Research Article
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JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ

Year 2022, Volume: 30 Issue: 1, 16 - 30, 15.04.2022

Soner Top , Mahmut Altıner , Burçin Kaymakoğlu

https://doi.org/10.31796/ogummf.935300

Abstract

Bu çalışmada, desülfürizasyon ünitesinden elde edilen jips (DJ) taneciklerinin çöktürülmüş kalsiyum karbonat (ÇKK) taneciklerine direk mineral karbonatlaştırma yöntemi ile dönüştürülmesi sırasında ultrasonik güç uygulama, sıcaklık, karbondioksit (CO2) besleme hızı deneysel parametrelerinin etkileri Taguchi yaklaşımı kullanılarak araştırılmıştır. Deneylerde venturimetre ünitesi karbonatlaştırma zonu olarak kullanılmıştır. Elde edilen ürünlerin karakterizasyonu XRD, SEM ve tane boyutu analiz yöntemleri ile belirlenmiştir. Ayrıca ürünlerin özellikleri ASTM standartları dikkate alınarak değerlendirilmiştir. Sonuç olarak; üretim şartlarına bağlı olarak iğnemsi, kübik veya delikli yapıda kalsit kristallerinden oluşan ÇKK tanecikleri elde edilmiştir. ASTM standartlarına göre endüstriyel bir artıktan üretilen bu ürün, boya ve plastik sektörlerinde değerlendirilebilmesi için gereken özellikleri sağlamaktadır.

Keywords

Jips Çöktürülmüş kalsiyum karbonat Venturimetre Ultrasonik güç Mineral Karbonatlaştırma

Supporting Institution

TÜBİTAK

Project Number

119M134

Thanks

Bu çalışma, Türkiye Bilimsel ve Teknolojik Araştırma Kurumu (TÜBİTAK) tarafından desteklenmiştir (Proje numarası: 119M134).

