Yıl 2019, Cilt 31 , Sayı 3, Sayfalar 255 - 260 2019-09-01

Zn0.96Cu0.01Ni0.03O nanoparçacıkların yapısal ve manyetik özellikleri
Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles

Adi̇l Güler [1]


Zn0.96Cu0.01Ni0.03O nanoparçacıkları, sol-gel tekniği ile hazırlanıp geniş sıcaklık aralığında (450, 500, 550, 600, 700, 800, 900 ° C) tavlandı. Olası yapısal fazları belirlemek için X-ışını kırınım tekniği (XRD) kullanılmıştır. Kafes parametreleri Rietveld analizi ile hesaplanmış ve tavlama sıcaklıkları ile ilişkilendirilmiştir. Sentezlenen nanoparçacıklar için, optimum tavlama sıcaklıkları 450, 500 ve 550 ° C'de elde edildi ve ayrıca tavlama sıcaklığı artışı ikincil NiO fazlarına yol açmıştır. Taramalı Elektron Mikroskobu (SEM) görüntüleri rastgele küre şeklindeki parçacık dağılımını göstermektedir. Enerji dağıtıcı X-ışını spektroskopisi (EDX) sadece kompozisyona ait pikleri göstermektedir. Zn0.96Cu0.01Ni0.03O nanoparçacıkları için manyetik ölçümler, Kuantum Dizayn Titreşen Örnek Manyetometresi (QDVSM) kullanılarak yapıldı. DC manyetik alana bağlı mıknatıslanma eğrilerinden, tüm Cu-Ni ortak katkılı ZnO nanoparçacıklarının net paramanyetik davranışı gösterildi.

Zn0.96Cu0.01Ni0.03O nanoparticles were prepared by sol-gel technique and annealed under wide temperature range (450, 500, 550, 600, 700, 800, and 900 0C). To figure out the possible structural phases X-ray diffraction technique (XRD) was used. The lattice parameters were calculated by Rietveld analysis and correlated by annealing temperatures. For the synthesized nanoparticles, the optimum annealing temperatures were achieved at 450, 500, and 550 °C and further annealing temperature increment gave rise to secondary NiO peaks. The Scanning Electron Microscope (SEM) images show random ball-shaped particle distribution. Energy dispersive X-ray spectroscopy (EDX) showed only the peaks belong to the composition. Magnetic measurements were performed using Quantum Design Vibrating Sample Magnetometer (QDVSM) tool for Zn0.96Cu0.01Ni0.03O nanosystems. From the DC magnetic field dependent magnetization curves, clear paramagnetic behavior was revealed for all Cu-Ni co-doped ZnO nanoparticles.

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Birincil Dil en
Konular Temel Bilimler
Bölüm Araştırma Makaleleri
Yazarlar

Orcid: 0000-0002-5345-8731
Yazar: Adi̇l Güler (Sorumlu Yazar)
Kurum: Marmara University
Ülke: Turkey


Tarihler

Yayımlanma Tarihi : 1 Eylül 2019

Bibtex @araştırma makalesi { jeps560040, journal = {International Journal of Advances in Engineering and Pure Sciences}, issn = {}, eissn = {2636-8277}, address = {fbedergi@marmara.edu.tr}, publisher = {Marmara Üniversitesi}, year = {2019}, volume = {31}, pages = {255 - 260}, doi = {10.7240/jeps.560040}, title = {Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles}, key = {cite}, author = {Güler, Adi̇l} }
APA Güler, A . (2019). Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles. International Journal of Advances in Engineering and Pure Sciences , 31 (3) , 255-260 . DOI: 10.7240/jeps.560040
MLA Güler, A . "Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles". International Journal of Advances in Engineering and Pure Sciences 31 (2019 ): 255-260 <https://dergipark.org.tr/tr/pub/jeps/issue/48917/560040>
Chicago Güler, A . "Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles". International Journal of Advances in Engineering and Pure Sciences 31 (2019 ): 255-260
RIS TY - JOUR T1 - Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles AU - Adi̇l Güler Y1 - 2019 PY - 2019 N1 - doi: 10.7240/jeps.560040 DO - 10.7240/jeps.560040 T2 - International Journal of Advances in Engineering and Pure Sciences JF - Journal JO - JOR SP - 255 EP - 260 VL - 31 IS - 3 SN - -2636-8277 M3 - doi: 10.7240/jeps.560040 UR - https://doi.org/10.7240/jeps.560040 Y2 - 2019 ER -
EndNote %0 International Journal of Advances in Engineering and Pure Sciences Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles %A Adi̇l Güler %T Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles %D 2019 %J International Journal of Advances in Engineering and Pure Sciences %P -2636-8277 %V 31 %N 3 %R doi: 10.7240/jeps.560040 %U 10.7240/jeps.560040
ISNAD Güler, Adi̇l . "Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles". International Journal of Advances in Engineering and Pure Sciences 31 / 3 (Eylül 2019): 255-260 . https://doi.org/10.7240/jeps.560040
AMA Güler A . Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles. JEPS. 2019; 31(3): 255-260.
Vancouver Güler A . Structure and magnetic properties Zn0.96Cu0.01Ni0.03O nanoparticles. International Journal of Advances in Engineering and Pure Sciences. 2019; 31(3): 260-255.