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SUSTAINABLE COMPOSITES: INVESTIGATION OF OLIVE SEED AND BASIL LEAF POWDER MATERIALS

Year 2026, Volume: 27 Issue: 1 , 39 - 62 , 27.03.2026
https://doi.org/10.18038/estubtda.1715002
https://izlik.org/JA23EJ27PN

Abstract

In this study, biocomposite materials resistant to various effects (heat and humidity) were produced by using olive seed powder and basil leaf powder as reinforcing elements at different ratios (30%-0%, 25%-5%, 20%-10%, 15%-15%, 10%-20%, 5%-25%, 0%-30%) and the effects of these ratios were obtained as a result of tests. In the samples produced using olive kernel powder and basil leaf powder, it was observed that the powder ratio added to the mixture had significant effects on the properties in tensile, impact, hardness, water absorption, and ignition loss tests. In the tensile strength test, the sample produced using 30% olive pomace powder showed the highest tensile strength with 28.892 MPa, while a value of 23.39 MPa was observed with 30% basil leaf powder. In the impact energy test, the BLP5 sample produced using 5% basil leaf powder had the highest resistance with 0.808 J. In the Vickers hardness test, the BLP30 sample with 30% basil leaf powder reached the highest value (150.4 HV) among the samples produced using basil leaf powder, while the BLP0 sample produced using olive pomace powder with the same 30% pomace powder ratio reached 120.11 HV. In the water absorption test, a decrease in water absorption capacity was observed as the basil leaf powder ratio increased and the lowest absorption capacity was observed in BLP30 specimen produced using 30% basil leaf powder. However, it was observed that the specimens produced using olive seed powder by weight had less water absorption capacity than the specimens produced using basil leaf powder by weight. In the ignition loss test, the weight loss increased with higher olive seed or basil leaf powder content, reflecting the greater organic fraction in these samples. Based on these results, it is aimed to be used in the automotive sector in areas where water and heat contact is high.

