Year 2020, Volume 15 , Issue 1, Pages 167 - 176 2020-05-31

Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi
Synthesis of Functionalized Titanium Dioxide Nanotube

Banu TÜRKASLAN [1] , Melek AKTAŞ [2] , Sultan AKAR [3]


TiO2 nanotüp sentezi ile ilgili yapılan çalışmalarda belirtilen koşullarda nanotüplerin oluştuğu yönünde sonuçlar verilirken, karakterizasyon sonuçlarının nano malzemenin toz formuna ait olduğu, tübüler yapılara ait formların oluşmadığı görülmektedir. Bu çalışmada titanyum dioksit (TiO2) tozundan hidrotermal sentez yöntemi ile TiO2 nanotüpleri elde edildi. Nanotüp sentezi için deney şartları optimize edildikten sonra elde edilen TiO2 nanotüplerin metakrilik asit ile fonksiyonlaştırma işlemi gerçekleştirildi. TiO2 tozunun yapısı, hidrotermal koşullar (sıcaklık, reaktiflerin konsantrasyonu ve hidrotermal süresi) ve sonraki yıkama işlemleri, TiO2 nanotüp yapısını (kristalografi ve morfoloji) ve fiziksel-kimyasal özelliklerini belirlemede önemli bir rol aldığı gözlendi. Sentezlenen nanotüp yapıları, Enerji Dağılım Spektrometresi (EDS), Fourier Dönüşümlü Kızılötesi Spektroskopisi (FTIR), X-Işını Kırınım Difraktometresi (XRD) ve Taramalı Elektron Mikroskobu (SEM) ile karakterize edildi.

Several studies releated on TiO2 nanotubes synthesis show that nanotubes do not occur under the specified conditions, while the characterization results belong to the powder form of the nanomaterials. In this study, titanium dioxide (TiO2) nanotubes were synthesized via hydrothermal process fromcommercial TiO2 powder. After optimizing the experimental conditions for nanotube synthesis, the obtained TiO2 nanotubes were functionalized with methacrylic acid. The structure of TiO2 powder, hydrothermal conditions (temperature, concentration of reagents and hydrothermal time) and subsequent washing processes were observed to play an important role in determining the TiO2 nanotube structure (crystallography and morphology) and physical-chemical properties. The morphology of the nanotubes were characterized by Energy Dispersion Spectrometry (EDS), Fourier Transform Infrared Spectroscopy (FTIR), X-Ray Diffraction (XRD) and Scanning Electron Microscopy (SEM).

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Primary Language tr
Subjects Engineering, Chemical
Journal Section Makaleler
Authors

Orcid: 0000-0003-3948-6207
Author: Banu TÜRKASLAN (Primary Author)
Institution: Süleyman Demirel Üniversitesi
Country: Turkey


Orcid: 0000-0001-5172-5261
Author: Melek AKTAŞ
Institution: Kimya Mühendisi
Country: Turkey


Orcid: 0000-0003-2449-0975
Author: Sultan AKAR
Institution: Kimya Mühendisi
Country: Turkey


Dates

Publication Date : May 31, 2020

Bibtex @research article { sdufeffd666020, journal = {Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi}, issn = {}, eissn = {1306-7575}, address = {}, publisher = {Süleyman Demirel University}, year = {2020}, volume = {15}, pages = {167 - 176}, doi = {10.29233/sdufeffd.666020}, title = {Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi}, key = {cite}, author = {Türkaslan, Banu and Aktaş, Melek and Akar, Sultan} }
APA Türkaslan, B , Aktaş, M , Akar, S . (2020). Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi . Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi , 15 (1) , 167-176 . DOI: 10.29233/sdufeffd.666020
MLA Türkaslan, B , Aktaş, M , Akar, S . "Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi" . Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi 15 (2020 ): 167-176 <https://dergipark.org.tr/en/pub/sdufeffd/issue/54573/666020>
Chicago Türkaslan, B , Aktaş, M , Akar, S . "Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi". Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi 15 (2020 ): 167-176
RIS TY - JOUR T1 - Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi AU - Banu Türkaslan , Melek Aktaş , Sultan Akar Y1 - 2020 PY - 2020 N1 - doi: 10.29233/sdufeffd.666020 DO - 10.29233/sdufeffd.666020 T2 - Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi JF - Journal JO - JOR SP - 167 EP - 176 VL - 15 IS - 1 SN - -1306-7575 M3 - doi: 10.29233/sdufeffd.666020 UR - https://doi.org/10.29233/sdufeffd.666020 Y2 - 2020 ER -
EndNote %0 Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi %A Banu Türkaslan , Melek Aktaş , Sultan Akar %T Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi %D 2020 %J Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi %P -1306-7575 %V 15 %N 1 %R doi: 10.29233/sdufeffd.666020 %U 10.29233/sdufeffd.666020
ISNAD Türkaslan, Banu , Aktaş, Melek , Akar, Sultan . "Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi". Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi 15 / 1 (May 2020): 167-176 . https://doi.org/10.29233/sdufeffd.666020
AMA Türkaslan B , Aktaş M , Akar S . Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi. SDÜFEFFD. 2020; 15(1): 167-176.
Vancouver Türkaslan B , Aktaş M , Akar S . Fonksiyonelleştirilmiş Titanyum Dioksit Nanotüp Sentezi. Süleyman Demirel Üniversitesi Fen Edebiyat Fakültesi Fen Dergisi. 2020; 15(1): 167-176.