Year 2020, Volume 7 , Issue 2, Pages 127 - 131 2020-08-15

Synthesize of low price stationary phases with permanent groups for reversed-phase liquid chromatography (RP-HPLC) has gained great importance in the past several years. In chromatographic analyses, silica gels are commonly used as a supporting material as they give high mechanical strength and swelling resistance. Additionally, different particle and pore size availability and low cost makes these materials one of the most suitable stationary phase. In this work, chemically bonded C8 phase was synthesized by sol-gel route and instead of toxic silicone alkoxides, non-toxic water glass was chosen as a precursor. Linking process of C8 groups to silica gel was carried out by trimethoxy(octyl)silane. The end-capping and C8 binding procedure was analyzed by Fourier transform infrared (FTIR) spectroscopy and morphology of C8 particles were characterized by scanning electron microscope (SEM).
Water glass, C8 packing material, HPLC
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Primary Language en
Subjects Engineering
Journal Section Research Articles
Authors

Orcid: 0000-0003-1368-5689
Author: Abdullah AKSU
Institution: ISTANBUL UNIVERSITY
Country: Turkey


Orcid: 0000-0002-6284-1337
Author: Ömer Suat TAŞKIN
Institution: ISTANBUL UNIVERSITY
Country: Turkey


Orcid: 0000-0001-8207-238X
Author: Mehmet Emre ÇETİNTASOGLU (Primary Author)
Institution: ISTANBUL UNIVERSITY
Country: Turkey


Orcid: 0000-0002-9492-5105
Author: Nagihan ERSOY KORKMAZ ERSOY
Institution: ISTANBUL UNIVERSITY
Country: Turkey


Orcid: 0000-0003-0227-5203
Author: Cihan TORLAK
Institution: ISTANBUL UNIVERSITY
Country: Turkey


Orcid: 0000-0001-7608-6339
Author: Nuray ÇAĞLAR BALKIS
Institution: ISTANBUL UNIVERSITY
Country: Turkey


Supporting Institution Scientific Research Projects Unit of Istanbul University
Project Number BYP-2018-28592
Thanks The authors thank Scientific Research Projects Unit of Istanbul University for their supports to BYP-2018- 28592 numbered project about this study.
Dates

Publication Date : August 15, 2020

Bibtex @research article { ijegeo700599, journal = {International Journal of Environment and Geoinformatics}, issn = {}, eissn = {2148-9173}, address = {}, publisher = {Cem GAZİOĞLU}, year = {2020}, volume = {7}, pages = {127 - 131}, doi = {10.30897/ijegeo.700599}, title = {Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass}, key = {cite}, author = {Aksu, Abdullah and Taşkın, Ömer Suat and Çeti̇ntasoglu, Mehmet Emre and Ersoy Korkmaz, Nagihan and Torlak, Cihan and Çağlar, Nuray} }
APA Aksu, A , Taşkın, Ö , Çeti̇ntasoglu, M , Ersoy Korkmaz, N , Torlak, C , Çağlar, N . (2020). Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass . International Journal of Environment and Geoinformatics , 7 (2) , 127-131 . DOI: 10.30897/ijegeo.700599
MLA Aksu, A , Taşkın, Ö , Çeti̇ntasoglu, M , Ersoy Korkmaz, N , Torlak, C , Çağlar, N . "Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass" . International Journal of Environment and Geoinformatics 7 (2020 ): 127-131 <https://dergipark.org.tr/en/pub/ijegeo/issue/54146/700599>
Chicago Aksu, A , Taşkın, Ö , Çeti̇ntasoglu, M , Ersoy Korkmaz, N , Torlak, C , Çağlar, N . "Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass". International Journal of Environment and Geoinformatics 7 (2020 ): 127-131
RIS TY - JOUR T1 - Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass AU - Abdullah Aksu , Ömer Suat Taşkın , Mehmet Emre Çeti̇ntasoglu , Nagihan Ersoy Korkmaz , Cihan Torlak , Nuray Çağlar Y1 - 2020 PY - 2020 N1 - doi: 10.30897/ijegeo.700599 DO - 10.30897/ijegeo.700599 T2 - International Journal of Environment and Geoinformatics JF - Journal JO - JOR SP - 127 EP - 131 VL - 7 IS - 2 SN - -2148-9173 M3 - doi: 10.30897/ijegeo.700599 UR - https://doi.org/10.30897/ijegeo.700599 Y2 - 2020 ER -
EndNote %0 International Journal of Environment and Geoinformatics Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass %A Abdullah Aksu , Ömer Suat Taşkın , Mehmet Emre Çeti̇ntasoglu , Nagihan Ersoy Korkmaz , Cihan Torlak , Nuray Çağlar %T Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass %D 2020 %J International Journal of Environment and Geoinformatics %P -2148-9173 %V 7 %N 2 %R doi: 10.30897/ijegeo.700599 %U 10.30897/ijegeo.700599
ISNAD Aksu, Abdullah , Taşkın, Ömer Suat , Çeti̇ntasoglu, Mehmet Emre , Ersoy Korkmaz, Nagihan , Torlak, Cihan , Çağlar, Nuray . "Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass". International Journal of Environment and Geoinformatics 7 / 2 (August 2020): 127-131 . https://doi.org/10.30897/ijegeo.700599
AMA Aksu A , Taşkın Ö , Çeti̇ntasoglu M , Ersoy Korkmaz N , Torlak C , Çağlar N . Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. International Journal of Environment and Geoinformatics. 2020; 7(2): 127-131.
Vancouver Aksu A , Taşkın Ö , Çeti̇ntasoglu M , Ersoy Korkmaz N , Torlak C , Çağlar N . Preparation of Silica based C8 Packing Material from Non-Toxic Water Glass. International Journal of Environment and Geoinformatics. 2020; 7(2): 127-131.