References

  • Altiner, M., Top, S., & Kaymakoğlu, B. (2021). Ultrasonic-assisted production of precipitated calcium carbonate particles from desulfurization gypsum. Ultrasonics sonochemistry, 72, 105421. doi: https://doi.org/10.1016/j.ultsonch.2020.105421
  • Altiner, M., Top, S., Kaymakoğlu, B., Seçkin, İ. Y., & Vapur, H. (2019). Production of precipitated calcium carbonate particles from gypsum waste using venturi tubes as a carbonation zone. Journal of CO2 utilization, 29, 117-125. doi: https://doi.org/10.1016/j.jcou.2018.12.004
  • ASTM D1199-86, 2020. “Standard Specification for Calcium Carbonate Pigments”, American Society for Testing and Materials, West Conshohocken, PA.
  • ASTM D1366 – 86, 2020. “Standard Practice for Reporting Particle Size Characteristics of Pigments”, American Society for Testing and Materials, West Conshohocken, PA.
  • ASTM STP 1135, 1992. "Lime Used for Precipitated Calcium Carbonate (PCC) for the Paper Industry," Innovations and Uses for Lime, D. D. Walker, Jr., T. B. Hardy, D. C. Hoffman, and D. D. Stanley, Eds., American Society for Testing and Materials,Philadelphia, PA, 1-7.
  • Başaran, M. (2007). Karbondioksit (CO2) tutma ve depolama, TMMOB Türkiye Vi. Enerji Sempozyumu - Küresel Enerji Politikalari Ve Türkiye Gerçeği, 442-456.
  • Blue, C.R., Giuffre, A., Mergelsberg, S., Han, N., De Yoreo, J.J., Dove, P.M. (2017). Chemical and physical controls on the transformation of amorphous calcium carbonate into crystalline CaCO3 polymorphs. Geochimica et Cosmochimica Acta, 196, 179-196. doi: https://doi.org/10.1016/j.gca.2016.09.004
  • Boyjoo, Y., Pareek, V.K., Liu, J. (2014). Synthesis of micro and nano-sized calcium carbonate particles and their applications, J. Mater. Chemi. A, 35 (2), 14270-14288. doi: https://doi.org/10.1039/C4TA02070G
  • Casanova, H., Higuit, L.P. (2011). Synthesis of calcium carbonate nanoparticles by reactive precipitation using a high pressure jet homogenizer, Chemical Engineering Journal, 175, 569-578, 2011. Doi: https://doi.org/10.1016/j.cej.2011.09.051
  • Ercan, M., Koltka, S., Sabah, E. (2018). Mermer Artıklarından Öğütülmüş Kalsiyum Karbonat (GCC) Üretimi: Yaş Ve Kuru Öğütme Ürünlerinin Karşılaştırılması, Madencilik, 2018, 57 (1), 35-43.
  • Huijgen W.J., Witkamp G.-J., Comans R.N. (2006). Mechanisms of aqueous wollastonite carbonation as a possible CO2 sequestration process, Chemical Engineering Science, 61 (13), 4242-4251. doi: https://doi.org/10.1016/j.ces.2006.01.048
  • Jimoh, O.A., Ariffin, K.S., Hussin, H.B., Temitope, A.E. (2018). Synthesis of precipitated calcium carbonate: a review, Carbonates and Evaporites, 33 (2), 331-346. doi: https://doi.org/10.1007/s13146-017-0341-x
  • Karakaş, F., Celik, M. (2012). Effect of quantity and size distribution of calcite filler on the quality of water borne paints, Progress in Organic Coatings, 74 (3), 555-563. doi: https://doi.org/10.1016/j.porgcoat.2012.02.002
  • Konopacka-Łyskawa, D., Cisiak, Z., Kawalec-Pietrenko, B. (2009). Effect of liquid circulation in the draft-tube reactor on precipitation of calcium carbonate via carbonation, Powder Technology, 190 (3), 319-323. doi: https://doi.org/10.1016/j.powtec.2008.08.014
  • Lackner, K.S. (2002). Carbonate chemistry for sequestering fossil carbon, Annual review of energy and the environment, 27 (1), 193-232. doi: https://doi.org/10.1146/annurev.energy.27.122001.083433
  • Lee, M.G., Ryu, K.W., Chae, S.C., Jang, Y.N. (2015). Effects of temperature on the carbonation of flue gas desulphurization gypsum using a CO2/N2 gas mixture, Environmental Technology, 36 (1), 106-114. doi: https://doi.org/10.1080/09593330.2014.938126
