BİYOKÜTLEDEN GÖZENEKLİ KARBONLU MALZEME ÜRETİMİ: BİYOKÜTLE TİPİ VE SICAKLIĞIN FİZİKOKİMYASAL ÖZELLİKLERE ETKİSİ

Yıl 2023, Cilt: 11 Sayı: 1, 261 - 273, 01.03.2023

Aynur Aşma Elif Yaman Sinan Temel

https://doi.org/10.36306/konjes.1205637

Öz

Bu çalışmada, yenilenebilir bir kaynak olan 2 farklı biyokütlenin (karaçam ağacı talaşı ve meşe ağacı talaşı) detaylı karakterizasyonu, bu biyokütlelerden farklı sıcaklıklarda (400, 500 ve 700 °C) karbonizasyon yöntemi ile karbonlu malzeme üretilmesi ve üretilen bu malzemelerin karakterizasyonu gerçekleştirilmiştir. Çalışmanın amacı, biyokütle tipinin ve karbonizasyon sıcaklığının elde edilen karbonlu malzemenin fizikokimyasal özellikleri üzerine etkisinin belirlenmesidir. Bu sebeple biyokütle örnekleri seçilirken, birinin sert odun (hard wood) diğerinin yumuşak odun (soft wood) olmasına dikkat edilmiştir. Biyokütle ve elde edilen örneklerin ön analizleri gerçekleştirilmiştir. Elementel analiz, Fourier dönüşümlü kızılötesi spektrometresi (FT-IR) ve Taramalı elektron mikroskobu (SEM) teknikleri kullanılarak karakterizasyon çalışmaları tamamlanmıştır. Elde edilen sonuçlara göre, karbonizasyon sonucu elde edilen karbonlu malzemenin fizikokimyasal özelliklerinin hammadde tipi ve reaksiyon koşullarına bağlı olduğu belirlenmiştir.

Anahtar Kelimeler

Biyokütle, karbonizasyon, karakterizasyon

Production of Porous Carbon Materials From Biomass: The Effect of Biomass Type and Temperature on Physiochemical Properties

Öz

In this study, detailed characterization of two different biomass samples (black pine wood sawdust and oak wood sawdust) which is a renewable resource, carbonization of these biomass at different temperatures (400, 500 and 700 °C) and the characterization of produced carbonaceous materials were carried out. The aim of the study is to specify the effect of biomass type and carbonization temperature on the physicochemical properties of the carbonaceous materials obtained. For this reason, while selecting biomass samples, importance was attached to ensure that one of them is hard wood and the other is soft wood. Pre-liminary analyses of biomass and obtained carbonaceous samples were executed. Characterization studies were completed using elemental analysis, Fourier transform infrared spectroscopy (FT-IR) and Scanning electron microscopy (SEM) techniques. According to the results, it was determined that the physicochemical properties of the carbonaceous material obtained as a result of carbonization depend on the raw material type and reaction conditions.

Anahtar Kelimeler

Biomass, Carbonization, Characterization

Kaynakça

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