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An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals

Year 2021, Volume: 60 Issue: 3, 169 - 174, 01.09.2021
https://doi.org/10.30797/madencilik.800948

Abstract

Flotation behavior of a lead ore sample containing both sulfide and oxide Pb minerals taken from transition zone was investigated. Detailed mineralogical analyses were conducted to determine the type of lead and gangue minerals. The results revealed that galena, cerussite and pulmbogummite were the major lead minerals and observed in close association. In the flotation tests, following determination of the optimum particle size, effects of sulfidization, type of collector, and frother were examined. Potassium amyl xanthate, a modified mercaptan (Aero 412), and and the frother (Dow250) produced the best results. Use of Flash flotation was tested to reduce the flotation time and recover the fast floating liberated galena particles at coarse particle size. A locked cycle flotation test was conducted using the optimum flotation conditions to determine grade and recovery of the final concentrate that can be produced in plant scale operation.

References

  • Abkhoshk, E., Jorjani, E., Al-Harahsheh, M., Rashchi, F., & Naazari, M. 2014. Review of the Hydrometallurgical Processing of Non-Sulfide Zinc Ores. Hydrometallurgy, 153-167.
  • Bulatovic, S. 2010. Handbook of Flotation Reagent Chemistry, Theory and Practice Volume 2: Flotation of Gold, PGM and Oxide Minerals. Elsevier.
  • Drzymala, J. 2007. Mineral Processing Foundations of Theory and Practices of Minerallugy.
  • Fa, K., Miller, J., Jiang , T., & Li, G. 2005. Sulphidization Flotation for Recovery of Lead and Zinc from Oxide-Sulfide Ores. Trans. Nonferrous Met. Soc. China, 1138-1144.
  • Fuerstenau, M. C., Olivas, S. A., Herrera-Urbina, R., & Han, K. N. 1987. The surface characteristics and flotation behavior of anglesite and cerussite. International journal of mineral processing, 20(1-2), 73-85.
  • Herrera-Urbina, R., Sotillo, F., & Fuerstenau, D. 1998. Amyl Xanthate Uptake by Natural and Sulfide-Treated Cerussite and Galena. International Journal of Mineral Processing, 113-128.
  • Herrera-Urbina, R., Sotillo, F. J., & Fuerstenau, D. W. 1999. Effect of sodium sulfide additions on the pulp potential and amyl xanthate flotation of cerussite and galena. International Journal of Mineral Processing, 55(3), 157-170.
  • Liu, C., Zhang, W., Song, S., Li, H., & Jiao, X. 2019. A novel insight of the effect of sodium chloride on the sulfidization flotation of cerussite. Powder Technology, 344, 103-107.
  • Marabini, A., Ciriachi, M., Plescia, P., & Barbaro, M. 2007. Chelating Reagents for Flotation. Minerals Engineering, 1014-1025.Mining Chemicals Handbook, 2002. Cytec Industries Inc
  • Onal, G., Bulut, G., Gul, A., Kangal, O., Perek, K.T. and Arslan, F., 2005, Flotation of Aladag oxide lead–zinc ores, Minerals Engineering 18 (2005), 279–282.
  • Popov, S. R., & Vučinić, D. R. 1994. Kinetics of ethylxanthate adsorption on cerussite in alkaline media in presence or absence of dissolved lead ions. International journal of mineral processing, 41(1-2), 115-128.
  • Somasundaran, P., Lou, A. 1999. Oxide Mineral Flotation Fundementals. In B. K. Parekh, & J. D. Miller, Advances in Flotation Technology Society for Mining, Metallurgy and Exploration, Inc s. 23-43.
  • Wills, B., Napier-Munn, T. 2006. Wills' Mineral Processing Technology An Introduction to the Practical Aspects of Ore Treatment and Mineral Recovery. Elsevier Science & Technology Books.
  • Liu, R., Liu, D., Li, J., Liu, S., Liu, Z., Gao, L., ... & Ao, S. 2020. Improved understanding of the sulfidization mechanism in cerussite flotation: An XPS, ToF-SIMS and FESEM investigation. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 124508.