  • Leip, A., Achermann, B., Billen, G., Bleeker, A., Bouwman, A., De Vries, W., Winiwarter, W. (2011). Integrating nitrogen fluxes at the European scale, In M. Sutton, C. Howard, J. Erisman, G. Billen, A. Bleeker, P. Grennfelt, et al. (Eds.), The European Nitrogen Assessment: Sources, Effects and Policy Perspectives (pp. 345-376). Cambridge: Cambridge University Press.
  • Matsumoto, M., Fukunaga, T., Onoe, K. (2010). Polymorph control of calcium carbonate by reactive crystallization using microbubble technique, Chem. Eng. Res. Des., 88 (12), 1624-1630. doi: https://doi.org/10.1016/j.cherd.2010.02.007
  • Mattila, H.-P., Zevenhoven, R. (2015). Mineral carbonation of phosphogypsum waste for production of useful carbonate and sulfate salts, Frontiers in Energy Research, 3, 48, 1-8. doi: https://doi.org/10.3389/fenrg.2015.00048
  • Mori, Y., Isogai, A., Enomae, T. (2010). Application of vaterite-type calcium carbonate prepared by ultrasound for ink jet paper, Journal of Imaging Science and Technology, 54 (2), 20504-1-20504-6(6). Doi: https://doi.org/10.2352/J.ImagingSci.Technol.2010.54.2.020504
  • Peng, F.F., Yu, X. (2015). Pico–nano bubble column flotation using static mixer-venturi tube for Pittsburgh No. 8 coal seam, International Journal of Mining Science and Technology, 25 (3), 347-354. doi: https://doi.org/10.1016/j.ijmst.2015.03.004
  • Radha, A., Forbes, T.Z., Killian, C.E., Gilbert, P., Navrotsky, A. (2010). Transformation and crystallization energetics of synthetic and biogenic amorphous calcium carbonate, Proceedings of the National Academy of Sciences, 107 (38), 16438-16443.
  • Roskill, 2012. The economics of precipitated calcium carbonate. Seventh Edition. Roskill Information Services Ltd.
  • Roth, R., Schoelkopf, J., Huwyler, J., Puchkov, M. (2018). Functionalized calcium carbonate microparticles for the delivery of proteins, European Journal of Pharmaceutics and Biopharmaceutics, 122, 96-103. doi: https://doi.org/10.1016/j.ejpb.2017.10.012
  • Song, K., Kim, W., Park, S., Bang, J.-H., Jeon, C.W., Ahn, J.-W. (2016). Effect of polyacrylic acid on direct aqueous mineral carbonation of flue gas desulfurization gypsum, Chemical Engineering Journal, 301, 51-57. doi: https://doi.org/10.1016/j.cej.2016.04.142
  • Toroman, Ö.Y., İnal, H. (2014). Ultrasonik enerji ile nano boyutta fonksiyonel mineral dolgu üretilmesi ve ürün özelliklerinin geliştirilmesi, TÜBİTAK projesi, Proje No: 112M037, ss. 27.
  • Ulkeryildiz, E., Kilic, S., Ozdemir, E. (2017). Nano-CaCO3 synthesis by jet flow, Colloids and Surfaces A: Physicochemical and Engineering Aspects, 512, 34-40. doi: https://doi.org/10.1016/j.colsurfa.2016.10.037
  • Wang, B., Pan, Z., Cheng, H., Chen, Z., Cheng, F. (2018). High-yield synthesis of vaterite microparticles in gypsum suspension system via ultrasonic probe vibration/magnetic stirring, Journal of Crystal Growth, 492, 122-131. doi: https://doi.org/10.1016/j.jcrysgro.2018.02.021
  • Wang, L., Sondi, I., Matijevic, E. (1999). Preparation of uniform needle-like aragonite particles by homogeneous precipitation, J. Colloid Interf. Sci., 218 (2), 545-553. doi: https://doi.org/10.1006/jcis.1999.6463
  • Wu, J.-L., Wang, C.-Q., Zhuo, R.-X., Cheng, S.-X. (2014). Multi-drug delivery system based on alginate/calcium carbonate hybrid nanoparticles for combination chemotherapy, Colloids and Surfaces B: Biointerfaces, 123, 498-505. Doi: https://doi.org/10.1016/j.colsurfb.2014.09.047
  • Wu, W.S., Queiroz, M.E., Mohallem, N.D.S. (2016). The effect of precipitated calcium carbonate nanoparticles in coatings, Journal of Coatings Technology and Research, 13 (2), 277-286. doi: https://doi.org/10.1007/s11998-015-9740-x
  • Zhang, H., Chen, J.F., Zhou, H.K., Wang, G.Q., Yun, J. (2002). Preparation of nano-sized precipitated calcium carbonate for PVC plastisol rheology modification, Journal of materials science letters, 21 (16), 1305-1306, doi: https://doi.org/10.1023/A:1016579724682

