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Gümüş nanomalzeme sentezi ve antimikrobiyal uygulamaları

Year 2019, Volume: 10 Issue: 2, 689 - 695, 20.06.2019
https://doi.org/10.24012/dumf.518897

Abstract

Çevre dostu sentez yöntemlerinin her geçen gün daha etkin olması ve nanopartiküllerin (NP’lerin) kullanım alanlarının yaygınlığı bu yöntemlere olan ilginin oldukça artmasına neden olmaktadır. Biz atık durumunda ki zeytin yapraklarından elde ettiğimiz özüt ile gümüş nano partikülleri (AgNP’leri) basit, ucuz ve çevre dostu bir yöntemle sentezledik. Bu partiküllerin Ultraviyole ve Görünür Işık Absorpsiyon Spektroskopi (UV-Vis.), Fourıer Dönüşümlü Kızılötesi Spektroskopisi (FTIR), X-Işınları Kırınım Cihazı (XRD), Taramalı Elektron Mikroskobu- Enerji Yayılımlı X-ışını (SEM-EDX) ve Termo Gravimetrik (TGA-DTA) analizleri kullanılarak karakterizasyon işlemi yapılmıştır. Antibiyotik dirençliliği günümüz dünyasının ciddi sorunlarından biri bu sebeple elde edilen partiküllerin patojen gram pozitif Staphylococcus aureus ATCC 29213, gram negatif Escherichia coli ATCC 25922 suşları ve Candida albicans mayası üzerinde etkili bir anti-mikrobiyal aktivite gösterdiği tespit edilmiştir. AgNP’lerin MİK (Minimum İnhibisyon Konsantarasyon) değerleri sırası 0.112, 0.028, ve 0.007 olarak bulunmuştur.

References

  • Ahmed, S.W., Anwar, H., Shama, Siddiqui, A., Shah, M.R., Ahmed, A., Ali, S.A., 2018. Synthesis and chemosensing of nitrofurazone using olive oil based silver nanoparticles (O-AgNPs). Sensors Actuators, B Chem.
  • Ali, K., Ahmed, B., Dwivedi, S., Saquib, Q., Al-Khedhairy, A.A., Musarrat, J., 2015. Microwave accelerated green synthesis of stable silver nanoparticles with Eucalyptus globulus leaf extract and their antibacterial and antibiofilm activity on clinical isolates. PLoS One 10, 1–20.
  • Baran M, F., Duz M, Z., Uzan, S., Dolak, brahim, Celik K, S., Kilinc, E., 2018. Removal of Hg(II) from Aqueous Solution by Bacillus subtilis ATCC 6051 (B1). J. Bioprocess. Biotech. 08, 1–7.
  • Dubey, S.P., Lahtinen, M., Sillanpää, M., 2010. Green synthesis and characterizations of silver and gold nanoparticles using leaf extract of Rosa rugosa. Colloids Surfaces A Physicochem. Eng. Asp. 364, 34–41.
  • El-Batal, A.I., Al-Hazmi, N.E., Mosallam, F.M., El-Sayyad, G.S., 2018. Biogenic synthesis of copper nanoparticles by natural polysaccharides and Pleurotus ostreatus fermented fenugreek using gamma rays with antioxidant and antimicrobial potential towards some wound pathogens. Microb. Pathog. 118, 159–169.
  • Kumar, V., Singh, D.K., Mohan, S., Gundampati, R.K., Hasan, S.H., 2017. Photoinduced green synthesis of silver nanoparticles using aqueous extract of Physalis angulata and its antibacterial and antioxidant activity. J. Environ. Chem. Eng. 5, 744–756.
  • Owaid, M.N., Raman, J., Lakshmanan, H., Al-Saeedi, S.S.S., Sabaratnam, V., Ali Abed, I., 2015. Mycosynthesis of silver nanoparticles by Pleurotus cornucopiae var. citrinopileatus and its inhibitory effects against Candida sp. Mater. Lett. 153, 186–190.
  • Saravanakumar, K., Chelliah, R., Shanmugam, S., Varukattu, N.B., Oh, D.H., Kathiresan, K., Wang, M.H., 2018. Green synthesis and characterization of biologically active nanosilver from seed extract of Gardenia jasminoides Ellis. J. Photochem. Photobiol. B Biol.
  • Singh, A.K., Tiwari, R., Kumar, V., Singh, P., Riyazat Khadim, S.K., Tiwari, A., Srivastava, V., Hasan, S.H., Asthana, R.K., 2017. Photo-induced biosynthesis of silver nanoparticles from aqueous extract of Dunaliella salina and their anticancer potential. J. Photochem. Photobiol. B Biol. 166, 202–211.
  • Sreekanth, T.V.M., Jung, M.-J., Eom, I.-Y., 2016. Green synthesis of silver nanoparticles, decorated on graphene oxide nanosheets and their catalytic activity. Appl. Surf. Sci.
  • Swamy, M.K., Akhtar, M.S., Mohanty, S.K., Sinniah, U.R., 2015. Synthesis and characterization of silver nanoparticles using fruit extract of Momordica cymbalaria and assessment of their in vitro antimicrobial, antioxidant and cytotoxicity activities. Spectrochim. Acta - Part A Mol. Biomol. Spectrosc. 151, 939–944.
  • Umamaheswari, C., Lakshmanan, A., Nagarajan, N.S., 2018. Green synthesis, characterization and catalytic degradation studies of gold nanoparticles against congo red and methyl orange. J. Photochem. Photobiol. B Biol. 178, 33–39.
  • Vastrad, J., 2016. Green Synthesis and Characterization of Silver Nanoparticles Using Leaf Extract of Tridax Procumbens 7, 2–6.
  • Yasin, S., Liu, L., Yao, J., 2013. Biosynthesis of Silver Nanoparticles by Bamboo Leaves Extract and Their Antimicrobial Activity. J. Fiber Bioeng. Informatics 1, 77–84.
Year 2019, Volume: 10 Issue: 2, 689 - 695, 20.06.2019
https://doi.org/10.24012/dumf.518897

