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Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments

Year 2016, Volume: 1 Issue: 1, 23 - 32, 02.01.2016

Abstract

This research represents the results of flocculation of quartz particles in suspensions with an anionic flocculant by applying response surface method (RSM). The experiments were designed and carried out according to the Bohn-Behnken Design (BBD) which is a type of RSM. A BBD with five independent parameters at three levels was applied to jar test studies to investigate the effect of variables examined on quartz flocculation process. Flocculant dosage, rapid mixing time, rapid mixing rate, solid ratio and settling time were tested to evaluate the main and interaction effects of these factors on residual turbidity. An empirical quadratic model with a high correlation coefficient was obtained for the estimation of residual turbidity within the investigated ranges of parameters.

References

  • . R. Hogg, “Flocculation and dewatering,” International Journal Mineral Processing, vol. 58, pp. 223-236, 2000.
  • . T. Tripathy and De, B. Ranjan, “Flocculation : A New Way to Treat the Waste Water,” Journal of Physical Sciences, vol. 10, pp. 93-127, 2006.
  • . A. Özkan, H. Uçbeyiay, and S. Düzyol, “Comparison of stages in oil agglomeration process of quartz with sodium oleate in the presence of Ca (II) and Mg(II) ions,” Journal of Colloid and Interface Science, vol. 329, pp. 81-89, 2009.
  • . J. M. Ebeling, P. L. Sibrell, S. R. Ogden and S. T. Summerfelt, “Evaluation of chemical coagulation-/flocculation aids for the removal of suspended solids and phosphorus from intensive recirculating aquaculture effluent discharge,” Aquacultural Engineering, vol. 29, pp. 23-42, 2003.
  • . M. Rossini, J. Garrido and M. Garcia Galluzzo, “Optimization of the coagulation-flocculation treatment influence of rapid mix parameters,” Water Research, vol. 33(8), pp. 1817–1826, 1999.
  • . Ü. İpekoğlu, Dewatering and Methods, İzmir, Turkey: Dokuz Eylül University, Mining Faculty Impress, No: 179, 1997.
  • . J. Gregory, Particles in Water: Properties and Process, London, United Kingdom: University College, 2005.
  • . T. K. Trinh, and L. S. Kang, “Application of response surface method as an experimental design to optimize coagulation tests,” Environmental Engineering Research, vol. 15(2), pp. 63-70, 2010.
  • . M. Zainal-Abideen, A. Aris, F. Yusof, Z. Abdul-Majid, A. Selamat, and S. I. Omar, “Optimizing the Coagulation Process in A Drinking Water Treatment Plant-Comparison Between Traditional and Statistical Experimental Design Jar Tests,” Water Science & Technology, pp. 496-503, 2012.
  • . J. P. Wang, Y. Z.Chen, X. W. Ge, H. Q. Yu, “Optimization of coagulation-flocculation process for a paper-recycling wastewater treatment using response surface methodology,” Colloids and Surfaces A: Physicochem. Eng. Aspects, vol. 302, pp. 204-210, 2007.
  • . T. Taşdemir, and H. Kurama, “Fine Particle Removal from Natural Stone Processing Effluent by Flocculation,” Environmental Progress&Sustainable Energy, vol. 32(2), pp. 317-324, 2013.
  • . E. Sabah, and C. Açıksöz, “Flocculation Performance of Fine Particles in Travertine Slime Suspension,” Physicochemical Problems of Mineral Processing, vol. 48(2), pp. 555-566, 2012.
  • . A. Taşdemir, T. Taşdemir, and H. Kılıç, “Usage of Box-Behnken Experimental Design for The Flocculation of Quartz Suspensions,” in Proc. The 14th Balkan Mineral Processing Congress, 2011, pp. 250-256.
