Research Article
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Year 2024, Volume: 1 Issue: 1, 7 - 11, 26.07.2024

Abstract

References

  • Abdulhameed, O., Al-Ahmari, A., Ameen, W., & Mian, S. H. (2019). Additive manufacturing: Challenges, trends, and applications. Advances in Mechanical Engineering, 11(2), 1687814018822880.
  • Chung, H., & Das, S. (2008). Functionally graded Nylon-11/silica nanocomposites produced by selective laser sintering. Materials Science and Engineering: A, 487(1-2), 251-257.
  • Chunze, Y., Yusheng, S., Jinsong, Y., & Jinhui, L. (2009). A nanosilica/nylon-12 composite powder for selective laser sintering. Journal of Reinforced Plastics and Composites, 28(23), 2889-2902.
  • Deckard, C. R. (1988). Selective Laser Sintering.
  • Espera, A. H., Dizon, J. R. C., Chen, Q., & Advincula, R. C. (2019). 3D-printing and advanced manufacturing for electronics. Progress in Additive Manufacturing, 4, 245-267.
  • Gibson, I., & Shi, D. (1997). Material properties and fabrication parameters in selective laser sintering process. Rapid prototyping journal, 3(4), 129-136.
  • Gu, D. (2015). Laser additive manufacturing of high-performance materials. Springer.
  • Han, W., Kong, L., & Xu, M. (2022). Advances in selective laser sintering of polymers. International Journal of Extreme Manufacturing, 4(4), 042002.
  • Marcus, H. L., Beeman, J. J., Barlow, J. W., Bourell, D. L., & Crawford, R. H. (1993). Solid Freeform Fabrication Symposium Proceedings Held in Austin, Texas on August 9-11, 1993.
  • ISO, I. (2016). 11357-1 Plastics—Differential Scanning Calorimetry (DSC) Part 1: General Principles. International Organization for Standardization: Geneva, Switzerland.
  • Kerns, J. (2015). What’s the difference between stereolithography and selective laser sintering. Machine Design, 17.
  • Kim, G. D., & Oh, Y. T. (2008). A benchmark study on rapid prototyping processes and machines: quantitative comparisons of mechanical properties, accuracy, roughness, speed, and material cost. Proceedings of the Institution of Mechanical Engineers, Part B: Journal of Engineering Manufacture, 222(2), 201-215.
  • Mohanavel, V., Ali, K. A., Ranganathan, K., Jeffrey, J. A., Ravikumar, M. M., & Rajkumar, S. (2021). The roles and applications of additive manufacturing in the aerospace and automobile sector. Materials Today: Proceedings, 47, 405-409.
  • Monfared, V., Bakhsheshi-Rad, H. R., Ramakrishna, S., Razzaghi, M., & Berto, F. (2021). A Brief Review on Additive Manufacturing of Polymeric Composites and Nanocomposites. Micromachines 2021, 12, 704.
  • Mousa, A. A. (2014). The Effects of Content and Surface Modification of Filler on the Mechanical Properties of Selective Laser Sintered Polyamide12 Composites. Jordan Journal of Mechanical & Industrial Engineering, 8(5), 265 - 274.
  • Özbay, B., & Serhatlı, İ. E. (2022). Processing and characterization of hollow glass-filled polyamide 12 composites by selective laser sintering method. Materials Technology, 37(4), 213-223.
  • Özbay, B., Bekem, A., Serhatlı, İ. E., Öztürk, S., & Bulduk, M. E. (2022). Effects of copper fillers on mechanical and electrical properties of selective laser sintered PA 12-Cu composites. Materials Technology, 37(10), 1541–1553.
  • Sachs, E., Cima, M., & Cornie, J. (1990). Three-dimensional printing: rapid tooling and prototypes directly from a CAD model. CIRP annals, 39(1), 201-204.
  • Wudy, K., & Drummer, D. (2019). Infiltration behavior of thermosets for use in a combined selective laser sintering process of polymers. JOM, 71(3), 920-927.

Characterization of PA 12 Matrix Composites Produced by Selective Laser Sintering Method

Year 2024, Volume: 1 Issue: 1, 7 - 11, 26.07.2024

Abstract

The Selective Laser Sintering (SLS) method is a promising additive manufacturing (AM) technique for the production of thermoplastic polymers and polymer composite materials. Polyamides, Polyamide 12 (PA 12) and Polyamide 11 (PA 11), followed by Polyamide 6 (PA 6), are the most widely used matrix materials for the SLS AM method. Various additives are made from polymer materials to provide the desired physical, mechanical, and tribological properties. In this study, composites with PA 12 matrix were produced by SLS method with 20% hollow ceramic microsphere (W) reinforcement. Before production, PA 12 and ceramic additives were mixed by dry mixing method with a rotary tumbler. Then, thermal analysis ((Differential Scanning Microscopy (DSC) and Thermogravimetric Analysis (TGA)) was performed to characterize the thermal properties of the powder mixture. One of the most important factors affecting SLS production is the production parameters. In this study, composite samples and virgin PA 12 were produced with various SLS production parameters such as laser energy, scanning speed and hatch distance, and the effect of energy values on physical and mechanical properties were investigated. The mechanical properties of the samples were determined by impact tests. Also, the fracture surfaces of the studied samples were analysed.

