Yıl 2020, Cilt 11 , Sayı , Sayfalar 1 - 4 2020-12-31

Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water

Jelena LUKIĆ [1] , Tatjana ĐURKIĆ [2] , Jelena RADULOVIĆ [3] , Tamara BAKIĆ [4] , Antonije ONJIA [5]


A Plackett-Burman factorial design (PBD) has been used for the optimization of dispersive liquid-liquid microextraction (DLLME) of UV filters from water. The experimental procedure included a DLLME sample preparation prior to high-performance liquid chromatography triple quadrupole mass spectrometry (HPLC-MS/MS) measurements. The variables of the DLLME process for simultaneous preconcentration of UV filters (avobenzone and octocrylene) have been studied using PBD with twelve experimental runs. Several experimental variables including the extractant type, pH value, the disperser type, extractant volume, disperser volume, vortexing/sonication, centrifugation speed, reconstitution solvent, salt content, temperature, and centrifugation time were considered in the optimization process. PBD results revealed the most important variables that affected the extraction efficiency (EF). The first three most influential variables, as showed using a Pareto graph, were in the following order: the extractant volume > the disperser type > the extraction temperature. Based on the main effects plot, it was revealed that some variables (pH value, the disperser type, extractant volume, temperature, centrifugation speed, salt content) increased over the experimental domain, while the others (the extractant type, disperser volume, vortexing/sonication, centrifugation time, reconstitution solvent) decreased
UV filters, Plackett- Burman, DLLME, HPLC-MS/MS
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Birincil Dil en
Konular Mühendislik
Bölüm Makaleler
Yazarlar

Yazar: Jelena LUKIĆ
Kurum: Innovation Center of the Faculty of Technology and Metallurgy
Ülke: Serbia


Yazar: Tatjana ĐURKIĆ
Kurum: Belgrade University
Ülke: Serbia


Yazar: Jelena RADULOVIĆ
Kurum: Anahem Laboratory
Ülke: Serbia


Yazar: Tamara BAKIĆ
Kurum: Innovation Center of the Faculty of Technology and Metallurgy
Ülke: Serbia


Yazar: Antonije ONJIA
Kurum: Belgrade University
Ülke: Serbia


Tarihler

Yayımlanma Tarihi : 31 Aralık 2020

Bibtex @konferans bildirisi { epstem836125, journal = {The Eurasia Proceedings of Science Technology Engineering and Mathematics}, issn = {}, eissn = {2602-3199}, address = {isresoffice@gmail.com}, publisher = {ISRES Organizasyon Turizm Eğitim Danışmanlık Ltd. Şti.}, year = {2020}, volume = {11}, pages = {1 - 4}, doi = {}, title = {Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water}, key = {cite}, author = {Lukıć, Jelena and Đurkıć, Tatjana and Radulovıć, Jelena and Bakıć, Tamara and Onjıa, Antonije} }
APA Lukıć, J , Đurkıć, T , Radulovıć, J , Bakıć, T , Onjıa, A . (2020). Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water . The Eurasia Proceedings of Science Technology Engineering and Mathematics , 11 , 1-4 . Retrieved from https://dergipark.org.tr/tr/pub/epstem/issue/58065/836125
MLA Lukıć, J , Đurkıć, T , Radulovıć, J , Bakıć, T , Onjıa, A . "Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water" . The Eurasia Proceedings of Science Technology Engineering and Mathematics 11 (2020 ): 1-4 <https://dergipark.org.tr/tr/pub/epstem/issue/58065/836125>
Chicago Lukıć, J , Đurkıć, T , Radulovıć, J , Bakıć, T , Onjıa, A . "Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water". The Eurasia Proceedings of Science Technology Engineering and Mathematics 11 (2020 ): 1-4
RIS TY - JOUR T1 - Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water AU - Jelena Lukıć , Tatjana Đurkıć , Jelena Radulovıć , Tamara Bakıć , Antonije Onjıa Y1 - 2020 PY - 2020 N1 - DO - T2 - The Eurasia Proceedings of Science Technology Engineering and Mathematics JF - Journal JO - JOR SP - 1 EP - 4 VL - 11 IS - SN - -2602-3199 M3 - UR - Y2 - 2020 ER -
EndNote %0 The Eurasia Proceedings of Science Technology Engineering and Mathematics Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water %A Jelena Lukıć , Tatjana Đurkıć , Jelena Radulovıć , Tamara Bakıć , Antonije Onjıa %T Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water %D 2020 %J The Eurasia Proceedings of Science Technology Engineering and Mathematics %P -2602-3199 %V 11 %N %R %U
ISNAD Lukıć, Jelena , Đurkıć, Tatjana , Radulovıć, Jelena , Bakıć, Tamara , Onjıa, Antonije . "Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water". The Eurasia Proceedings of Science Technology Engineering and Mathematics 11 / (Aralık 2020): 1-4 .
AMA Lukıć J , Đurkıć T , Radulovıć J , Bakıć T , Onjıa A . Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water. EPSTEM. 2020; 11: 1-4.
Vancouver Lukıć J , Đurkıć T , Radulovıć J , Bakıć T , Onjıa A . Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water. The Eurasia Proceedings of Science Technology Engineering and Mathematics. 2020; 11: 1-4.
IEEE J. Lukıć , T. Đurkıć , J. Radulovıć , T. Bakıć ve A. Onjıa , "Screening Design of Experiment Applied to Dispersive Liquid-Liquid Microextraction of UV Filters from Water", The Eurasia Proceedings of Science Technology Engineering and Mathematics, c. 11, ss. 1-4, Ara. 2021