  • . E. Sabah, and Z. E. Erkan, “Interaction mechanism of flocculants with coal waste slurry,” Fuel, vol. 85, pp. 350-359, 2006.
  • . A. Sworska, J. S. Laskowski, G. Cymerman, “Flocculation of the Syncrude fine tailings Part I. Effect of pH, polymer dosage and Mg2+ and Ca2+ cations,” International Journal of Mineral Processing, vol. 60, pp. 143–152, 2000.
  • . P. Somasundaran, and S. Krishnakumar, “Adsorption of surfactants and polymers at the solid-liquid interface,” Colloids Surfaces A: Physicochemical and Engineering Aspects, pp. 491-513, 1997.
  • . M.L. Taylor, G.E. Morrıs, P.G. Self, and R.St.C. Smart, “Kinetics of Adsorption of High Molecular Weight Anionic Polyacrylamide onto Kaolinite: The Flocculation Process,” Journal of Colloid and Interface Science, vol. 250, pp. 28–36, 2002.
  • . J.M. Henderson, and A.D.Wheatley, “Factors Affecting the efficient flocculation of tailings by polacrylamides,” Coal Preparation, vol. 1987(4), pp. 1-49, 2007.
  • . X. Yu, and P. Somasundaran, “Role of Polymer Conformation in Interparticle-Bridging Dominated Flocculation,” Journal of Colloid and Interface Science, vol. 177, pp. 283-287, 1996.
  • . L. Besra, D. K. Sengupta, S. K. Roy, and P. Ay, “Influence of polymer adsorption and conformation on flocculation and dewatering of kaolin suspension,” Separation and Purification Technology, vol. 37, pp. 231-246, 2004.
  • . B. Ersoy, “Effect of pH and polymer charge density on settling rate and turbidity of natural stone suspensions,” International Journal of Mineral Processing, vol. 75, pp. 207 – 216, 2005.
  • . J. Gregory, and L. Guibai, “Effects of dosing and mixing conditions on polymer flocculation of concentrated suspensions,” Chemical Engineering Communications, vol. 108, pp. 3-21, 1991.
  • . M.M. Nourouzi, T.G. Chuah, and T.S.Y. Choong, “Optimization of flocculation process for cut-stone wastewater Effect of rapid mix parameters,” Desalination and Water Treatment, vol. 22, pp. 127-132, 2010.
  • . M. A. Yukselen, and J. Gregory, “The effect of rapid mixing on the break-up and re-formation of flocs,” Journal of Chemical Technology and Biotechnology, vol. 79, pp. 782–788, 2004.
  • . T. Taşdemir, and A. Taşdemir, “Effect of Mixing Conditions on Flocculation” in Proceedings of XIIIth International Mineral Processing Symposium, 2012, pp. 831-837.
  • . A. Sworska, J. S. Laskowskı, and G. Cymerman, “Flocculation of the Syncrude fine tailings Part II. Effect of hydrodynamic conditions,” Int. J. Miner. Process., vol. 60, pp. 153–161, 2000.
  • . M.G. Kılıç, Ç. Hoşten, and Ş. Demirci, “A Parametric Comparative Study of Electrocoagulation and Coagulation Using Ultrafine Quartz Suspensions,” Journal of Hazardous Materials, vol. 171, pp. 247-252, 2009.
  • . D. C. Montgomery, Design and Analysis of Experiments. 5th Edition, Hoboken, New Jersey: John Wiley & Sons, Inc., 2001.
  • . B. Boltoa, and J. Gregory, “Organic polyelectrolytes in water treatment,” Water Research, vol. 41, pp. 2301-2324, 2007.
  • . K. Miyanami, K. Tojo, M. Yokota, Y. Fujiwara, and T. Aratani, “Effect of Mixing on Flocculation,” Ind. Eng. Chem. Fundam., vol. 21, pp. 132-135, 1982.
  • . S. Biggs, M. Habgood, G. J. Jameson, and Y. Yan Y, “Aggregate structures formed via a bridging flocculation mechanism,” Chemical Engineering Journal, vol. 80, pp. 13–22, 2000.
Year 2016, Volume: 1 Issue: 1, 23 - 32, 02.01.2016