Abstract

References

  • Ahmed, S.W., Anwar, H., Shama, Siddiqui, A., Shah, M.R., Ahmed, A., Ali, S.A., 2018. Synthesis and chemosensing of nitrofurazone using olive oil based silver nanoparticles (O-AgNPs). Sensors Actuators, B Chem.
  • Ali, K., Ahmed, B., Dwivedi, S., Saquib, Q., Al-Khedhairy, A.A., Musarrat, J., 2015. Microwave accelerated green synthesis of stable silver nanoparticles with Eucalyptus globulus leaf extract and their antibacterial and antibiofilm activity on clinical isolates. PLoS One 10, 1–20.
  • Baran M, F., Duz M, Z., Uzan, S., Dolak, brahim, Celik K, S., Kilinc, E., 2018. Removal of Hg(II) from Aqueous Solution by Bacillus subtilis ATCC 6051 (B1). J. Bioprocess. Biotech. 08, 1–7.
  • Dubey, S.P., Lahtinen, M., Sillanpää, M., 2010. Green synthesis and characterizations of silver and gold nanoparticles using leaf extract of Rosa rugosa. Colloids Surfaces A Physicochem. Eng. Asp. 364, 34–41.
  • El-Batal, A.I., Al-Hazmi, N.E., Mosallam, F.M., El-Sayyad, G.S., 2018. Biogenic synthesis of copper nanoparticles by natural polysaccharides and Pleurotus ostreatus fermented fenugreek using gamma rays with antioxidant and antimicrobial potential towards some wound pathogens. Microb. Pathog. 118, 159–169.
  • Kumar, V., Singh, D.K., Mohan, S., Gundampati, R.K., Hasan, S.H., 2017. Photoinduced green synthesis of silver nanoparticles using aqueous extract of Physalis angulata and its antibacterial and antioxidant activity. J. Environ. Chem. Eng. 5, 744–756.
  • Owaid, M.N., Raman, J., Lakshmanan, H., Al-Saeedi, S.S.S., Sabaratnam, V., Ali Abed, I., 2015. Mycosynthesis of silver nanoparticles by Pleurotus cornucopiae var. citrinopileatus and its inhibitory effects against Candida sp. Mater. Lett. 153, 186–190.
  • Saravanakumar, K., Chelliah, R., Shanmugam, S., Varukattu, N.B., Oh, D.H., Kathiresan, K., Wang, M.H., 2018. Green synthesis and characterization of biologically active nanosilver from seed extract of Gardenia jasminoides Ellis. J. Photochem. Photobiol. B Biol.
  • Singh, A.K., Tiwari, R., Kumar, V., Singh, P., Riyazat Khadim, S.K., Tiwari, A., Srivastava, V., Hasan, S.H., Asthana, R.K., 2017. Photo-induced biosynthesis of silver nanoparticles from aqueous extract of Dunaliella salina and their anticancer potential. J. Photochem. Photobiol. B Biol. 166, 202–211.
  • Sreekanth, T.V.M., Jung, M.-J., Eom, I.-Y., 2016. Green synthesis of silver nanoparticles, decorated on graphene oxide nanosheets and their catalytic activity. Appl. Surf. Sci.
  • Swamy, M.K., Akhtar, M.S., Mohanty, S.K., Sinniah, U.R., 2015. Synthesis and characterization of silver nanoparticles using fruit extract of Momordica cymbalaria and assessment of their in vitro antimicrobial, antioxidant and cytotoxicity activities. Spectrochim. Acta - Part A Mol. Biomol. Spectrosc. 151, 939–944.
  • Umamaheswari, C., Lakshmanan, A., Nagarajan, N.S., 2018. Green synthesis, characterization and catalytic degradation studies of gold nanoparticles against congo red and methyl orange. J. Photochem. Photobiol. B Biol. 178, 33–39.
  • Vastrad, J., 2016. Green Synthesis and Characterization of Silver Nanoparticles Using Leaf Extract of Tridax Procumbens 7, 2–6.
  • Yasin, S., Liu, L., Yao, J., 2013. Biosynthesis of Silver Nanoparticles by Bamboo Leaves Extract and Their Antimicrobial Activity. J. Fiber Bioeng. Informatics 1, 77–84.
There are 14 citations in total.

Details

Primary Language Turkish
Journal Section Articles
Authors

Mehmet Fırat Baran 0000-0001-8133-6670

Abdurrahman Saydut This is me

Adil Umaz 0000-0003-2438-5454

Publication Date June 20, 2019
Submission Date January 28, 2019
Published in Issue Year 2019 Volume: 10 Issue: 2

Cite

IEEE M. F. Baran, A. Saydut, and A. Umaz, “Gümüş nanomalzeme sentezi ve antimikrobiyal uygulamaları”, DUJE, vol. 10, no. 2, pp. 689–695, 2019, doi: 10.24012/dumf.518897.
DUJE tarafından yayınlanan tüm makaleler, Creative Commons Atıf 4.0 Uluslararası Lisansı ile lisanslanmıştır. Bu, orijinal eser ve kaynağın uygun şekilde belirtilmesi koşuluyla, herkesin eseri kopyalamasına, yeniden dağıtmasına, yeniden düzenlemesine, iletmesine ve uyarlamasına izin verir. 24456