SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI

Sema Vural; Aysel Bayrak Alphan; Süleyman Köytepe; Turgay Seçkin

doi:10.18038/btda.19450

TR

SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI

Abstract

Kobalt, nikel ve çinko ferrit nano parçacıkları hidrotermal sentez yöntemi kullanılarak sentezlenmiştir. Sentez koşullarının elde edilen spinel ferritlerin kristal yapısı, parçacık boyutu, örgü parametreleri, mikroyapı ve manyetik özellikler üzerine etkileri X-Işını Kırınım Analizi (XRD), taramalı elektron mikroskopu (SEM), Enerji-dağılımlı X-ışınları spektroskopisi (EDX) ve Mapping yöntemleriyle belirlenmiştir. Hazırlanan ferritlerin parçacık boyutu 25-70 nm arasında değişmektedir. Ayrıca, nano parçacıkların manyetik özellikleri titreşimli örnek magnetometresi (VSM) kullanılarak araştırılmıştır. Manyetik özelliklerin sıcaklık ve iyon çeşidine bağlı olarak değiştiği gözlenmiştir. Elde edilen manyetik özelliklere göre hazırlanan örnekler yüksek yoğunluklu manyetik kayıtlama cihazlarında, yüksek kullanım potansiyeline sahiptir.

Keywords

Kontrollü morfoloji, spinel ferrit, nano parçacik, manyetik nano malzeme

References

Sattler KD. Handbook of Nanophysics: Nanoparticles and Quantum Dots. 1th ed. United States: CRC Press: Florida; 2010.
Costa ACFM, Diniz AP, Silva VJ, Kiminami RHGA, Cornejo DR, Gama AM, Rezende MC, Gama L, Influence of calcination temperature on the morphology and magnetic properties of Ni–Zn ferrite applied as an electromagnetic energy absorber, J. Alloys Compd., 483, 563-565, 2009. doi:10.1016/j.jallcom.2008.08.108.
Lima UR, Nasar MC, Nasar RS, Rezende MC, Araşjo JH, Ni–Zn nanoferrite for radar-absorbing material, J. Magn. Magn. Mater., 320, 1666-1670, 2008. doi: 10.1016/j.jmmm.2008.01.022.
Sugimoto M, The past, present, and future of ferrites, J. Am. Ceram. Soc., 82, 269-280, 1999. doi:10.1111/j.1551-2916.1999.tb20058.x.
Sousa, MH, Hasmonay E, Depeyrot J, Tourinho FA, Bacri JC, Dubois E, Perzynski R, Raikherb YL, NiFe2O4 nanoparticles in ferrofluids: evidence of spin disorder in the surface layer, J. Magn. Magn. Mater., 572, 242-245, 2002. doi:10.1016/S0304-8853(01)01122-2.
Bhat PB, Bhat BR, Magnetically retrievable nickel hydroxide functionalised AFe2O4(A=Mn, Ni) spinel nanocatalyst for alcohol oxidation, Appl Nanosci, 6, 425–435, 2016. DOI 10.1007/s13204-015- 0456-0.
Sepelak V, Baabe D, Mienert D, Schultze D, Krumeich F, Litterst FJ, Becker KD, Evolution of structure and magnetic properties with annealing temperature in nanoscale high-energy-milled nickel ferrite, J. Magn. Magn. Mater., 257, 377-386, 2003. doi:10.1016/S0304-8853(02)01279-9.
Naiden EP, Zhuravlev VA, Itin VI, Terekhova OG, Magaeva AA, Ivanov YF, Structure and magnetic properties of mechanically alloyed ferrite nanopowders, Russian Physics Journal, 49(9), 946-951, 2006. doi:10.1007/s11182-006-0207-5.
Shobana MK, Kwonb H, Choe H, Structural studies on the yttrium-doped cobalt ferrite powders synthesized by sol–gel combustion method, Journal of Magnetism and Magnetic Materials., 324, 2245- 2248, 2012. doi:10.1016/j.jmmm.2012.02.110.
Peng CH, Hwang CC, Hong CK, Chen SY, A self-propagating high-temperature synthesis method for

