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Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base

Year 2017, Volume: 21 Issue: 3, 812 - 815, 13.10.2017
https://doi.org/10.19113/sdufbed.34496

Abstract

Our study contains a novel sulfonyl hydrazide. For this, N'-((1H-pyrrol-2-yl)methylene)-N-methylbenzenesulfonohydrazide were  synthesized. The structures of this new compound was characterized by elementary analysis, 1H NMR, 13C NMR, FT-IR, DTA/TG. Also this study is contain performed on optimized geometry at the B3LYP/6.311+G**level for this organic compounds.

References

  • [1] Sneader, W. 1985. Drug Discovery: the evolution of modern medicines. Wiley-New York, 153-160, 217-219, 278-291.
  • [2] Hansch, C., Sammes, P.G., Taylor, J.B. 1990. In Comprehensive Medicinal Chemistry. Pergamon Press, Oxford, 2(7): 255.
  • [3] Dural, E. 2002. Farmakoloji. Nobel Tıp Kitap, İstanbul, 454-457.
  • [4] Noss, M.B., Christ, G.J., Melman, A. 1999. Sildenafil: a new oral therapy for erectile Dysfunction. Drugs Today, 35(1999), 211-217.
  • [5] Brock, G. 2000. Sildenafil citrate. Drugs Today., 36(2000) 125-134.
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  • [7] Conway, B., Shafran, S.D. 2000. Pharmacology and clinical experience with amprenavir. Opin.Invest. Drug, 9(2000), 371-382.
  • [8] Dhar, D.N., Sharma, R.L., Bansal, G.C. 1982. Gastrointestinal nematodes in sheep in Kashmir. Veterinary Parasitology, 11(1982), 271–277.
  • [9] Kesimli, B., Topacli, A. 2001. Infrared studies on Co and Cd complexes of Sulfamethoxazole. Spectrochim. Acta.57(2001), 1031-1036.
  • [10] Cami, G.E., Chufan, E.E., Pedregosa, J.C., Varetti, E.L. 2001. Infrared and Raman spectra of 5-amino-1,3,4-thiadiazole-2- Experimental data and quantum chemistry calculations. J. Mol. Struc. 570(2001), 119-127.
  • [11] Sas, E.B., Kose, E., Kurt, M.,Karabacak M. 2015. FT-IR, FT-Raman, NMR and UV-VIS spectra and DFT calculations of 5-bromo-2-ethoxyphenylboronic acid (monomer and dimer structures). Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 137(2015), 1315-1333.
  • [12] Kurt, M.,Karabacak M., Okur, S., Sayın, S., Yılmaz, M. 2012. Sundaraganesan, N. Synthesis, FT-IR, FT-Raman, dispersive Raman and and NMR spectroscopic study of, host molecule which potential applications in sensor devices. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 137 (2012), 126-133.
  • [13] Karabacak M., Kose, E., Sas, E.B., Kurt, M., Asiri, A.M., Atac, A. 2015. DFT calculations and experimental FT-IR, FT-Raman, NMR and UV-VIS spectral studies of 3-fluorophenylboronic acid. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 136(2015), 306-320.
  • [14] Cai L. F., Huang X. B., Rong M. Z., Ruan W. H., Zhang M. Q. 2006. Effect of grafted polymeric foaming agent on the structure and properties of nano-silica/ polypropylene composites. Polymer. 47(2006), 7043–7050.
  • [15] Cai L. F., Mai Y. L., Rong M. Z., Ruan W. H., Zhang M. Q. 2007. Interfacial effects in nano-silica/polypropylene composites fabricated by in-situ chemical blowing. Polymer Letters. 1(2007),2-7.
  • [16] Michalková A., Tunega D. 2007. Kaolinite:Dimethylsulfoxide Intercalate A Theoretical Study. J. Phys. Chem. 2007, 111 (2007), 11259–11266.
  • [17] Tıan A.Q., Chen J.L.,Feng X., Wang W.Z., Wang L.Y. 2014. Thermal Behavior Of Several Stable Hydroxyl Free Radicals And Of Their Parent Hydrazines. Chinese J. Struct. Chem. Vol. 33(2014), 1443─1450.
Year 2017, Volume: 21 Issue: 3, 812 - 815, 13.10.2017
https://doi.org/10.19113/sdufbed.34496