An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals

Year 2021, Volume: 60 Issue: 3, 169 - 174, 01.09.2021
https://doi.org/10.30797/madencilik.800948

Abstract

Bu çalışmada hem sülfürlü hem de oksit yapıdaki Pb minerallerini barındıran, geçiş zonuna ait bir kurşun cevherinin flotasyon davranışı incelenmiştir. Detaylı bir mineraloji analizi yapılarak kurşun ve gang mineralleri tespit edilmiştir. Kurşun minerallerinden galen ve serüzit ile birlikte plumbogummit belirlenmiş olup, oksit ve sülfürlü kurşun minerallerinin birlikte bulunduğu bir yapı görülmektedir. Flotasyon testlerinde, öncelikle tane boyutunun etkisi incelenmiş, daha sonra sülfürleştirici, toplayıcı ve köpürtücü reaktiflerin türlerinin kurşun flotasyon üzerindeki etkisi araştırılmıştır. Flotasyon testlerinde potasyum amil ksantat, modifiye merkaptan (Aero 412) ve köpürtücü (Dow250) birlikte kullanıldığı durumda en yüksek verime ulaşılmıştır. Flotasyon süresini kısaltmak ve görece iri boyutta serbestleşen kurşun tanelerinin yüzdürülmesi amacıyla flaş flotasyonun etkisi araştırılarak en uygun açık devre tasarımı yapılmıştır. En iyi flotasyon performansının elde edildiği koşularda kapalı devre flotasyon testi yapılmış ve tesis koşullarında elde edilebilecek nihai konsantre tenör ve verimleri belirlenmiştir.

Thanks

Çalışmaya katkılarından dolayı Prof. Dr. Zafir Ekmekçi’ye teşekkür ederiz.

References

  • Abkhoshk, E., Jorjani, E., Al-Harahsheh, M., Rashchi, F., & Naazari, M. 2014. Review of the Hydrometallurgical Processing of Non-Sulfide Zinc Ores. Hydrometallurgy, 153-167.
  • Bulatovic, S. 2010. Handbook of Flotation Reagent Chemistry, Theory and Practice Volume 2: Flotation of Gold, PGM and Oxide Minerals. Elsevier.
  • Drzymala, J. 2007. Mineral Processing Foundations of Theory and Practices of Minerallugy.
  • Fa, K., Miller, J., Jiang , T., & Li, G. 2005. Sulphidization Flotation for Recovery of Lead and Zinc from Oxide-Sulfide Ores. Trans. Nonferrous Met. Soc. China, 1138-1144.
  • Fuerstenau, M. C., Olivas, S. A., Herrera-Urbina, R., & Han, K. N. 1987. The surface characteristics and flotation behavior of anglesite and cerussite. International journal of mineral processing, 20(1-2), 73-85.
  • Herrera-Urbina, R., Sotillo, F., & Fuerstenau, D. 1998. Amyl Xanthate Uptake by Natural and Sulfide-Treated Cerussite and Galena. International Journal of Mineral Processing, 113-128.
  • Herrera-Urbina, R., Sotillo, F. J., & Fuerstenau, D. W. 1999. Effect of sodium sulfide additions on the pulp potential and amyl xanthate flotation of cerussite and galena. International Journal of Mineral Processing, 55(3), 157-170.
  • Liu, C., Zhang, W., Song, S., Li, H., & Jiao, X. 2019. A novel insight of the effect of sodium chloride on the sulfidization flotation of cerussite. Powder Technology, 344, 103-107.
  • Marabini, A., Ciriachi, M., Plescia, P., & Barbaro, M. 2007. Chelating Reagents for Flotation. Minerals Engineering, 1014-1025.Mining Chemicals Handbook, 2002. Cytec Industries Inc
  • Onal, G., Bulut, G., Gul, A., Kangal, O., Perek, K.T. and Arslan, F., 2005, Flotation of Aladag oxide lead–zinc ores, Minerals Engineering 18 (2005), 279–282.
  • Popov, S. R., & Vučinić, D. R. 1994. Kinetics of ethylxanthate adsorption on cerussite in alkaline media in presence or absence of dissolved lead ions. International journal of mineral processing, 41(1-2), 115-128.
  • Somasundaran, P., Lou, A. 1999. Oxide Mineral Flotation Fundementals. In B. K. Parekh, & J. D. Miller, Advances in Flotation Technology Society for Mining, Metallurgy and Exploration, Inc s. 23-43.
  • Wills, B., Napier-Munn, T. 2006. Wills' Mineral Processing Technology An Introduction to the Practical Aspects of Ore Treatment and Mineral Recovery. Elsevier Science & Technology Books.
  • Liu, R., Liu, D., Li, J., Liu, S., Liu, Z., Gao, L., ... & Ao, S. 2020. Improved understanding of the sulfidization mechanism in cerussite flotation: An XPS, ToF-SIMS and FESEM investigation. Colloids and Surfaces A: Physicochemical and Engineering Aspects, 124508.
There are 14 citations in total.

