Thermally Stable Rice Husk Microcrystalline Cellulose as Adsorbent in PTLC Plates
Yıl 2018,
Cilt: 5 Sayı: 3, 1177 - 1184, 01.09.2018
Mariam Arowona
,
Gabriel Ademola Olatuji
Oluwakemi Rachel Adeniyi
Oluwaseyi David Saliu
,
Olubunmi Atolani
Jamiu Adisa
Öz
Microcrystalline
cellulose (MCC) was prepared from rice husk by subjecting it to alkaline
pretreatment, delignification, bleaching and hydrolytic operations. MCC was
also prepared from cotton wool and used as a reference because of its high
cellulose content to estimate a relative yield and quality of the MCC produced
from rice husk. The characteristic morphological feature was established by
scanning electron micrograph (SEM); the functional group was confirmed by the
Fourier transform infrared (FTIR) spectroscopic method and the thermal
stability was determined from thermogravimetric analysis (TGA) and this
characterized MCC of rice husk was applied as a stationary phase in Preparative Thin Layer Chromatography (PTLC).
Kaynakça
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- Liu C.F.S., Run Cang Zhang, Ai Ping Qin, Men Hua Ren, Jun Li Wang and Xin Ai,. Preparation and characterization of phthalated cellulose derivatives in room-temperature ionic liquid without catalysts. Journal of Agricultural and Food Chemistry, 2006, 55, 2399.
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- Sun, Y. and Cheng J. Hydrolysis of lignocellulosic materials for ethanol production: A review. Bioresource Technology, 2002, 83(1): 1-11.
- Sun, R. C., Sun, X. F., & Tomkinson, J., Hemicelluloses and their derivatives. ACS Symposium Series, 2004a, 864, 2–22.
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Yıl 2018,
Cilt: 5 Sayı: 3, 1177 - 1184, 01.09.2018
Mariam Arowona
,
Gabriel Ademola Olatuji
Oluwakemi Rachel Adeniyi
Oluwaseyi David Saliu
,
Olubunmi Atolani
Jamiu Adisa
Kaynakça
- Ejikeme, P. M. Investigation of the physicochemical properties of microcrystalline cellulose from agricultural wastes I:Orange mesocarp. Cellulose, 2008, 15, 141–147.
- Laka, M., and Chernyavskaya, S., Obtaining microcrystalline cellulose from softwood and hardwood pulp. Bioresources, 2007, 2(3), 583–589.
- Liu C.F.S., Run Cang Zhang, Ai Ping Qin, Men Hua Ren, Jun Li Wang and Xin Ai,. Preparation and characterization of phthalated cellulose derivatives in room-temperature ionic liquid without catalysts. Journal of Agricultural and Food Chemistry, 2006, 55, 2399.
- Liu, C. F., Sun, R. C., Zhang, A.P.,and Ren, J. L., Preparation of sugarcane bagasse cellulosic phthalate using ionic liquid as reaction medium. Elsevier Ltd. ,2007, 2006.07.002.
- Sánchez, O. J., and Cardona, C. A. , Trends in biotechnological production of fuel ethanol from different feed stocks. Bioresource Technology. 2008, 99, 5270-5295.
- Sun, Y. and Cheng J. Hydrolysis of lignocellulosic materials for ethanol production: A review. Bioresource Technology, 2002, 83(1): 1-11.
- Sun, R. C., Sun, X. F., & Tomkinson, J., Hemicelluloses and their derivatives. ACS Symposium Series, 2004a, 864, 2–22.
- Sun, J. X., Sun, X. F., Zhao, H., & Sun, R. C. , Isolation and characterization of cellulose from sugarcane bagasse. Polymer Degradation and Stability, 2004b, 84, 331–339.