Year 2019, Volume 32, Issue 2, Pages 426 - 438 2019-06-01

Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry

Serap TITRETIR DURAN [1]

93 128

Bisphenol A (BPA) is important matter in chemical industry used in the produce of some food contact materials such as plastics, adhesives and coatings. But BPA has also some toxic effects for human endocrine system and environment. Therefore, novel sensitive and selective methods for determination the level of BPA in environmental, medical samples and foods new measurement methods need to be developed. A novel, sensitive, simple and cheap electrochemical sensor based on poly (p-aminobenzoic acid) p(p-ABA) modified gold electrode (AuE) was developed for the measurement of BPA in water samples. Firstly, AuEs were modified with polymerization of the p-amino benzoic acid as a monomer by using bulk electrolysis in 0.01 M HCl at -250 mV. Then the electrochemical oxidation of BPA carried out in 0.1 M phosphate buffer solution (PBS) pH=6 on p(p-ABA) modified AuE. The effects of various electrochemical parameters, such as scan rate, electroyte type and electrolyte pH were examined. Differential pulse voltammetry (DPV) was used as an ideal analytical method for the qualitative and quantitative detect of BPA in water samples. The developed electrochemical sensor has linear signal to BPA in the range of 2–100 μM. Prepared electrode was showed the limit of detection (LOD) of 0.26 µM and R2 of 0.999. Additionally, the developed sensor s used to determination the BPA in bottled drinking water sold in Turkish markets by using DPV, and obtains satisfactory results. The recovery values of the bottle water samples in the freezer, at room temperature and in the car were calculated as 102.22%, 104.68% and 106.06% respectively

Bisphenol A, Sensor, Bottled water, Bottled water, Poly (p-aminobenzoic acid)
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Primary Language en
Subjects Engineering
Journal Section Chemistry
Authors

Author: Serap TITRETIR DURAN (Primary Author)
Institution: İNÖNÜ ÜNİVERSİTESİ, FEN-EDEBİYAT FAKÜLTESİ, KİMYA BÖLÜMÜ
Country: Turkey


Dates

Publication Date: June 1, 2019

Bibtex @research article { gujs450639, journal = {GAZI UNIVERSITY JOURNAL OF SCIENCE}, issn = {}, eissn = {2147-1762}, address = {Gazi University}, year = {2019}, volume = {32}, pages = {426 - 438}, doi = {}, title = {Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry}, key = {cite}, author = {TITRETIR DURAN, Serap} }
APA TITRETIR DURAN, S . (2019). Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. GAZI UNIVERSITY JOURNAL OF SCIENCE, 32 (2), 426-438. Retrieved from http://dergipark.org.tr/gujs/issue/45480/450639
MLA TITRETIR DURAN, S . "Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry". GAZI UNIVERSITY JOURNAL OF SCIENCE 32 (2019): 426-438 <http://dergipark.org.tr/gujs/issue/45480/450639>
Chicago TITRETIR DURAN, S . "Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry". GAZI UNIVERSITY JOURNAL OF SCIENCE 32 (2019): 426-438
RIS TY - JOUR T1 - Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry AU - Serap TITRETIR DURAN Y1 - 2019 PY - 2019 N1 - DO - T2 - GAZI UNIVERSITY JOURNAL OF SCIENCE JF - Journal JO - JOR SP - 426 EP - 438 VL - 32 IS - 2 SN - -2147-1762 M3 - UR - Y2 - 2018 ER -
EndNote %0 GAZI UNIVERSITY JOURNAL OF SCIENCE Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry %A Serap TITRETIR DURAN %T Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry %D 2019 %J GAZI UNIVERSITY JOURNAL OF SCIENCE %P -2147-1762 %V 32 %N 2 %R %U
ISNAD TITRETIR DURAN, Serap . "Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry". GAZI UNIVERSITY JOURNAL OF SCIENCE 32 / 2 (June 2019): 426-438.
AMA TITRETIR DURAN S . Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. GAZI UNIVERSITY JOURNAL OF SCIENCE. 2019; 32(2): 426-438.
Vancouver TITRETIR DURAN S . Determination of Bisphenol a with Poly (p-Aminobenzoic Acid) Modified Gold Electrode by Using Differential Pulse Voltammetry. GAZI UNIVERSITY JOURNAL OF SCIENCE. 2019; 32(2): 438-426.