TY  - JOUR
T1  - SCREENING OF TETRACYCLINE AND FLORFENICOL ANTIBIOTIC RESIDUES IN BROILER MEAT USING ELISA AND CONFIRMATION BY LIQUID CHROMATOGRAPHY/TANDEM MASS SPECTROMETRY
TT  - BROİLER ETLERİNDEKİ TETRASİKLİN VE FLORFENİKOL ANTİBİYOTİK KALINTILARININ ELISA İLE GÖRÜNTÜLENMESİ VE SIVI KROMATOGRAFİSİ KÜTLE/ KÜTLE SPEKTROMETRESİ İLE DOĞRULANMASI
AU  - Tekgül, Yeliz
AU  - Kök, Filiz
PY  - 2018
DA  - May
DO  - 10.15237/gida.GD17082
JF  - Gıda
JO  - GIDA
PB  - Gıda Teknolojisi Derneği
WT  - DergiPark
SN  - 1300-3070
SP  - 403
EP  - 412
VL  - 43
IS  - 3
LA  - en
AB  - The aim of this study was toinvestigate the presence of tetracycline and florfenicol residues in broilermeat that sailed in Aydın city, Turkey. For this purpose, 80 broiler meats thatbrands of local and national commercial were used. ELISA technique was used toinvestigate the presence of antibiotic residues and liquid chromatography/tandem mass spectrometry (LC-MS/MS) technique was used to confirm the residue.As result of the ELISA, 24 samples 30%) were positive for tetracycline.Florfenicol residues were found in any of the samples. 24 samples that isconfirmed by LC-MS/MS were included an average of 30 ppb level. Residualamounts of the samples were found to be below the maximum residue limit (MRL)values.
KW  - Florfenicol
KW  - tetracycline
KW  - ELISA
KW  - LC-MS/MS
N2  - Bu çalışmada Aydın ilindetüketime sunulan broiler etlerindeki tetrasiklin ve florfenikol antibiyotikkalıntılarının araştırılması amaçlanmıştır. Bu amaçla farklı satış yerlerindenfarklı zamanlarda toplanan 80 adet broiler örneği kullanılmıştır. Antibiyotikkalıntı varlığı ELISA test kitleriyle belirlenmiş ve LC-MS/MS cihazı iledoğrulama yapılmıştır. ELISA test sonuçlarına göre incelenen örneklerin 24’ünün(%30) tetrasiklin pozitif olduğu ve örneklerin hiçbirinde florfenikolerastlanılmadığı gözlenmiştir. Tetrasiklin içeren ve LC-MS/MS’de doğrulamasıyapılan 24 örnekteki antibiyotik düzeyi ortalama 30 ppm olarak bulunmuştur.Bulunan değerin maksimum kalıntı düzeyinin (MRL) altıda olduğu görülmüştür.
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UR  - https://doi.org/10.15237/gida.GD17082
L1  - https://dergipark.org.tr/tr/download/article-file/453071
ER  -