Abstract

References

  • [1] Sneader, W. 1985. Drug Discovery: the evolution of modern medicines. Wiley-New York, 153-160, 217-219, 278-291.
  • [2] Hansch, C., Sammes, P.G., Taylor, J.B. 1990. In Comprehensive Medicinal Chemistry. Pergamon Press, Oxford, 2(7): 255.
  • [3] Dural, E. 2002. Farmakoloji. Nobel Tıp Kitap, İstanbul, 454-457.
  • [4] Noss, M.B., Christ, G.J., Melman, A. 1999. Sildenafil: a new oral therapy for erectile Dysfunction. Drugs Today, 35(1999), 211-217.
  • [5] Brock, G. 2000. Sildenafil citrate. Drugs Today., 36(2000) 125-134.
  • [6] Adkins, J., Faulds, D., “Amprenavir’’, Drugs Today., 55(1998), 837-842.
  • [7] Conway, B., Shafran, S.D. 2000. Pharmacology and clinical experience with amprenavir. Opin.Invest. Drug, 9(2000), 371-382.
  • [8] Dhar, D.N., Sharma, R.L., Bansal, G.C. 1982. Gastrointestinal nematodes in sheep in Kashmir. Veterinary Parasitology, 11(1982), 271–277.
  • [9] Kesimli, B., Topacli, A. 2001. Infrared studies on Co and Cd complexes of Sulfamethoxazole. Spectrochim. Acta.57(2001), 1031-1036.
  • [10] Cami, G.E., Chufan, E.E., Pedregosa, J.C., Varetti, E.L. 2001. Infrared and Raman spectra of 5-amino-1,3,4-thiadiazole-2- Experimental data and quantum chemistry calculations. J. Mol. Struc. 570(2001), 119-127.
  • [11] Sas, E.B., Kose, E., Kurt, M.,Karabacak M. 2015. FT-IR, FT-Raman, NMR and UV-VIS spectra and DFT calculations of 5-bromo-2-ethoxyphenylboronic acid (monomer and dimer structures). Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 137(2015), 1315-1333.
  • [12] Kurt, M.,Karabacak M., Okur, S., Sayın, S., Yılmaz, M. 2012. Sundaraganesan, N. Synthesis, FT-IR, FT-Raman, dispersive Raman and and NMR spectroscopic study of, host molecule which potential applications in sensor devices. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 137 (2012), 126-133.
  • [13] Karabacak M., Kose, E., Sas, E.B., Kurt, M., Asiri, A.M., Atac, A. 2015. DFT calculations and experimental FT-IR, FT-Raman, NMR and UV-VIS spectral studies of 3-fluorophenylboronic acid. Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy. 136(2015), 306-320.
  • [14] Cai L. F., Huang X. B., Rong M. Z., Ruan W. H., Zhang M. Q. 2006. Effect of grafted polymeric foaming agent on the structure and properties of nano-silica/ polypropylene composites. Polymer. 47(2006), 7043–7050.
  • [15] Cai L. F., Mai Y. L., Rong M. Z., Ruan W. H., Zhang M. Q. 2007. Interfacial effects in nano-silica/polypropylene composites fabricated by in-situ chemical blowing. Polymer Letters. 1(2007),2-7.
  • [16] Michalková A., Tunega D. 2007. Kaolinite:Dimethylsulfoxide Intercalate A Theoretical Study. J. Phys. Chem. 2007, 111 (2007), 11259–11266.
  • [17] Tıan A.Q., Chen J.L.,Feng X., Wang W.Z., Wang L.Y. 2014. Thermal Behavior Of Several Stable Hydroxyl Free Radicals And Of Their Parent Hydrazines. Chinese J. Struct. Chem. Vol. 33(2014), 1443─1450.
There are 17 citations in total.

Details

Journal Section Articles
Authors

Halime Güzin Aslan

Publication Date October 13, 2017
Published in Issue Year 2017 Volume: 21 Issue: 3

Cite

APA Aslan, H. G. (2017). Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, 21(3), 812-815. https://doi.org/10.19113/sdufbed.34496
AMA Aslan HG. Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base. SDÜ Fen Bil Enst Der. December 2017;21(3):812-815. doi:10.19113/sdufbed.34496
Chicago Aslan, Halime Güzin. “Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21, no. 3 (December 2017): 812-15. https://doi.org/10.19113/sdufbed.34496.
EndNote Aslan HG (December 1, 2017) Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21 3 812–815.
IEEE H. G. Aslan, “Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base”, SDÜ Fen Bil Enst Der, vol. 21, no. 3, pp. 812–815, 2017, doi: 10.19113/sdufbed.34496.
ISNAD Aslan, Halime Güzin. “Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi 21/3 (December 2017), 812-815. https://doi.org/10.19113/sdufbed.34496.
JAMA Aslan HG. Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base. SDÜ Fen Bil Enst Der. 2017;21:812–815.
MLA Aslan, Halime Güzin. “Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base”. Süleyman Demirel Üniversitesi Fen Bilimleri Enstitüsü Dergisi, vol. 21, no. 3, 2017, pp. 812-5, doi:10.19113/sdufbed.34496.
Vancouver Aslan HG. Synthesis, Structural Characterization and DTA/TG Studies of a Schiff Base. SDÜ Fen Bil Enst Der. 2017;21(3):812-5.

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