SYNTHESIS OF COBALT III ACETATE IN BIPOLAR TRICKLE REACTOR AND PRODUCTION OF POWDER COBALT III ACETATE

Year 2003, Issue: 005, 77 - 85, 15.12.2003

Zakir Poyraz

Abstract

In this study, Cobalt 1II acetate was electrochemically synthesized by using granule

coke electrodes in a bipolar trickle reactor and its regeneration was researched after

using as a catalyst in the oxidation of organic compounds.

The influence of applied voltage. current and the flow rates of electrolyte on the

synthesis data. Current efficiency. time efficiency. energy consumption and volumetime

yield were calculated as a function of time.

Cobalt II acetate was obtained by %27 conversion, the product in the form of

solution was converted into powder product containing %89.2 Cobalt III acetate.

Keywords

Cobalt Ill Acetate, Cobalt II Acetate, Synthesis, Trickle reactor

iKi KUTUPLU DAMLAMALI REAKTORDE KOBAL Till ASETAT SENTEZi ve TOZ KOBALT III ASETAT URETiMi

Abstract

Bu cahsrnada Kobalt III Asetatmm iki kutuplu darnlamah reakrorde; granul kok kornur

elektrot kullanilarak elektrokimyasal sentezi yapilrms ve organik rnaddc in

yukseltgenrnelerinde katalizor olarak kullaruldrktan sonra rejenerasyonu arasunirm,

Sentez verilerine; uygulanan gerilim, akirn elektrolit akis hrzlannm f "si

incelenmistir. Zarnanm bir fonksiyonu olarak akim verirni, zaman vcr imi. enerji,

tuketimi ve hacim zaman verirni hesaplanrrusnr.

Kobalt III asetati %27'lik bir donusurnle elde edilrnis, cozelti halindeki bu urun %89.2

Kobalt III asetau iceren toz urune donusturulmustur.

Keywords

Kobalt III Asetat, Kobalt, ] Asetat, Sentez, Damlamah Reaktor

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