THE COMPARATIVE METHODS POWDER AND GLASS DONE BY XRF DETERMINE OF MAIN OXIDE COMPONENTS IN CEMENT CLINKER

Yıl 2005, Sayı: 009, 157 - 163, 15.12.2005

B. Yılmaz

Öz

The aim of this study is to compare the results of chemical analysis done by XRF method with the result of chemical analyses done by traditional method for the samples of cement clinker. Initially, the sample of clinker were being chemically analyzed in accordance with traditional methot. Socondly, the same samples were being prepared both powder and glass specimen and analyzed by XRF method. Later on the each resuls of the latter are being comparedto the results of former one separately. İt is concluded that the results of both analysis done by XRF method are about the same as the results of the analyses done by the traditional method.

Anahtar Kelimeler

Traditional chemical analysis, Clinker, Powder and glass specimen, XRF

ÇİMENTO KLİNKERİNİN ANA OKSİT BİLEŞENLERİNİN XRF İLE SAPTANMASINDA TOZ ve CAM YÖNTEMLERİNİN KARŞILAŞTIRILMASI

Öz

Bu çalışma çimento klinkerinin ana oksit bileşenlerinin analizinde klasik kimyasal yöntemlerle, toz ve cam örnek hazırlama metotlarına göre hazırlanmış örneklerin XRF analizlerinin karşılaştırılması amacıyla yapılmıştır. Klinker örnekleri önce klasik kimyasal yöntemlerle analiz edilmiş ve daha sonra aynı örnekler toz ve cam tablet (flux) metotlarıyla hazırlanarak XRF’de analiz edilmiş ve bulunan sonuçlar karşılaştırılmıştır. Klasik kimyasal yöntemle bulunan sonuçlarla örnek hazırlamada oluşan hataların kabul edilebilir sınırlar içinde olması nedeniyle XRF teknikleriyle bulunan sonuçların tekrarlanabilirlik açısından benzer değerler verdiği görülmüştür.

Anahtar Kelimeler

Klasik kimyasal analiz, Klinker, Toz ve cam tablet, XRF

Kaynakça

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