Yıl 2019, Cilt 7 , Sayı , Sayfalar 192 - 198 2019-11-24

PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film

Ahmed ZOUAOUI [1]


Actually, lead dioxide (PbO2) is used as electrodes (cathode) in electrochemical power generators in particular in car batteries. The synthesis of lead dioxide is essentially obtained by chemical or electrochemical oxidation of lead salts processes. A very ambitious objective of this study is based on preparing lead dioxide by a newly developed method carried out in our laboratory. This consists in a first step to deposit a conductive polymer film poly[4-(pyrrol-1-yl methyl) benzoïc acid] having complexing properties performed by electrochemical oxidation in acetonitrile medium of the monomer 4-(pyrrol-1-yl methyl) benzoïc acid on the surface of a substrate such as carbon felt having a very high specific surface. In a second step, we proceed to the incorporation of lead dioxide by complexing the metal cations of lead in the polymer film performed by immersion of the modified electrode in a solution of lead nitrate to complex the Pb2 + cation with the carboxylic group COOH present in the polymer structure followed by electrooxidation in a solution free of lead to precipitate lead dioxide into the polymer in the form of metal microparticles. This material is used as the cathode material in batteries.
Conductive polymer, Modified electrodes, Lead dioxide, Batteries
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Birincil Dil en
Konular Mühendislik
Bölüm Makaleler
Yazarlar

Yazar: Ahmed ZOUAOUI
Kurum: Université Ferhat Abbas Sétif 1
Ülke: Algeria


Tarihler

Yayımlanma Tarihi : 24 Kasım 2019

Bibtex @araştırma makalesi { epstem655388, journal = {The Eurasia Proceedings of Science Technology Engineering and Mathematics}, issn = {}, eissn = {2602-3199}, address = {isresoffice@gmail.com}, publisher = {ISRES Organizasyon Turizm Eğitim Danışmanlık Ltd. Şti.}, year = {2019}, volume = {7}, pages = {192 - 198}, doi = {}, title = {PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film}, key = {cite}, author = {ZOUAOUI, Ahmed} }
APA ZOUAOUI, A . (2019). PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film. The Eurasia Proceedings of Science Technology Engineering and Mathematics , 7 () , 192-198 . Retrieved from https://dergipark.org.tr/tr/pub/epstem/issue/50288/655388
MLA ZOUAOUI, A . "PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film". The Eurasia Proceedings of Science Technology Engineering and Mathematics 7 (2019 ): 192-198 <https://dergipark.org.tr/tr/pub/epstem/issue/50288/655388>
Chicago ZOUAOUI, A . "PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film". The Eurasia Proceedings of Science Technology Engineering and Mathematics 7 (2019 ): 192-198
RIS TY - JOUR T1 - PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film AU - Ahmed ZOUAOUI Y1 - 2019 PY - 2019 N1 - DO - T2 - The Eurasia Proceedings of Science Technology Engineering and Mathematics JF - Journal JO - JOR SP - 192 EP - 198 VL - 7 IS - SN - -2602-3199 M3 - UR - Y2 - 2020 ER -
EndNote %0 The Eurasia Proceedings of Science Technology Engineering and Mathematics PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film %A Ahmed ZOUAOUI %T PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film %D 2019 %J The Eurasia Proceedings of Science Technology Engineering and Mathematics %P -2602-3199 %V 7 %N %R %U
ISNAD ZOUAOUI, Ahmed . "PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film". The Eurasia Proceedings of Science Technology Engineering and Mathematics 7 / (Kasım 2019): 192-198 .
AMA ZOUAOUI A . PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film. EPSTEM. 2019; 7: 192-198.
Vancouver ZOUAOUI A . PbO2 Synthesis by Complexation and Electrooxidation of Pb2+ in Poly[4-(pyrrol-1-yl methyl) benzoic acid] Film. The Eurasia Proceedings of Science Technology Engineering and Mathematics. 2019; 7: 198-192.