FEB 2011/02-BAGEP
A new asymmetric bidentate Schiff base ligand was synthesized from 4-Methoxysalicylaldehyde. The complex was prepared by adding Zn(II) acetate salt dissolved in methanol to the Schiff base ligand. The ligand and its metal complex were characterized by elemental analysis (CHN), FT-IR, UV-Vis spectroscopy, 1H NMR, TG/DTG, SEM and conductometric measurements. The spectroscopic data reveals that the Zn(II) atom in the center of the complex is four-coordinated by two phenolic oxygen atoms and two azomethine nitrogen atoms of two Schiff base ligands. The Zn(II) complex is diamagnetic as expected for d10 metal ions in a tetrahedral geometry. The Zn(II) complex is soluble in DMSO and DMF and is insoluble in acetone, chloroform, ethanol and methanol. The conductance data indicate that the complex is non-electrolytes.
Schiff base Zinc(II) complexes IR analysis Thermogravimetric analysis
Niğde Ömer Halisdemir University Scientific Research Projects Coordinator
FEB 2011/02-BAGEP
The work was supported by Niğde Ömer Halisdemir University Scientific Research Projects Coordinator (FEB 2011/02-BAGEP).
Birincil Dil | İngilizce |
---|---|
Konular | Klasik Fizik (Diğer) |
Bölüm | Araştırma Makaleleri |
Yazarlar | |
Proje Numarası | FEB 2011/02-BAGEP |
Yayımlanma Tarihi | 3 Kasım 2020 |
Yayımlandığı Sayı | Yıl 2020 Cilt: 1 Sayı: 1 |