, B. J. 1990. ICP-MS—A powerful tool for high-precision trace-element analysis in Earth sciences: Evidence from analysis of selected USGS reference samples. Chemical Geology 83, 1-2, 133-148.
  • Jochum, K. P., Weis, U., Stoll, B., Kuzmin, D., Yang, Q., Raczek, I., Enzweiler, J. 2011. Determination of reference values for NIST SRM 610–617 glasses following ISO guidelines. Geostandards and Geoanalytical Research 35, 4, 397-429.
  • Jochum, K. P., Weis, U., Schwager, B., Stoll, B., Wilson, S. A., Haug, G. H., Enzweiler, J. 2016 . Reference values following ISO guidelines for frequently requested rock reference materials. Geostandards and Geoanalytical Research 40, 3, 333-350.
  • Kurosawa, M., Shima, K., Ishii, S., Sasa, K. 2006. Trace element analysis of fused whole‐rock glasses by laser ablation‐ICP‐MS and PIXE. Geostandards and Geoanalytical Research 30, 1, 17-30.
  • Liu, Y., Hu, Z., Zong, K., Gao, C., Gao, S., Xu, J., Chen, H. 2010. Reappraisement and refinement of zircon U-Pb isotope and trace element analyses by LA-ICP-MS. Chinese Science Bulletin 55, 15, 1535-1546.
  • Liu, Y., Hu, Z., Li, M., Gao, S. 2013. Applications of LA-ICP-MS in the elemental analyses of geological samples. Chinese Science Bulletin 58, 32, 3863-3878.
  • Longerich, H. P., Jackson, S. E., Günther, D. 1996. Inter-laboratory note. Laser ablation inductively coupled plasma mass spectrometric transient signal data acquisition and analyte concentration calculation. Journal of analytical atomic spectrometry 11, 9, 899-904.
  • Navarro, M. S., Ulbrich, H. H. G. J., Andrade, S., Janasi, V. A. 2002. Adaptation of ICP–OES routine determination techniques for the analysis of rare earth elements by chromatographic separation in geologic materials: tests with reference materials and granitic rocks. Journal of alloys and compounds 344, 1-2, 40-45.
  • Norman, M. D., Pearson, N. J., Sharma, A., Griffin, W. L. 1996. Quantitative analysis of trace elements in geological materials by laser ablation ICPMS: instrumental operating conditions and calibration values of NIST glasses. Geostandards Newsletter 20, 2, 247-261.
  • Pearce, J. A., Harris, N. B., Tindle, A. G. 1984. Trace element discrimination diagrams for the tectonic interpretation of granitic rocks. Journal of petrology 25, 4, 956-983.
  • Petrelli, M., Perugini, D., Alagna, K. E., Poli, G., Peccerillo, A. 2008. Spatially resolved and bulk trace element analysis by laser ablation-inductively coupled plasma-mass spectrometry LA-ICP-MS . Periodico di Mineralogia 77, 3, 3-21.
  • Potts, P. J., Webb, P. C. 1992. X-ray fluorescence spectrometry. Journal of Geochemical Exploration 44, 1-3, 251-296.
  • Shao, F., Niu, Y., Liu, Y., Chen, S., Kong, J., Duan, M. 2017. Petrogenesis of Triassic granitoids in the East Kunlun Orogenic Belt, northern Tibetan Plateau and their tectonic implications. Lithos 282, 33-44.
  • Tamura, A., Akizawa, N., Otsuka, R., Kanayama, K., Python, M., Morishita, T., Arai, S. 2015. Measurement of whole-rock trace-element composition by flux-free fused glass and LA-ICP-MS: evaluation of simple and rapid routine work. Geochemical Journal 49, 3, 243-258.
  • Wilson, S. 2017. USGS microanalytical reference materials MRMS development. Microscopy and Microanalysis 23, 492-493.
  • GEOREM database. http://georem.mpch-mainz.gwdg.de/start.asp?dataversion=current . February 27, 2021.
  • Mendeley Database for Tables. https://data.mendeley.com/datasets/tfxzf3v44s/draft?a=d0b2dfde-46dd-4c6b-b024-ea27310b85e1 . February 27, 2021.
  • Perkin Elmer Syngistix Software. https://www.perkinelmer.com/lab-solutions/resources/docs/PRD_Syngistix-Atomic-Spec-Software-Family_011968_01.pdf . February 27, 2021.

Details

Primary Language English
Subjects Engineering
Journal Section Articles
Authors

Gönenç GÖÇMENGİL (Primary Author)
Geochronology and Geochemistry Laboratory, Faculty of Engineering, Istanbul University-Cerrahpaşa, İstanbul, Turkey
0000-0002-1955-8026
Türkiye


Fatma ŞİŞMAN TÜKEL
Geological Engineering Department, Faculty of Engineering, Istanbul University-Cerrahpaşa, İstanbul, Turkey
0000-0001-2345-6785
Türkiye


Fulya UZUN
Geological Engineering Department, Institute of Graduate Studies, Istanbul University-Cerrahpaşa, İstanbul, Turkey
0000-0003-0105-2083
Türkiye


Marcel GUILLONG This is me
Department of Earth Sciences, Faculty of Engineering, ETH, Zurich, Switzerland
0000-0002-6920-3362
Switzerland