References

  • [1] Ayyanar CB, Kumar R, Helaili S, Gayathri B, Rinusuba V, Nalini EH, et al. Experimental and numerical analysis of natural fillers loaded and E-glass reinforced epoxy sandwich composites. J Mater Res Technol. 2024; 32:1235-1244. doi: 10.1016/j.jmrt.2024.07.142.
  • [2] Ilhan R, Feyzullahoğlu E. Natural fibers and filler materials used in glass fiber reinforced polyester (GFRP) composite materials. El-Cezerî J Sci Eng. 2019; 6:355-381. doi:10.31202/ecjse.519072.
  • [3] Dhanabalan D, Rathanasamy R, Vediappan V, Raghuraj N, Kathiresan P, Jeyakumar T, Muthaiya P. Experimental investigation of date seed and neem powder reinforced natural fiber composites. Medžiagotyra. 2024; 30:334-339. doi:10.5755/j02.ms.34033.
  • [4] Taşdemir M, Kaştan A. Mechanical properties of polypropylene composite with added olive seed powder. Uluslararası Batı Karadeniz Mühendislik ve Fen Bilimleri Dergisi. 2022; 4:36-49.
  • [5] Tuna S, Şen İ. Characterization of olive seed powder incorporated low density polyethylene composites. Sakarya Univ J Sci. 2025; 29:71-82.
  • [6] Omrani E, Menezes PL, Rohatgi PK. State of the art on tribological behavior of polymer matrix composites reinforced with natural fibers in the green materials world. Eng Sci Technol Int J. 2016;19(2):717-736.
  • [7] Giyatmi G, Irianto HE, Anggoro B, Fransiska D. Use of basil leaf ethanol extract in alginate base edible film. J Phys Conf Ser. 2021; 1933:012001.
  • [8] Rana AK, Mandal A, Bandyopadhyay S. Short jute fiber reinforced polypropylene composites: effect of compatibiliser, impact modifier and fiber loading. Compos Sci Technol. 2003; 63:801-806.
  • [9] Panaitescu I, Koch T, Archodoulaki VM. Effects of temperature, humidity and automotive fluids exposure on glass fiber/polyurethane composites. Polym Compos. 2019;40(6):2357-2367.
  • [10] Bledzki AK, Gassan J. Composites reinforced with cellulose-based fibres. Prog Polym Sci. 1999; 24:221-274.
  • [11] Jawaid M, Khalil HPSA. Cellulosic/synthetic fibre reinforced polymer hybrid composites: A review. Carbohydr Polym. 2011; 86:1-18.
  • [12] Menezes PL, Rohatgi PK, Lovell MR. Studies on the tribological behavior of natural fiber reinforced polymer composite. In: Green Tribology: Biomimetics, Energy Conservation and Sustainability. 2012:329-345.
  • [13] Dittenber DB, GangaRao HV. Critical review of recent publications on use of natural composites in infrastructure. Compos Part A Appl Sci Manuf. 2012; 43:1419-1429.
  • [14] Potluri R, Krishna NC. Potential and applications of green composites in industrial space. Mater Today Proc. 2020; 22:2041-2048.
  • [15] Holbery J, Houston D. Natural-fiber-reinforced polymer composites in automotive applications. JOM. 2006;58(11):80–86. doi:10.1007/s11837-006-0234-2
  • [16] Mathieux F, Evrard D, Brissaud D, De F. Use of recycled natural fibres in industrial products: A comparative LCA case study on acoustic components in the Brazilian automotive sector. Resour Conserv Recycl. 2014; 84:1-14.
  • [17] Fan M, Fu F. Introduction: A perspective–natural fibre composites in construction. In: Advanced High Strength Natural Fibre Composites in Construction. Woodhead Publishing; 2017:1-20.
  • [18] Potluri R. Natural fiber-based hybrid bio-composites: processing, characterization, and applications. In: Green Composites: Processing, Characterisation and Applications for Textiles. Springer Singapore; 2018:1-46.
  • [19] Lucintel B. Opportunities in Natural Fiber Composites. Dallas, TX: Lucintel; 2011.
  • [20] Zuhair MRM, et al. Application of Natural Fibre Composite in the Aviation Industry. Journal of Aviation Science and Technology, 2020;1(1), 1–5
  • [21] John MJ, Thomas S. Biofibres and biocomposites. Carbohydr Polym. 2008; 71:343-364.
  • [22] Madhu P, Sanjay MR, Senthamaraikannan P, Pradeep S, Saravanakumar SS, Yogesha B. A review on synthesis and characterization of commercially available natural fibers: Part II. J Nat Fibers. 2019; 16:25-36.
  • [23] Al Rashid A, Khalid MY, Imran R, Ali U, Koc M. Utilization of banana fiber-reinforced hybrid composites in the sports industry. Materials. 2020; 13:3167.