doi:10.1016/j.mseb.2003.12.004. synthesis, Mater. Sci. Eng.
B., 107(3), 295-300,
[11] Sridhar R, Ravinder Da, Kumar KV, Synthesis and Characterization of Copper Substituted Nickel Nano-Ferrites by Citrate-Gel Technique, Advances in Materials Physics and Chemistry, 2, 192-199, 2012. doi: 10.4236/ampc.2012.23029.
Nathani H, Gubbala S, Misra RDK, Magnetic behavior of nickel ferrite–nanocomposites synthesized by mechanical milling process, Mater. Sci. Eng. B., 111, 95-100, 2004. doi:10.1016/j.mseb.2004.03.002.
Giannakopoulou T, Kompotiatis L, Kontogeorgakos A, Kordas G, Microwave behavior of ferrites prepared via sol–gel method, J. Magn.Magn. Mater., 246(3), 360-365, 2002. doi:10.1016/S0304- 8853(02)00106-3.
Konishi Y, Nomura T, Mizoe K, A new synthesis route from spent sulfuric acid pickling solution to ferrite nanoparticles, Hydrometallurgy, 74, 57-65, 2004. doi:10.1016/j.hydromet.2004.01.007.
Zhu W, Li Y, Zeng F, Yin H, Wang L, Zhu H, Superparamagnetic Fe3O4 nanoparticles modified by water-soluble and biocompatible polyethylenimine for lipase immobilization with physical and chemical mechanisms, RSC Adv., 5, 23039–23045, 2015. doi: 10.1039/C4RA15832F.
Chen D, Chen D, Jiao X, Zhao Y, He M, Hydrothermal synthesis and characterization of octahedral nickel ferrite particles, Powder Technology,133, 247-250, 2003. doi:10.1016/S0032-5910(03)00079-2. [17] Deraz NM, Production and characterization of pure and doped copper ferrite nanoparticles, J. Anal. Appl. Pyrolysis, 82(2), 212-222, 2008. doi:10.1016/j.jaap.2008.03.009.
Alarifi A, Deraz NM, Shaban S, Structural, morphological and magnetic properties of NiFe2O4 nano-particles, J Alloys Compd., 486(1-2), 501-506, 2009. doi:10.1016/j.jallcom.2009.06.192.
Oliveira FCC, Rossi LM, Jardim RF, Rubim JC, Magnetic Fluids Based on γ-Fe2O3 and CoFe2O4 Nanoparticles Dispersed in Ionic Liquids, J. Phys. Chem. C, 113(18), 8566–8572, 2009. doi: 10.1021/jp810501m.
El-Sayed AM, Influence of zinc content on some properties of Ni-Zn ferrites, Ceram. Int., 28(4), 363-367, 2002. doi:10.1016/S0272-8842(01)00103-1.
Manikandan A, Vijaya JJ, Kennedy LJ, Bououdina M, Microwave combustion synthesis, structural, optical and magnetic properties of Zn1−xSrxFe2O4 nanoparticles, Ceramics International, 39, 5909- 5917, 2013. doi:10.1016/j.ceramint.2013.01.012.
Manikandan A, Vijaya JJ, L. Kennedy J, Bououdina M, Structural, optical and magnetic properties of Zn1−xCuxFe2O4nanoparticles prepared by microwave combustion method, Journal of Molecular Structure, 1035, 332-340, 2013. doi:10.1016/j.molstruc.2012.11.007.
Bastami TR, Entezari MH, Kwong C, Qiao S, Influences of spinel type and polymeric surfactants on thesize evolution of colloidal magnetic nanocrystals (MFe2O4,M = Fe, Mn), Chem. Sci. Eng., 8(3), 378–385, 2014. doi: 10.1007/s11705-014-1441-y
Nejati K, Zabihi R, Preparation and magnetic properties of nano size nickel ferrite particles using hydrothermal method, Chemistry Central Journal, 6, 23, 2012. doi: 10.1186/1752-153X-6-23.
Manova E, Tsoncheva T, Estournes C, Paneva D, Tenchev K, Mitov I, Petrov L, Nanosized iron and iron-cobalt spinel oxides as catalysts formethanol decomposition, Appl. Catal. A, 300(2), 170-180, 2006. doi:10.1016/j.apcata.2005.11.005.
Hi J, Wang Y, Lu Y, Ma J, Luo G, In situ preparation of magneticchitosan/Fe3O4 composite nanoparticles in tiny pools of water-in-oilmicroemulsion, Reac. Funct. Polym., 66(12), 1552-1558, 2006. doi:10.1016/j.reactfunctpolym.2006.05.006.