İsak YILMAZ
Geological Engineering Department, Faculty of Engineering, Istanbul University-Cerrahpaşa , İstanbul, Turkey
0000-0003-3313-3275
Türkiye


Namik AYSAL
Geological Engineering Department, Faculty of Engineering, Istanbul University-Cerrahpaşa, İstanbul, Turkey
0000-0001-9669-7305
Türkiye


Nurullah HANİLÇİ
Geological Engineering Department, Faculty of Engineering, Istanbul University-Cerrahpaşa,, İstanbul, Turkey
0000-0002-7720-1551
Türkiye

Supporting Institution Istanbul University - Cerrahpaşa
Project Number 23384
Thanks This work was supported by the Research Funds of the Istanbul University - Cerrahpaşa, project number: 23384.
Early Pub Date November 24, 2021
Publication Date November 23, 2021
Published in Issue Year 2022, Volume early view, Issue early view

Cite

Bibtex @short communication { bulletinofmre947703, journal = {Bulletin of the Mineral Research and Exploration}, issn = {0026-4563}, address = {}, publisher = {Maden Tetkik Arama Genel Müdürlüğü}, year = {2021}, volume = {early view}, number = {early view}, pages = {0 - 0}, doi = {10.19111/bulletinofmre.947703}, title = {Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments}, key = {cite}, author = {Göçmengil, Gönenç and Şişman Tükel, Fatma and Uzun, Fulya and Guıllong, Marcel and Yılmaz, İsak and Aysal, Namik and Hanilçi, Nurullah} }
APA Göçmengil, G. , Şişman Tükel, F. , Uzun, F. , Guıllong, M. , Yılmaz, İ. , Aysal, N. & Hanilçi, N. (2021). Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments . Bulletin of the Mineral Research and Exploration , early view (early view) , 0-0 . DOI: 10.19111/bulletinofmre.947703
MLA Göçmengil, G. , Şişman Tükel, F. , Uzun, F. , Guıllong, M. , Yılmaz, İ. , Aysal, N. , Hanilçi, N. "Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments" . Bulletin of the Mineral Research and Exploration early view (2021 ): 0-0 <https://dergipark.org.tr/en/pub/bulletinofmre/issue/65897/947703>
Chicago Göçmengil, G. , Şişman Tükel, F. , Uzun, F. , Guıllong, M. , Yılmaz, İ. , Aysal, N. , Hanilçi, N. "Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments". Bulletin of the Mineral Research and Exploration early view (2021 ): 0-0
RIS TY - JOUR T1 - Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments AU - Gönenç Göçmengil , Fatma Şişman Tükel , Fulya Uzun , Marcel Guıllong , İsak Yılmaz , Namik Aysal , Nurullah Hanilçi Y1 - 2021 PY - 2021 N1 - doi: 10.19111/bulletinofmre.947703 DO - 10.19111/bulletinofmre.947703 T2 - Bulletin of the Mineral Research and Exploration JF - Journal JO - JOR SP - 0 EP - 0 VL - early view IS - early view SN - 0026-4563- M3 - doi: 10.19111/bulletinofmre.947703 UR - https://doi.org/10.19111/bulletinofmre.947703 Y2 - 2021 ER -
EndNote %0 Bulletin of the Mineral Research and Exploration Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments %A Gönenç Göçmengil , Fatma Şişman Tükel , Fulya Uzun , Marcel Guıllong , İsak Yılmaz , Namik Aysal , Nurullah Hanilçi %T Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments %D 2021 %J Bulletin of the Mineral Research and Exploration %P 0026-4563- %V early view %N early view %R doi: 10.19111/bulletinofmre.947703 %U 10.19111/bulletinofmre.947703
ISNAD Göçmengil, Gönenç , Şişman Tükel, Fatma , Uzun, Fulya , Guıllong, Marcel , Yılmaz, İsak , Aysal, Namik , Hanilçi, Nurullah . "Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments". Bulletin of the Mineral Research and Exploration early view / early view (November 2021): 0-0 . https://doi.org/10.19111/bulletinofmre.947703
AMA Göçmengil G. , Şişman Tükel F. , Uzun F. , Guıllong M. , Yılmaz İ. , Aysal N. , Hanilçi N. Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments. Bull.Min.Res.Exp.. 2021; early view(early view): 0-0.
Vancouver Göçmengil G. , Şişman Tükel F. , Uzun F. , Guıllong M. , Yılmaz İ. , Aysal N. , Hanilçi N. Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments. Bulletin of the Mineral Research and Exploration. 2021; early view(early view): 0-0.
IEEE G. Göçmengil , F. Şişman Tükel , F. Uzun , M. Guıllong , İ. Yılmaz , N. Aysal and N. Hanilçi , "Accurate whole-rock geochemistry analysis by combined ICP-OES and LA-ICP-MS instruments", Bulletin of the Mineral Research and Exploration, vol. early view, no. early view, pp. 0-0, Nov. 2021, doi:10.19111/bulletinofmre.947703

Copyright and Licence
The Bulletin of Mineral Research and Exploration keeps the Law on Intellectual and Artistic Works No: 5846. The Bulletin of Mineral Research and Exploration publishes the articles under the terms of “Creatice Common Attribution-NonCommercial-NoDerivs (CC-BY-NC-ND 4.0)” licence which allows to others to download your works and share them with others as long as they credit you, but they can’t change them in any way or use them commercially.

For further details;
https://creativecommons.org/licenses/?lang=en