Year 2022, Volume: 30 Issue: 1, 16 - 30, 15.04.2022

Soner Top , Mahmut Altıner , Burçin Kaymakoğlu

https://doi.org/10.31796/ogummf.935300

Abstract

Project Number

119M134

References

  • Altiner, M., Top, S., & Kaymakoğlu, B. (2021). Ultrasonic-assisted production of precipitated calcium carbonate particles from desulfurization gypsum. Ultrasonics sonochemistry, 72, 105421. doi: https://doi.org/10.1016/j.ultsonch.2020.105421
  • Altiner, M., Top, S., Kaymakoğlu, B., Seçkin, İ. Y., & Vapur, H. (2019). Production of precipitated calcium carbonate particles from gypsum waste using venturi tubes as a carbonation zone. Journal of CO2 utilization, 29, 117-125. doi: https://doi.org/10.1016/j.jcou.2018.12.004
  • ASTM D1199-86, 2020. “Standard Specification for Calcium Carbonate Pigments”, American Society for Testing and Materials, West Conshohocken, PA.
  • ASTM D1366 – 86, 2020. “Standard Practice for Reporting Particle Size Characteristics of Pigments”, American Society for Testing and Materials, West Conshohocken, PA.
  • ASTM STP 1135, 1992. "Lime Used for Precipitated Calcium Carbonate (PCC) for the Paper Industry," Innovations and Uses for Lime, D. D. Walker, Jr., T. B. Hardy, D. C. Hoffman, and D. D. Stanley, Eds., American Society for Testing and Materials,Philadelphia, PA, 1-7.
  • Başaran, M. (2007). Karbondioksit (CO2) tutma ve depolama, TMMOB Türkiye Vi. Enerji Sempozyumu - Küresel Enerji Politikalari Ve Türkiye Gerçeği, 442-456.
  • Blue, C.R., Giuffre, A., Mergelsberg, S., Han, N., De Yoreo, J.J., Dove, P.M. (2017). Chemical and physical controls on the transformation of amorphous calcium carbonate into crystalline CaCO3 polymorphs. Geochimica et Cosmochimica Acta, 196, 179-196. doi: https://doi.org/10.1016/j.gca.2016.09.004
  • Boyjoo, Y., Pareek, V.K., Liu, J. (2014). Synthesis of micro and nano-sized calcium carbonate particles and their applications, J. Mater. Chemi. A, 35 (2), 14270-14288. doi: https://doi.org/10.1039/C4TA02070G
  • Casanova, H., Higuit, L.P. (2011). Synthesis of calcium carbonate nanoparticles by reactive precipitation using a high pressure jet homogenizer, Chemical Engineering Journal, 175, 569-578, 2011. Doi: https://doi.org/10.1016/j.cej.2011.09.051
  • Ercan, M., Koltka, S., Sabah, E. (2018). Mermer Artıklarından Öğütülmüş Kalsiyum Karbonat (GCC) Üretimi: Yaş Ve Kuru Öğütme Ürünlerinin Karşılaştırılması, Madencilik, 2018, 57 (1), 35-43.
  • Huijgen W.J., Witkamp G.-J., Comans R.N. (2006). Mechanisms of aqueous wollastonite carbonation as a possible CO2 sequestration process, Chemical Engineering Science, 61 (13), 4242-4251. doi: https://doi.org/10.1016/j.ces.2006.01.048
  • Jimoh, O.A., Ariffin, K.S., Hussin, H.B., Temitope, A.E. (2018). Synthesis of precipitated calcium carbonate: a review, Carbonates and Evaporites, 33 (2), 331-346. doi: https://doi.org/10.1007/s13146-017-0341-x
  • Karakaş, F., Celik, M. (2012). Effect of quantity and size distribution of calcite filler on the quality of water borne paints, Progress in Organic Coatings, 74 (3), 555-563. doi: https://doi.org/10.1016/j.porgcoat.2012.02.002
  • Konopacka-Łyskawa, D., Cisiak, Z., Kawalec-Pietrenko, B. (2009). Effect of liquid circulation in the draft-tube reactor on precipitation of calcium carbonate via carbonation, Powder Technology, 190 (3), 319-323. doi: https://doi.org/10.1016/j.powtec.2008.08.014
  • Lackner, K.S. (2002). Carbonate chemistry for sequestering fossil carbon, Annual review of energy and the environment, 27 (1), 193-232. doi: https://doi.org/10.1146/annurev.energy.27.122001.083433
  • Lee, M.G., Ryu, K.W., Chae, S.C., Jang, Y.N. (2015). Effects of temperature on the carbonation of flue gas desulphurization gypsum using a CO2/N2 gas mixture, Environmental Technology, 36 (1), 106-114. doi: https://doi.org/10.1080/09593330.2014.938126