Details

Primary Language

English

Subjects

-

Journal Section

-

Authors

Sema Vural

Aysel Bayrak Alphan This is me

Süleyman Köytepe This is me

Turgay Seçkin This is me

Publication Date

April 25, 2016

Submission Date

January 20, 2016

Acceptance Date

-

Published in Issue

Year 2016 Volume: 17 Number: 1

DOI

https://doi.org/10.18038/btda.19450

IZ

https://izlik.org/JA83KT84PT

APA

Vural, S., Bayrak Alphan, A., Köytepe, S., & Seçkin, T. (2016). SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI. Anadolu University Journal of Science and Technology A - Applied Sciences and Engineering, 17(1), 111-120. https://doi.org/10.18038/btda.19450

AMA

1.Vural S, Bayrak Alphan A, Köytepe S, Seçkin T. SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI. AUJST-A. 2016;17(1):111-120. doi:10.18038/btda.19450

Chicago

Vural, Sema, Aysel Bayrak Alphan, Süleyman Köytepe, and Turgay Seçkin. 2016. “SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI Ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI”. Anadolu University Journal of Science and Technology A - Applied Sciences and Engineering 17 (1): 111-20. https://doi.org/10.18038/btda.19450.

EndNote

Vural S, Bayrak Alphan A, Köytepe S, Seçkin T (June 1, 2016) SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI. Anadolu University Journal of Science and Technology A - Applied Sciences and Engineering 17 1 111–120.

IEEE

[1]S. Vural, A. Bayrak Alphan, S. Köytepe, and T. Seçkin, “SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI”, AUJST-A, vol. 17, no. 1, pp. 111–120, June 2016, doi: 10.18038/btda.19450.

ISNAD

Vural, Sema - Bayrak Alphan, Aysel - Köytepe, Süleyman - Seçkin, Turgay. “SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI Ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI”. Anadolu University Journal of Science and Technology A - Applied Sciences and Engineering 17/1 (June 1, 2016): 111-120. https://doi.org/10.18038/btda.19450.

JAMA

1.Vural S, Bayrak Alphan A, Köytepe S, Seçkin T. SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI. AUJST-A. 2016;17:111–120.

MLA

Vural, Sema, et al. “SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI Ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI”. Anadolu University Journal of Science and Technology A - Applied Sciences and Engineering, vol. 17, no. 1, June 2016, pp. 111-20, doi:10.18038/btda.19450.

Vancouver

1.Sema Vural, Aysel Bayrak Alphan, Süleyman Köytepe, Turgay Seçkin. SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI. AUJST-A. 2016 Jun. 1;17(1):111-20. doi:10.18038/btda.19450

Abstract

SPİNEL FERRİT NANO-PARÇACIKLARININ HİDROTERMAL SENTEZ TEKNİĞİ KULLANILARAK HAZIRLANMASI ve MANYETİK ÖZELLİKLERİNİN ARAŞTIRILMASI

Abstract

Keywords

References

Details

Primary Language

Subjects

Journal Section

Authors

Publication Date

Submission Date

Acceptance Date

Published in Issue

DOI

IZ

Cite