  • [24] Devadiga DG, Bhat KS, Mahesha GT. Sugarcane bagasse fiber reinforced composites: Recent advances and applications. Cogent Eng. 2020;7(1):1823159.
  • [25] Jothibasu S, Mohanamurugan S, Vijay R, Singaravelu DL, Vinod A, Sanjay MR. Investigation on the mechanical behavior of areca sheath fibers/jute fibers/glass fabrics reinforced hybrid composite for light weight applications. J Ind Text. 2020; 49:1036-1060.
  • [26] Roumeli E, Terzopoulou Z, Pavlidou E, Chrissafis K, Papadopoulou E, Athanasiadou E, et al. Effect of maleic anhydride on the mechanical and thermal properties of hemp/high-density polyethylene green composites. J Therm Anal Calorim. 2015; 121:93-105.
  • [27] Russo P, Simeoli G, Acierno D, Lopresto V. Mechanical properties of virgin and recycled polyolefin‐based composite laminates reinforced with jute fabric. Polym Compos. 2015; 36:2022-2029.
  • [28] Sakar E, Ünver H. Olive cultivation and some conducted selection and adaptation studies in Turkey. J Agric Fac HR.U. 2011; 15:19-25.
  • [29] Savran MK. Olive cultivation in the world and in Turkey. Available at: https://www.tarimorman.gov.tr/BUGEM/kumelenme/Belgeler/Budama/Du%C C%88nyada%20ve%20Tu%CC%88rkiye%27de%20Zeytincilik.pdf. Accessed August 15, 2025.
  • [30] Mohammed AA. Study the thermal properties and water absorption of composite materials reinforced with date and olive seeds. Iraqi J Mech Mater Eng. 2015;15(2):138-152.
  • [31] El-Aassar MR, Mohamed FM, Alsohaimi IH, Khalifa RE. Fabrication of novel valorized ecofriendly olive seed residue/anthracite/chitosan composite for removal of Cr(VI): Kinetics, isotherms and thermodynamics modeling. Cellulose. 2021; 28:7165-7183.
  • [32] Valvez S, Maceiras A, Santos P, Reis PNB. Olive stones as filler for polymer-based composites: a review. Materials. 2021;14(4):845.
  • [33] Pardalis N, Xanthopoulou E, Zamboulis A, Bikiaris DN. Olive stone as a filler for recycled high-density polyethylene: A promising valorization of solid wastes from olive oil industry. Sustain Chem Environ. 2024; 6:100090.
  • [34] Adibelli Ü, Mutlu D, Çakir Yiğit N, Karagöz İ. Preparation and characterization of walnut shell filled epoxy hybrid composites. 10th Int. Symp. Fibers Polym Symp. Res.; 2022. 13–14 th May,81-89.
  • [35] Özmeral N, Kocaman S, Soydal Ü, Ahmetli G. Investigation of epoxy biocomposites filled with almond shell waste. Pamukkale Univ. J Eng. Sci. 2023; 29:546–52.
  • [36] Aydın HY, Altun S. Polylactic acid matrix composites reinforced with wood-based materials. Bartin Orman Fak. Derg. 2020; 22:1061–76.
  • [37] TOS The Organic Spices. Official website. Available at: https://www.tosmagaza.com/. Accessed August 23, 2025.
  • [38] Dost Kimya. (n.d.). MGS Laminasyon Epoksi Reçine L160. Dost Kimya. Retrieved May 28, 2025, from https://dostkimya.com.tr/tr/urunler/epoksi-sistemler/mgs-laminasyon-epoksi-recine-l160.
  • [39] Saw SK, Purwar, R Nandy S, Ghose J, and Sarkhel G. Fabrication, Characterization, and Evaluation of Luffa cylindrica Fiber Reinforced Epoxy Composites. BioResources, 2013;8(4), 4805-4826.
  • [40] Rudawska A, Adhesives and adhesive joints in industry applications. IntechOpen, London, United Kingdom, 2019.
  • [41] ASTM D3039/D3039-M. Standard Test Method for Tensile Properties of Polymer Matrix Composite Material, ASTM International, West Conshohocken, 2000.
  • [42] ASTM D6110-10. Standard Test Method for Determining the Charpy Impact Resistance of Notched Specimens of Plastics, ASTM International, West Conshohocken. 2010.
  • [43] ASTM E92–17. Standard Test Methods for Vickers Hardness and Knoop Hardness of Metallic Materials ASTM International, West Conshohocken. Philadelphia. 2017.
  • [44] ASTM D 5229. Standard Test Method for Moisture Absorption Properties and Equilibrium Conditioning of Polymer Matrix Composite Materials, ASTM International, West Conshohocken, 2004.
  • [45] ASTM D 2584-02. Standard Test Method for Ignition Loss of Cured Reinforced Resins, ASTM International, West Conshohocken 2002.
  • [46] Karacor B, Özcanlı M. Investigation of use of hybrid composite materials in automobile interior. Int. J. Automot. Eng. Technol. 2020;9(4):214–28.