  • Leip, A., Achermann, B., Billen, G., Bleeker, A., Bouwman, A., De Vries, W., Winiwarter, W. (2011). Integrating nitrogen fluxes at the European scale, In M. Sutton, C. Howard, J. Erisman, G. Billen, A. Bleeker, P. Grennfelt, et al. (Eds.), The European Nitrogen Assessment: Sources, Effects and Policy Perspectives (pp. 345-376). Cambridge: Cambridge University Press.
  • Matsumoto, M., Fukunaga, T., Onoe, K. (2010). Polymorph control of calcium carbonate by reactive crystallization using microbubble technique, Chem. Eng. Res. Des., 88 (12), 1624-1630. doi: https://doi.org/10.1016/j.cherd.2010.02.007
  • Mattila, H.-P., Zevenhoven, R. (2015). Mineral carbonation of phosphogypsum waste for production of useful carbonate and sulfate salts, Frontiers in Energy Research, 3, 48, 1-8. doi: https://doi.org/10.3389/fenrg.2015.00048
  • Mori, Y., Isogai, A., Enomae, T. (2010). Application of vaterite-type calcium carbonate prepared by ultrasound for ink jet paper, Journal of Imaging Science and Technology, 54 (2), 20504-1-20504-6(6). Doi: https://doi.org/10.2352/J.ImagingSci.Technol.2010.54.2.020504
  • Peng, F.F., Yu, X. (2015). Pico–nano bubble column flotation using static mixer-venturi tube for Pittsburgh No. 8 coal seam, International Journal of Mining Science and Technology, 25 (3), 347-354. doi: https://doi.org/10.1016/j.ijmst.2015.03.004
  • Radha, A., Forbes, T.Z., Killian, C.E., Gilbert, P., Navrotsky, A. (2010). Transformation and crystallization energetics of synthetic and biogenic amorphous calcium carbonate, Proceedings of the National Academy of Sciences, 107 (38), 16438-16443.
  • Roskill, 2012. The economics of precipitated calcium carbonate. Seventh Edition. Roskill Information Services Ltd.
  • Roth, R., Schoelkopf, J., Huwyler, J., Puchkov, M. (2018). Functionalized calcium carbonate microparticles for the delivery of proteins, European Journal of Pharmaceutics and Biopharmaceutics, 122, 96-103. doi: https://doi.org/10.1016/j.ejpb.2017.10.012
  • Song, K., Kim, W., Park, S., Bang, J.-H., Jeon, C.W., Ahn, J.-W. (2016). Effect of polyacrylic acid on direct aqueous mineral carbonation of flue gas desulfurization gypsum, Chemical Engineering Journal, 301, 51-57. doi: https://doi.org/10.1016/j.cej.2016.04.142
  • Toroman, Ö.Y., İnal, H. (2014). Ultrasonik enerji ile nano boyutta fonksiyonel mineral dolgu üretilmesi ve ürün özelliklerinin geliştirilmesi, TÜBİTAK projesi, Proje No: 112M037, ss. 27.
  • Ulkeryildiz, E., Kilic, S., Ozdemir, E. (2017). Nano-CaCO3 synthesis by jet flow, Colloids and Surfaces A: Physicochemical and Engineering Aspects, 512, 34-40. doi: https://doi.org/10.1016/j.colsurfa.2016.10.037
  • Wang, B., Pan, Z., Cheng, H., Chen, Z., Cheng, F. (2018). High-yield synthesis of vaterite microparticles in gypsum suspension system via ultrasonic probe vibration/magnetic stirring, Journal of Crystal Growth, 492, 122-131. doi: https://doi.org/10.1016/j.jcrysgro.2018.02.021
  • Wang, L., Sondi, I., Matijevic, E. (1999). Preparation of uniform needle-like aragonite particles by homogeneous precipitation, J. Colloid Interf. Sci., 218 (2), 545-553. doi: https://doi.org/10.1006/jcis.1999.6463
  • Wu, J.-L., Wang, C.-Q., Zhuo, R.-X., Cheng, S.-X. (2014). Multi-drug delivery system based on alginate/calcium carbonate hybrid nanoparticles for combination chemotherapy, Colloids and Surfaces B: Biointerfaces, 123, 498-505. Doi: https://doi.org/10.1016/j.colsurfb.2014.09.047
  • Wu, W.S., Queiroz, M.E., Mohallem, N.D.S. (2016). The effect of precipitated calcium carbonate nanoparticles in coatings, Journal of Coatings Technology and Research, 13 (2), 277-286. doi: https://doi.org/10.1007/s11998-015-9740-x
  • Zhang, H., Chen, J.F., Zhou, H.K., Wang, G.Q., Yun, J. (2002). Preparation of nano-sized precipitated calcium carbonate for PVC plastisol rheology modification, Journal of materials science letters, 21 (16), 1305-1306, doi: https://doi.org/10.1023/A:1016579724682
There are 32 citations in total.

