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Synthesis, Spectroscopic and Thermal Properties of N,N'-Diethylnicotinamide Metal Complexes of 4-Formylbenzoic Acid

Year 2014, Volume: 7 Issue: 1, 48 - 59, 31.12.2014

Abstract

In this study, metal complexes of 4-formylbenzoate containing N,N’diethylnicotinamide were synthesized. Elemental analysis and IR Spectroscopy methods were used for the illuminate of the structures of complexes. By using TGDTG, DTA thermic analysis method in nitrogen atmosphere between 20-1000 °C heat, thermal features of complexes which are made syntehisis was spantenrausly studred. 

References

  • Barcalay J.A.and Kennard O.H. 1961. J.Chem.Soc., 12, s5224.
  • Daniels J. Et al. 1999. “Fluorescence characterisation and analysis of 4-carboxybenzaldehhyde, a colour precursor to the manufacture of trephthalic acid”, polymer degradation and stability 65(3): s347-s353
  • Dey D., Roy S., Dutta Purkayastha R.N., Pallepogu R., Male L., Mckee V. 2011. Syntheses, characterization, and crystal structures of two zinc(II) carboxylates containing pyridine. Journal of Coordination Chemistry, 64, 1165-1176.

4-Formilbenzoik Asitin N,N’-Dietilnikotinamid Metal Komplekslerinin Sentezi, Spektroskopik ve Termal Özellikleri

Year 2014, Volume: 7 Issue: 1, 48 - 59, 31.12.2014

Abstract

Bu
çalışmada Kobalt(II), Nikel(II), Mangan(II), Çinko(II), Kadmiyum(II) ve
Bakır(II) metallerinin 4-formilbenzoat ile N,N’-dietilnikotinamid’li
komplekslerinden oluşan altı adet kompleks sentezlenmiştir. Komplekslerin
yapılarını aydınlatmak için elementel analiz, FTIR spektroskopisi yöntemleri
kullanılmıştır. 20-1000 oC sıcaklık aralığında azot atmosferinde
TG-DTG-DTA termik analiz metodu kullanılarak, sentezlenen komplekslerin termal
özellikleri eş zamanlı incelendi. 

References

  • Barcalay J.A.and Kennard O.H. 1961. J.Chem.Soc., 12, s5224.
  • Daniels J. Et al. 1999. “Fluorescence characterisation and analysis of 4-carboxybenzaldehhyde, a colour precursor to the manufacture of trephthalic acid”, polymer degradation and stability 65(3): s347-s353
  • Dey D., Roy S., Dutta Purkayastha R.N., Pallepogu R., Male L., Mckee V. 2011. Syntheses, characterization, and crystal structures of two zinc(II) carboxylates containing pyridine. Journal of Coordination Chemistry, 64, 1165-1176.
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Details

Primary Language Turkish
Subjects Engineering
Journal Section Articles
Authors

Mustafa Sertçelik

Hacali Necefoğlu

Publication Date December 31, 2014
Submission Date August 13, 2017
Published in Issue Year 2014 Volume: 7 Issue: 1

Cite

APA Sertçelik, M., & Necefoğlu, H. (2014). 4-Formilbenzoik Asitin N,N’-Dietilnikotinamid Metal Komplekslerinin Sentezi, Spektroskopik ve Termal Özellikleri. Kafkas Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 7(1), 48-59.