Details

Primary Language Turkish
Subjects Geological Sciences and Engineering (Other)
Journal Section Technical Notes
Authors

Mete Tayhan Serdengeçti 0000-0001-9651-2980

Bekir Başkurt This is me 0000-0003-1715-8667

Kaan Özçelik This is me 0000-0001-6476-5895

Hüseyin Baştürkcü This is me 0000-0001-7301-9317

Publication Date September 1, 2021
Submission Date September 28, 2020
Published in Issue Year 2021 Volume: 60 Issue: 3

Cite

APA Serdengeçti, M. T., Başkurt, B., Özçelik, K., Baştürkcü, H. (2021). An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals. Bilimsel Madencilik Dergisi, 60(3), 169-174. https://doi.org/10.30797/madencilik.800948
AMA Serdengeçti MT, Başkurt B, Özçelik K, Baştürkcü H. An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals. Mining. September 2021;60(3):169-174. doi:10.30797/madencilik.800948
Chicago Serdengeçti, Mete Tayhan, Bekir Başkurt, Kaan Özçelik, and Hüseyin Baştürkcü. “An Investigation on Characterization and Floation Behavior of a Transitional Ore Containing Galena and Pb Oxide Minerals”. Bilimsel Madencilik Dergisi 60, no. 3 (September 2021): 169-74. https://doi.org/10.30797/madencilik.800948.
EndNote Serdengeçti MT, Başkurt B, Özçelik K, Baştürkcü H (September 1, 2021) An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals. Bilimsel Madencilik Dergisi 60 3 169–174.
IEEE M. T. Serdengeçti, B. Başkurt, K. Özçelik, and H. Baştürkcü, “An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals”, Mining, vol. 60, no. 3, pp. 169–174, 2021, doi: 10.30797/madencilik.800948.
ISNAD Serdengeçti, Mete Tayhan et al. “An Investigation on Characterization and Floation Behavior of a Transitional Ore Containing Galena and Pb Oxide Minerals”. Bilimsel Madencilik Dergisi 60/3 (September 2021), 169-174. https://doi.org/10.30797/madencilik.800948.
JAMA Serdengeçti MT, Başkurt B, Özçelik K, Baştürkcü H. An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals. Mining. 2021;60:169–174.
MLA Serdengeçti, Mete Tayhan et al. “An Investigation on Characterization and Floation Behavior of a Transitional Ore Containing Galena and Pb Oxide Minerals”. Bilimsel Madencilik Dergisi, vol. 60, no. 3, 2021, pp. 169-74, doi:10.30797/madencilik.800948.
Vancouver Serdengeçti MT, Başkurt B, Özçelik K, Baştürkcü H. An investigation on characterization and floation behavior of a transitional ore containing Galena and Pb Oxide minerals. Mining. 2021;60(3):169-74.

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