SUSTAINABLE COMPOSITES: INVESTIGATION OF OLIVE SEED AND BASIL LEAF POWDER MATERIALS

Year 2026, Volume: 27 Issue: 1 , 39 - 62 , 27.03.2026
https://doi.org/10.18038/estubtda.1715002
https://izlik.org/JA23EJ27PN

Abstract

In this study, biocomposite materials resistant to various effects (heat and humidity) were produced by using olive seed powder and basil leaf powder as reinforcing elements at different ratios (30%-0%, 25%-5%, 20%-10%, 15%-15%, 10%-20%, 5%-25%, 0%-30%) and the effects of these ratios were obtained as a result of tests. In the samples produced using olive kernel powder and basil leaf powder, it was observed that the powder ratio added to the mixture had significant effects on the properties in tensile, impact, hardness, water absorption, and ignition loss tests. In the tensile strength test, the sample produced using 30% olive pomace powder showed the highest tensile strength with 28.892 MPa, while a value of 23.39 MPa was observed with 30% basil leaf powder. In the impact energy test, the BLP5 sample produced using 5% basil leaf powder had the highest resistance with 0.808 J. In the Vickers hardness test, the BLP30 sample with 30% basil leaf powder reached the highest value (150.4 HV) among the samples produced using basil leaf powder, while the BLP0 sample produced using olive pomace powder with the same 30% pomace powder ratio reached 120.11 HV. In the water absorption test, a decrease in water absorption capacity was observed as the basil leaf powder ratio increased and the lowest absorption capacity was observed in BLP30 specimen produced using 30% basil leaf powder. However, it was observed that the specimens produced using olive seed powder by weight had less water absorption capacity than the specimens produced using basil leaf powder by weight. In the ignition loss test, the weight loss increased with higher olive seed or basil leaf powder content, reflecting the greater organic fraction in these samples. Based on these results, it is aimed to be used in the automotive sector in areas where water and heat contact is high.

