COMPARATIVE EVALUATION OF FREEZE–THAW RESISTANCE IN CONCRETE PAVEMENTS INCORPORATING SILICA FUME, CRUMB RUBBER, AND BASALT FIBER ADDITIVES

Year 2025, Volume: 26 Issue: 4, 460 - 477, 25.12.2025

Bekir Tuna Kayaalp , Rana Gizem Yaliniz

https://doi.org/10.18038/estubtda.1751392

Abstract

Concrete pavements in cold and de-icing environments are prone to progressive deterioration caused by freeze–thaw cycles, especially when exposed to moisture and salts. Ensuring freeze–thaw resistance is therefore critical for extending pavement service life and reducing maintenance costs. This study investigates the durability performance of concrete mixtures modified with silica fume, crumb rubber, and basalt fiber—three materials with distinct mechanisms for enhancing freeze–thaw behavior. Eight mix types—including two control groups with different water–cement ratios—were exposed to 56 freeze–thaw cycles in 3% NaCl solution and evaluated using surface scaling, mass loss, and ultrasonic pulse velocity (UPV) retention as complementary durability indicators. While the silica fume and crumb rubber blends demonstrated excellent surface resistance, the silica fume-only mix experienced complete internal degradation despite low mass loss, exposing the limitations of surface-based indicators alone. Basalt fiber-reinforced concretes showed a clear dosage-dependent improvement in internal integrity, with the 10BF and 15BF mixes retaining over 77% of their initial UPV. These results emphasize the necessity of multi-indicator durability assessments and suggest that hybrid modification strategies may offer robust protection against freeze–thaw damage in pavement-grade concretes.

Keywords

Concrete pavement , Freeze-thaw resistance , Basalt fiber , Silica fume , Crumb rubber

References

• [1] Zhang P, Wang X, Wang J, et al. Workability and Durability of Concrete Incorporating Waste Tire Rubber: A Review. JRM 2022;11:745–76.
• [2] Yılmazoğlu A, Yıldırım S. A review on mechanical and durability properties of concrete with waste rubber aggregate. Pamukkale Üniversitesi Mühendislik Bilimleri Dergisi 2023; 29, 513–28.
• [3] Bulut HA, Kandil U. Investigation of freeze-thaw performance for sustainable rubberized concrete composites with different water to cement ratios. Materiales de Construcción 2025; 75, 364–364.
• [4] Liu H, Wang X, Jiao Y, Sha T. Experimental Investigation of the Mechanical and Durability Properties of Crumb Rubber Concrete. Materials. 2016; 9(3):172.
• [5] Usman M, Gillani SAA, Hameed R, et al. Effect of crumb rubber and silica fume on the fresh, hardened and concrete-steel bond strength properties of SCC. 1 2022; 14, 427–40.
• [6] Zhou T, Mirzadeh M, Pellenq RJM, Bazant MZ. Freezing point depression and freeze–thaw damage by nanofluidic salt trapping. Phys Rev Fluids., 2020; 5 (12), 124201.
• [7] Rønning TF. Freeze-Thaw Resistance of Concrete: Effect of: Curing Conditions, Moisture Exchange and Materials. Ph.D. Thesis. The Norwegian Institute of Technology, 2001.
• [8] Karakurt C, Bayazıt Y. Freeze–thaw resistance of normal and high-strength concretes produced with fly ash and silica fume. Adv Mater Sci Eng., 2015; 2015, 830984.
• [9] Use of Crumb Rubber to Achieve Freeze/Thaw Resisting Concrete Challenges of Concrete Construction: Volume 6, Concrete for Extreme Conditions, Proceedings of the International Conference held at the University of Dundee, Scotland, UK on 9–11 September
• [10] Xiao L, Li J, Liu Q. Experimental study on the effect of short basalt fiber on properties of lightweight aggregate concrete. 2016 2nd International Conference on Architectural, Civil and Hydraulics Engineering (ICACHE 2016), Atlantis Press; 2016, p. 183–7.
• [11] Zeng H, Zhang J, Li Y, et al. Mechanical Properties and Microstructure of Basalt Fiber Reinforced Concrete Under the Single-Side Salt-Freezing–Drying–Wetting Cycles. International Journal of Concrete Structures and Materials 2022; 16-44.
• [12] Guo Y, Gao J, Lv J. Experimental Study on the Frost Resistance of Basalt Fiber Reinforced Concrete. Materials (Basel) 2024; 17, p 4593.
• [13] Liu M, Dai W, Zhong C, et al. Study on Mechanical Properties and Microstructure of Basalt Fiber Reactive Powder Concrete. Buildings 2022;12, p 1734.
• [14] Li W, Liu H, Zhu B, et al. Mechanical Properties and Freeze–Thaw Durability of Basalt Fiber Reactive Powder Concrete. Applied Sciences 2020; 10, p 5682.
• [15] Liang W, Wang S, Lv X, et al. Dynamic Mechanical Properties and Damage Constitutive Model of Frozen–Thawed Basalt Fiber-Reinforced Concrete Under Wide Strain Rate Range. Materials 2025;18, p 3337.
• [16] Yu J, Yi Z, Zhang Z, et al. The Effects of Hybrid Steel/Basalt Fibers on the Durability of Concrete Pavement against Freeze–Thaw Cycles. Materials (Basel) 2023; 16, p 7137.
• [17] Smarzewski P, Jancy A. Comparative study on mechanical performance and toughness of high-performance self-compacting concrete with polypropylene and basalt fibres. Materials, 2025; 18 (16), 3833.
• [18] Uzun M, Arslan MA. Effect of basalt fiber aspect ratio on mechanical and workability properties of self-compacting concrete. Konya J Eng Sci., 2024; 12 (1), 14–21.
• [19] Al-Rousan ET, Khalid HR, Rahman MK. Fresh, mechanical, and durability properties of basalt fiber-reinforced concrete (BFRC): a review. Dev Built Environ., 2023; 14, p 100155.
• [20] Wu H, Qin X, Huang X, Kaewunruen S. Engineering, mechanical and dynamic properties of basalt fiber reinforced concrete. Materials, 2023; 16 (2), 623.