Torna talaşı atıklarından demir oksit esaslı aerojel tozu üretimi ve karakterizasyonu

Öz

Mevcut çalışmada metal oksit aerojeller grubunun bir üyesi konumunda olan demir oksit aerojellerin torna talaşı atıklarından üretilebilirliği incelenmiştir. Bu amaçla halkalı değirmende öğütülerek ince taneli boyuta getirilmiş torna talaş atıkları, asitte çözdürülüp baz ile nötralize edilmiş ve jelleşmeye bırakılmıştır. Jelleşme süreci sonunda jel kaynar saf ile yıkanarak demir oksit esaslı aerojel tozu elde edilmiştir. Elde edilen demir oksit aerojel tozunun XRD ile faz analizi, SEM ve EDS görüntüleri ile mikroyapı analizi, Zeta potansiyeli ile ortalama tane boyut ve potansiyel aralıkları ve FTIR ile bağ yapıları karakterize edilmiştir.

Anahtar Kelimeler

• Demir Oksit Aerojel
• Metal oksit aerojel
• Torna Talaşı Atığı
• Sol-jel

Production and characterization of iron oxide based aerogel from steel sawdust waste

Öz

In the present study, the producibility of iron oxide aerogels, which is a member of the metal oxide aerogels group, from lathe waste was investigated. For this purpose, lathe sawdust wastes, which were ground in a ring mill and made fine-grained, were dissolved in acid, neutralized with base and left to gel. At the end of the gelation process, iron oxide aerogel powder was obtained by washing the gel with boiling distilled water. The iron oxide aerogel powder was analyzed for phase, microstructure, average grain size, potential ranges, and bond structures using XRD, SEM and EDS images, Zeta potential, and FTIR, respectively.

Anahtar Kelimeler

• Iron Oxide aerogel
• Metal Oxide Aerogel
• Steel Sawdust Waste
• Sol-gel

Kaynakça

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