References

  • [1] Ayyanar CB, Kumar R, Helaili S, Gayathri B, Rinusuba V, Nalini EH, et al. Experimental and numerical analysis of natural fillers loaded and E-glass reinforced epoxy sandwich composites. J Mater Res Technol. 2024; 32:1235-1244. doi: 10.1016/j.jmrt.2024.07.142.
  • [2] Ilhan R, Feyzullahoğlu E. Natural fibers and filler materials used in glass fiber reinforced polyester (GFRP) composite materials. El-Cezerî J Sci Eng. 2019; 6:355-381. doi:10.31202/ecjse.519072.
  • [3] Dhanabalan D, Rathanasamy R, Vediappan V, Raghuraj N, Kathiresan P, Jeyakumar T, Muthaiya P. Experimental investigation of date seed and neem powder reinforced natural fiber composites. Medžiagotyra. 2024; 30:334-339. doi:10.5755/j02.ms.34033.
  • [4] Taşdemir M, Kaştan A. Mechanical properties of polypropylene composite with added olive seed powder. Uluslararası Batı Karadeniz Mühendislik ve Fen Bilimleri Dergisi. 2022; 4:36-49.
  • [5] Tuna S, Şen İ. Characterization of olive seed powder incorporated low density polyethylene composites. Sakarya Univ J Sci. 2025; 29:71-82.
  • [6] Omrani E, Menezes PL, Rohatgi PK. State of the art on tribological behavior of polymer matrix composites reinforced with natural fibers in the green materials world. Eng Sci Technol Int J. 2016;19(2):717-736.
  • [7] Giyatmi G, Irianto HE, Anggoro B, Fransiska D. Use of basil leaf ethanol extract in alginate base edible film. J Phys Conf Ser. 2021; 1933:012001.
  • [8] Rana AK, Mandal A, Bandyopadhyay S. Short jute fiber reinforced polypropylene composites: effect of compatibiliser, impact modifier and fiber loading. Compos Sci Technol. 2003; 63:801-806.
  • [9] Panaitescu I, Koch T, Archodoulaki VM. Effects of temperature, humidity and automotive fluids exposure on glass fiber/polyurethane composites. Polym Compos. 2019;40(6):2357-2367.
  • [10] Bledzki AK, Gassan J. Composites reinforced with cellulose-based fibres. Prog Polym Sci. 1999; 24:221-274.
  • [11] Jawaid M, Khalil HPSA. Cellulosic/synthetic fibre reinforced polymer hybrid composites: A review. Carbohydr Polym. 2011; 86:1-18.
  • [12] Menezes PL, Rohatgi PK, Lovell MR. Studies on the tribological behavior of natural fiber reinforced polymer composite. In: Green Tribology: Biomimetics, Energy Conservation and Sustainability. 2012:329-345.
  • [13] Dittenber DB, GangaRao HV. Critical review of recent publications on use of natural composites in infrastructure. Compos Part A Appl Sci Manuf. 2012; 43:1419-1429.
  • [14] Potluri R, Krishna NC. Potential and applications of green composites in industrial space. Mater Today Proc. 2020; 22:2041-2048.
  • [15] Holbery J, Houston D. Natural-fiber-reinforced polymer composites in automotive applications. JOM. 2006;58(11):80–86. doi:10.1007/s11837-006-0234-2
  • [16] Mathieux F, Evrard D, Brissaud D, De F. Use of recycled natural fibres in industrial products: A comparative LCA case study on acoustic components in the Brazilian automotive sector. Resour Conserv Recycl. 2014; 84:1-14.
  • [17] Fan M, Fu F. Introduction: A perspective–natural fibre composites in construction. In: Advanced High Strength Natural Fibre Composites in Construction. Woodhead Publishing; 2017:1-20.
  • [18] Potluri R. Natural fiber-based hybrid bio-composites: processing, characterization, and applications. In: Green Composites: Processing, Characterisation and Applications for Textiles. Springer Singapore; 2018:1-46.
  • [19] Lucintel B. Opportunities in Natural Fiber Composites. Dallas, TX: Lucintel; 2011.
  • [20] Zuhair MRM, et al. Application of Natural Fibre Composite in the Aviation Industry. Journal of Aviation Science and Technology, 2020;1(1), 1–5
  • [21] John MJ, Thomas S. Biofibres and biocomposites. Carbohydr Polym. 2008; 71:343-364.
  • [22] Madhu P, Sanjay MR, Senthamaraikannan P, Pradeep S, Saravanakumar SS, Yogesha B. A review on synthesis and characterization of commercially available natural fibers: Part II. J Nat Fibers. 2019; 16:25-36.
  • [23] Al Rashid A, Khalid MY, Imran R, Ali U, Koc M. Utilization of banana fiber-reinforced hybrid composites in the sports industry. Materials. 2020; 13:3167.
  • [24] Devadiga DG, Bhat KS, Mahesha GT. Sugarcane bagasse fiber reinforced composites: Recent advances and applications. Cogent Eng. 2020;7(1):1823159.
  • [25] Jothibasu S, Mohanamurugan S, Vijay R, Singaravelu DL, Vinod A, Sanjay MR. Investigation on the mechanical behavior of areca sheath fibers/jute fibers/glass fabrics reinforced hybrid composite for light weight applications. J Ind Text. 2020; 49:1036-1060.
