Method Validation for The Determination of Toxic Elements in Fizzy Fruity Mineral Water Drinks Using ICP-MS

Yıl 2019, Cilt: 2 Sayı: 2, 38 - 41, 06.12.2019

Serpil Kılıç , Murat Kılıç

Öz

The presence of metallic impurities in fizzy fruity mineral water drinks
can constitute health hazards to the public. In this study, the Inductively
Coupled Plasma Mass Spectrometry (ICP-MS) was chosen to be validated, and
applied in suitable method of analysis for determination of antimony, lead and
cadmium in samples. The detection limits, quantification limits, linearity,
accuracy parameters were studied under optimised ICP-MS conditions. The method
trueness was confirmed by using certified references materials LGC soft drink
and obtained results were had acceptable Z-score values. The results obtained
make the method suitable for a precise determination of validated elements in
different brands of samples at these low concentration values.  Also, the results obtained were check with
permissible levels, daily intake (EDI), target hazard quotient (THQ) and hazard
index (HI).

Anahtar Kelimeler

Fizzy fruity mineral water, Health risk, ICP-MS

Destekleyen Kurum

AKDENİZ ÜNİVERSİTESİ

Proje Numarası

FBA-2019- 4371

Teşekkür

This work was financially supported by the University of Akdeniz Scientific Research Projects Support Unit (FBA-2019- 4371).

Kaynakça

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