Details

Primary Language Turkish
Subjects Geological Sciences and Engineering (Other)
Journal Section Research Articles
Authors

Soner Top 0000-0003-3486-4184

Mahmut Altıner 0000-0002-7428-5999

Burçin Kaymakoğlu 0000-0002-4885-6399

Project Number 119M134
Publication Date April 15, 2022
Acceptance Date November 12, 2021
Published in Issue Year 2022 Volume: 30 Issue: 1

Cite

APA Top, S., Altıner, M., & Kaymakoğlu, B. (2022). JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ. Eskişehir Osmangazi Üniversitesi Mühendislik Ve Mimarlık Fakültesi Dergisi, 30(1), 16-30. https://doi.org/10.31796/ogummf.935300
AMA Top S, Altıner M, Kaymakoğlu B. JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ. ESOGÜ Müh Mim Fak Derg. April 2022;30(1):16-30. doi:10.31796/ogummf.935300
Chicago Top, Soner, Mahmut Altıner, and Burçin Kaymakoğlu. “JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ”. Eskişehir Osmangazi Üniversitesi Mühendislik Ve Mimarlık Fakültesi Dergisi 30, no. 1 (April 2022): 16-30. https://doi.org/10.31796/ogummf.935300.
EndNote Top S, Altıner M, Kaymakoğlu B (April 1, 2022) JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ. Eskişehir Osmangazi Üniversitesi Mühendislik ve Mimarlık Fakültesi Dergisi 30 1 16–30.
IEEE S. Top, M. Altıner, and B. Kaymakoğlu, “JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ”, ESOGÜ Müh Mim Fak Derg, vol. 30, no. 1, pp. 16–30, 2022, doi: 10.31796/ogummf.935300.
ISNAD Top, Soner et al. “JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ”. Eskişehir Osmangazi Üniversitesi Mühendislik ve Mimarlık Fakültesi Dergisi 30/1 (April 2022), 16-30. https://doi.org/10.31796/ogummf.935300.
JAMA Top S, Altıner M, Kaymakoğlu B. JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ. ESOGÜ Müh Mim Fak Derg. 2022;30:16–30.
MLA Top, Soner et al. “JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ”. Eskişehir Osmangazi Üniversitesi Mühendislik Ve Mimarlık Fakültesi Dergisi, vol. 30, no. 1, 2022, pp. 16-30, doi:10.31796/ogummf.935300.
Vancouver Top S, Altıner M, Kaymakoğlu B. JİPS ARTIĞINDAN TAGUCHİ YAKLAŞIMI KULLANILARAK ÇÖKTÜRÜLMÜŞ KALSİYUM KARBONAT (ÇKK) ÜRETİMİ. ESOGÜ Müh Mim Fak Derg. 2022;30(1):16-30.
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