  • [26] Roumeli E, Terzopoulou Z, Pavlidou E, Chrissafis K, Papadopoulou E, Athanasiadou E, et al. Effect of maleic anhydride on the mechanical and thermal properties of hemp/high-density polyethylene green composites. J Therm Anal Calorim. 2015; 121:93-105.
  • [27] Russo P, Simeoli G, Acierno D, Lopresto V. Mechanical properties of virgin and recycled polyolefin‐based composite laminates reinforced with jute fabric. Polym Compos. 2015; 36:2022-2029.
  • [28] Sakar E, Ünver H. Olive cultivation and some conducted selection and adaptation studies in Turkey. J Agric Fac HR.U. 2011; 15:19-25.
  • [29] Savran MK. Olive cultivation in the world and in Turkey. Available at: https://www.tarimorman.gov.tr/BUGEM/kumelenme/Belgeler/Budama/Du%C C%88nyada%20ve%20Tu%CC%88rkiye%27de%20Zeytincilik.pdf. Accessed August 15, 2025.
  • [30] Mohammed AA. Study the thermal properties and water absorption of composite materials reinforced with date and olive seeds. Iraqi J Mech Mater Eng. 2015;15(2):138-152.
  • [31] El-Aassar MR, Mohamed FM, Alsohaimi IH, Khalifa RE. Fabrication of novel valorized ecofriendly olive seed residue/anthracite/chitosan composite for removal of Cr(VI): Kinetics, isotherms and thermodynamics modeling. Cellulose. 2021; 28:7165-7183.
  • [32] Valvez S, Maceiras A, Santos P, Reis PNB. Olive stones as filler for polymer-based composites: a review. Materials. 2021;14(4):845.
  • [33] Pardalis N, Xanthopoulou E, Zamboulis A, Bikiaris DN. Olive stone as a filler for recycled high-density polyethylene: A promising valorization of solid wastes from olive oil industry. Sustain Chem Environ. 2024; 6:100090.
  • [34] Adibelli Ü, Mutlu D, Çakir Yiğit N, Karagöz İ. Preparation and characterization of walnut shell filled epoxy hybrid composites. 10th Int. Symp. Fibers Polym Symp. Res.; 2022. 13–14 th May,81-89.
  • [35] Özmeral N, Kocaman S, Soydal Ü, Ahmetli G. Investigation of epoxy biocomposites filled with almond shell waste. Pamukkale Univ. J Eng. Sci. 2023; 29:546–52.
  • [36] Aydın HY, Altun S. Polylactic acid matrix composites reinforced with wood-based materials. Bartin Orman Fak. Derg. 2020; 22:1061–76.
  • [37] TOS The Organic Spices. Official website. Available at: https://www.tosmagaza.com/. Accessed August 23, 2025.
  • [38] Dost Kimya. (n.d.). MGS Laminasyon Epoksi Reçine L160. Dost Kimya. Retrieved May 28, 2025, from https://dostkimya.com.tr/tr/urunler/epoksi-sistemler/mgs-laminasyon-epoksi-recine-l160.
  • [39] Saw SK, Purwar, R Nandy S, Ghose J, and Sarkhel G. Fabrication, Characterization, and Evaluation of Luffa cylindrica Fiber Reinforced Epoxy Composites. BioResources, 2013;8(4), 4805-4826.
  • [40] Rudawska A, Adhesives and adhesive joints in industry applications. IntechOpen, London, United Kingdom, 2019.
  • [41] ASTM D3039/D3039-M. Standard Test Method for Tensile Properties of Polymer Matrix Composite Material, ASTM International, West Conshohocken, 2000.
  • [42] ASTM D6110-10. Standard Test Method for Determining the Charpy Impact Resistance of Notched Specimens of Plastics, ASTM International, West Conshohocken. 2010.
  • [43] ASTM E92–17. Standard Test Methods for Vickers Hardness and Knoop Hardness of Metallic Materials ASTM International, West Conshohocken. Philadelphia. 2017.
  • [44] ASTM D 5229. Standard Test Method for Moisture Absorption Properties and Equilibrium Conditioning of Polymer Matrix Composite Materials, ASTM International, West Conshohocken, 2004.
  • [45] ASTM D 2584-02. Standard Test Method for Ignition Loss of Cured Reinforced Resins, ASTM International, West Conshohocken 2002.
  • [46] Karacor B, Özcanlı M. Investigation of use of hybrid composite materials in automobile interior. Int. J. Automot. Eng. Technol. 2020;9(4):214–28.
There are 46 citations in total.

Details

Primary Language English
Subjects Composite and Hybrid Materials
Journal Section Research Article
Authors

Bekir Ender Bağ 0009-0008-5467-8307

Berkay Karacor 0000-0001-5208-366X

Abdulkadir Yaşar 0000-0002-1548-2386

Submission Date June 11, 2025
Acceptance Date January 5, 2026
Publication Date March 27, 2026
DOI https://doi.org/10.18038/estubtda.1715002
IZ https://izlik.org/JA23EJ27PN
Published in Issue Year 2026 Volume: 27 Issue: 1

Cite

AMA 1.Bağ BE, Karacor B, Yaşar A. SUSTAINABLE COMPOSITES: INVESTIGATION OF OLIVE SEED AND BASIL LEAF POWDER MATERIALS. Estuscience - Se. 2026;27(1):39-62. doi:10.18038/estubtda.1715002