Abstract

References

  • . R. Hogg, “Flocculation and dewatering,” International Journal Mineral Processing, vol. 58, pp. 223-236, 2000.
  • . T. Tripathy and De, B. Ranjan, “Flocculation : A New Way to Treat the Waste Water,” Journal of Physical Sciences, vol. 10, pp. 93-127, 2006.
  • . A. Özkan, H. Uçbeyiay, and S. Düzyol, “Comparison of stages in oil agglomeration process of quartz with sodium oleate in the presence of Ca (II) and Mg(II) ions,” Journal of Colloid and Interface Science, vol. 329, pp. 81-89, 2009.
  • . J. M. Ebeling, P. L. Sibrell, S. R. Ogden and S. T. Summerfelt, “Evaluation of chemical coagulation-/flocculation aids for the removal of suspended solids and phosphorus from intensive recirculating aquaculture effluent discharge,” Aquacultural Engineering, vol. 29, pp. 23-42, 2003.
  • . M. Rossini, J. Garrido and M. Garcia Galluzzo, “Optimization of the coagulation-flocculation treatment influence of rapid mix parameters,” Water Research, vol. 33(8), pp. 1817–1826, 1999.
  • . Ü. İpekoğlu, Dewatering and Methods, İzmir, Turkey: Dokuz Eylül University, Mining Faculty Impress, No: 179, 1997.
  • . J. Gregory, Particles in Water: Properties and Process, London, United Kingdom: University College, 2005.
  • . T. K. Trinh, and L. S. Kang, “Application of response surface method as an experimental design to optimize coagulation tests,” Environmental Engineering Research, vol. 15(2), pp. 63-70, 2010.
  • . M. Zainal-Abideen, A. Aris, F. Yusof, Z. Abdul-Majid, A. Selamat, and S. I. Omar, “Optimizing the Coagulation Process in A Drinking Water Treatment Plant-Comparison Between Traditional and Statistical Experimental Design Jar Tests,” Water Science & Technology, pp. 496-503, 2012.
  • . J. P. Wang, Y. Z.Chen, X. W. Ge, H. Q. Yu, “Optimization of coagulation-flocculation process for a paper-recycling wastewater treatment using response surface methodology,” Colloids and Surfaces A: Physicochem. Eng. Aspects, vol. 302, pp. 204-210, 2007.
  • . T. Taşdemir, and H. Kurama, “Fine Particle Removal from Natural Stone Processing Effluent by Flocculation,” Environmental Progress&Sustainable Energy, vol. 32(2), pp. 317-324, 2013.
  • . E. Sabah, and C. Açıksöz, “Flocculation Performance of Fine Particles in Travertine Slime Suspension,” Physicochemical Problems of Mineral Processing, vol. 48(2), pp. 555-566, 2012.
  • . A. Taşdemir, T. Taşdemir, and H. Kılıç, “Usage of Box-Behnken Experimental Design for The Flocculation of Quartz Suspensions,” in Proc. The 14th Balkan Mineral Processing Congress, 2011, pp. 250-256.
  • . E. Sabah, and Z. E. Erkan, “Interaction mechanism of flocculants with coal waste slurry,” Fuel, vol. 85, pp. 350-359, 2006.
  • . A. Sworska, J. S. Laskowski, G. Cymerman, “Flocculation of the Syncrude fine tailings Part I. Effect of pH, polymer dosage and Mg2+ and Ca2+ cations,” International Journal of Mineral Processing, vol. 60, pp. 143–152, 2000.
  • . P. Somasundaran, and S. Krishnakumar, “Adsorption of surfactants and polymers at the solid-liquid interface,” Colloids Surfaces A: Physicochemical and Engineering Aspects, pp. 491-513, 1997.
  • . M.L. Taylor, G.E. Morrıs, P.G. Self, and R.St.C. Smart, “Kinetics of Adsorption of High Molecular Weight Anionic Polyacrylamide onto Kaolinite: The Flocculation Process,” Journal of Colloid and Interface Science, vol. 250, pp. 28–36, 2002.
  • . J.M. Henderson, and A.D.Wheatley, “Factors Affecting the efficient flocculation of tailings by polacrylamides,” Coal Preparation, vol. 1987(4), pp. 1-49, 2007.
  • . X. Yu, and P. Somasundaran, “Role of Polymer Conformation in Interparticle-Bridging Dominated Flocculation,” Journal of Colloid and Interface Science, vol. 177, pp. 283-287, 1996.
  • . L. Besra, D. K. Sengupta, S. K. Roy, and P. Ay, “Influence of polymer adsorption and conformation on flocculation and dewatering of kaolin suspension,” Separation and Purification Technology, vol. 37, pp. 231-246, 2004.
  • . B. Ersoy, “Effect of pH and polymer charge density on settling rate and turbidity of natural stone suspensions,” International Journal of Mineral Processing, vol. 75, pp. 207 – 216, 2005.
  • . J. Gregory, and L. Guibai, “Effects of dosing and mixing conditions on polymer flocculation of concentrated suspensions,” Chemical Engineering Communications, vol. 108, pp. 3-21, 1991.
  • . M.M. Nourouzi, T.G. Chuah, and T.S.Y. Choong, “Optimization of flocculation process for cut-stone wastewater Effect of rapid mix parameters,” Desalination and Water Treatment, vol. 22, pp. 127-132, 2010.
  • . M. A. Yukselen, and J. Gregory, “The effect of rapid mixing on the break-up and re-formation of flocs,” Journal of Chemical Technology and Biotechnology, vol. 79, pp. 782–788, 2004.
  • . T. Taşdemir, and A. Taşdemir, “Effect of Mixing Conditions on Flocculation” in Proceedings of XIIIth International Mineral Processing Symposium, 2012, pp. 831-837.
  • . A. Sworska, J. S. Laskowskı, and G. Cymerman, “Flocculation of the Syncrude fine tailings Part II. Effect of hydrodynamic conditions,” Int. J. Miner. Process., vol. 60, pp. 153–161, 2000.
  • . M.G. Kılıç, Ç. Hoşten, and Ş. Demirci, “A Parametric Comparative Study of Electrocoagulation and Coagulation Using Ultrafine Quartz Suspensions,” Journal of Hazardous Materials, vol. 171, pp. 247-252, 2009.
  • . D. C. Montgomery, Design and Analysis of Experiments. 5th Edition, Hoboken, New Jersey: John Wiley & Sons, Inc., 2001.
  • . B. Boltoa, and J. Gregory, “Organic polyelectrolytes in water treatment,” Water Research, vol. 41, pp. 2301-2324, 2007.
  • . K. Miyanami, K. Tojo, M. Yokota, Y. Fujiwara, and T. Aratani, “Effect of Mixing on Flocculation,” Ind. Eng. Chem. Fundam., vol. 21, pp. 132-135, 1982.
  • . S. Biggs, M. Habgood, G. J. Jameson, and Y. Yan Y, “Aggregate structures formed via a bridging flocculation mechanism,” Chemical Engineering Journal, vol. 80, pp. 13–22, 2000.
There are 31 citations in total.