Ethical Statement

The authors declare no conflict of interest.

Supporting Institution

This project was supported by Yıldız Technical University Scientific Research Projects (YTU-BAPK) with project number FYL-2023-6036. This study was also supported by Fatih Sultan Mehmet Vakif University, Aluminum Test, Training and Research Center.

References

  • Abdulhameed, O., Al-Ahmari, A., Ameen, W., & Mian, S. H. (2019). Additive manufacturing: Challenges, trends, and applications. Advances in Mechanical Engineering, 11(2), 1687814018822880.
  • Chung, H., & Das, S. (2008). Functionally graded Nylon-11/silica nanocomposites produced by selective laser sintering. Materials Science and Engineering: A, 487(1-2), 251-257.
  • Chunze, Y., Yusheng, S., Jinsong, Y., & Jinhui, L. (2009). A nanosilica/nylon-12 composite powder for selective laser sintering. Journal of Reinforced Plastics and Composites, 28(23), 2889-2902.
  • Deckard, C. R. (1988). Selective Laser Sintering.
  • Espera, A. H., Dizon, J. R. C., Chen, Q., & Advincula, R. C. (2019). 3D-printing and advanced manufacturing for electronics. Progress in Additive Manufacturing, 4, 245-267.
  • Gibson, I., & Shi, D. (1997). Material properties and fabrication parameters in selective laser sintering process. Rapid prototyping journal, 3(4), 129-136.
  • Gu, D. (2015). Laser additive manufacturing of high-performance materials. Springer.
  • Han, W., Kong, L., & Xu, M. (2022). Advances in selective laser sintering of polymers. International Journal of Extreme Manufacturing, 4(4), 042002.
  • Marcus, H. L., Beeman, J. J., Barlow, J. W., Bourell, D. L., & Crawford, R. H. (1993). Solid Freeform Fabrication Symposium Proceedings Held in Austin, Texas on August 9-11, 1993.
  • ISO, I. (2016). 11357-1 Plastics—Differential Scanning Calorimetry (DSC) Part 1: General Principles. International Organization for Standardization: Geneva, Switzerland.
  • Kerns, J. (2015). What’s the difference between stereolithography and selective laser sintering. Machine Design, 17.
  • Kim, G. D., & Oh, Y. T. (2008). A benchmark study on rapid prototyping processes and machines: quantitative comparisons of mechanical properties, accuracy, roughness, speed, and material cost. Proceedings of the Institution of Mechanical Engineers, Part B: Journal of Engineering Manufacture, 222(2), 201-215.
  • Mohanavel, V., Ali, K. A., Ranganathan, K., Jeffrey, J. A., Ravikumar, M. M., & Rajkumar, S. (2021). The roles and applications of additive manufacturing in the aerospace and automobile sector. Materials Today: Proceedings, 47, 405-409.
  • Monfared, V., Bakhsheshi-Rad, H. R., Ramakrishna, S., Razzaghi, M., & Berto, F. (2021). A Brief Review on Additive Manufacturing of Polymeric Composites and Nanocomposites. Micromachines 2021, 12, 704.
  • Mousa, A. A. (2014). The Effects of Content and Surface Modification of Filler on the Mechanical Properties of Selective Laser Sintered Polyamide12 Composites. Jordan Journal of Mechanical & Industrial Engineering, 8(5), 265 - 274.
  • Özbay, B., & Serhatlı, İ. E. (2022). Processing and characterization of hollow glass-filled polyamide 12 composites by selective laser sintering method. Materials Technology, 37(4), 213-223.
  • Özbay, B., Bekem, A., Serhatlı, İ. E., Öztürk, S., & Bulduk, M. E. (2022). Effects of copper fillers on mechanical and electrical properties of selective laser sintered PA 12-Cu composites. Materials Technology, 37(10), 1541–1553.
  • Sachs, E., Cima, M., & Cornie, J. (1990). Three-dimensional printing: rapid tooling and prototypes directly from a CAD model. CIRP annals, 39(1), 201-204.
  • Wudy, K., & Drummer, D. (2019). Infiltration behavior of thermosets for use in a combined selective laser sintering process of polymers. JOM, 71(3), 920-927.
There are 19 citations in total.

Details

Primary Language English
Subjects Polymer Technologies, Materials Engineering (Other)
Journal Section Research Articles
Authors

Umut Can Cingöz

Burçin Özbay 0000-0001-5479-8474

Alptekin Kısasöz 0000-0001-8531-8162

Publication Date July 26, 2024
Submission Date March 19, 2024
Acceptance Date April 24, 2024
Published in Issue Year 2024 Volume: 1 Issue: 1

Cite

APA Cingöz, U. C., Özbay, B., & Kısasöz, A. (2024). Characterization of PA 12 Matrix Composites Produced by Selective Laser Sintering Method. ITU Journal of Metallurgy and Materials Engineering, 1(1), 7-11.