Details

Journal Section Makaleler
Authors

Adem Taşdemir

Tuba Taşdemir

Publication Date January 2, 2016
Published in Issue Year 2016 Volume: 1 Issue: 1

Cite

APA Taşdemir, A., & Taşdemir, T. (2016). Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments. European Journal of Engineering and Natural Sciences, 1(1), 23-32.
AMA Taşdemir A, Taşdemir T. Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments. European Journal of Engineering and Natural Sciences. January 2016;1(1):23-32.
Chicago Taşdemir, Adem, and Tuba Taşdemir. “Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments”. European Journal of Engineering and Natural Sciences 1, no. 1 (January 2016): 23-32.
EndNote Taşdemir A, Taşdemir T (January 1, 2016) Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments. European Journal of Engineering and Natural Sciences 1 1 23–32.
IEEE A. Taşdemir and T. Taşdemir, “Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments”, European Journal of Engineering and Natural Sciences, vol. 1, no. 1, pp. 23–32, 2016.
ISNAD Taşdemir, Adem - Taşdemir, Tuba. “Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments”. European Journal of Engineering and Natural Sciences 1/1 (January 2016), 23-32.
JAMA Taşdemir A, Taşdemir T. Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments. European Journal of Engineering and Natural Sciences. 2016;1:23–32.
MLA Taşdemir, Adem and Tuba Taşdemir. “Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments”. European Journal of Engineering and Natural Sciences, vol. 1, no. 1, 2016, pp. 23-32.
Vancouver Taşdemir A, Taşdemir T. Determination of the Effects of Operating Parameters on the Residual Turbidity of Quartz Suspensions by Design of Experiments. European Journal of Engineering and Natural Sciences. 2016;1(1):23-32.