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Yıl 2017, Cilt 41, Sayı 6, 536 - 544, 01.12.2017

Öz

Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies

Yıl 2017, Cilt 41, Sayı 6, 536 - 544, 01.12.2017

Öz

Microstructural features and surface morphologies of Ni-Fe thin films fabricated by the electrochemical deposition technique have been experimentally studied. Ni-Fe thin films have been deposited under different deposition potentials and FeSO$_{4}$ concentrations. Energy dispersive X-ray measurements demonstrate that the Fe content decreases (increases) as the deposition potential (FeSO$_{4}$ concentration) is enhanced. All of the produced films exhibit an anomalous codeposition behavior. The effects of deposition potential and FeSO$_{4}$ concentrations on the degree of anomalous codeposition have been also characterized. X-ray diffraction studies reveal that the films have face-centered cubic crystallographic structures with [111] preferred crystallographic orientation regardless of the applied deposition conditions. However, the crystallization and the crystallite size of the films are affected by changing of the FeSO$_{4}$ concentration and the deposition potential. The results of scanning electron microscopy analyses verify that the surface structure of the film electroplated from the electrolyte with higher FeSO$_{4}$ concentration under higher deposition potential exhibits a more homogeneous and dense structure with smaller grain sizes.

Ayrıntılar

Bölüm Makaleler
Yazarlar

Umut SARAÇ Bu kişi benim


Malik KAYA Bu kişi benim


Mevlana Celalettin BAYKUL Bu kişi benim

Yayımlanma Tarihi 1 Aralık 2017
Yayınlandığı Sayı Yıl 2017, Cilt 41, Sayı 6

Kaynak Göster

Bibtex @ { tbtkphysics401967, journal = {Turkish Journal of Physics}, issn = {1300-0101}, eissn = {1303-6122}, address = {}, publisher = {TÜBİTAK}, year = {2017}, volume = {41}, number = {6}, pages = {536 - 544}, title = {Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies}, key = {cite}, author = {Saraç, Umut and Kaya, Malik and Baykul, Mevlana Celalettin} }
APA Saraç, U. , Kaya, M. & Baykul, M. C. (2017). Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies . Turkish Journal of Physics , 41 (6) , 536-544 . Retrieved from https://dergipark.org.tr/tr/pub/tbtkphysics/issue/35854/401967
MLA Saraç, U. , Kaya, M. , Baykul, M. C. "Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies" . Turkish Journal of Physics 41 (2017 ): 536-544 <https://dergipark.org.tr/tr/pub/tbtkphysics/issue/35854/401967>
Chicago Saraç, U. , Kaya, M. , Baykul, M. C. "Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies". Turkish Journal of Physics 41 (2017 ): 536-544
RIS TY - JOUR T1 - Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies AU - UmutSaraç, MalikKaya, Mevlana CelalettinBaykul Y1 - 2017 PY - 2017 N1 - DO - T2 - Turkish Journal of Physics JF - Journal JO - JOR SP - 536 EP - 544 VL - 41 IS - 6 SN - 1300-0101-1303-6122 M3 - UR - Y2 - 2022 ER -
EndNote %0 Turkish Journal of Physics Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies %A Umut Saraç , Malik Kaya , Mevlana Celalettin Baykul %T Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies %D 2017 %J Turkish Journal of Physics %P 1300-0101-1303-6122 %V 41 %N 6 %R %U
ISNAD Saraç, Umut , Kaya, Malik , Baykul, Mevlana Celalettin . "Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies". Turkish Journal of Physics 41 / 6 (Aralık 2017): 536-544 .
AMA Saraç U. , Kaya M. , Baykul M. C. Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies. Turkish Journal of Physics. 2017; 41(6): 536-544.
Vancouver Saraç U. , Kaya M. , Baykul M. C. Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies. Turkish Journal of Physics. 2017; 41(6): 536-544.
IEEE U. Saraç , M. Kaya ve M. C. Baykul , "Synthesis of Ni-Fe thin films by electrochemical deposition technique and characterization of their microstructures and surface morphologies", Turkish Journal of Physics, c. 41, sayı. 6, ss. 536-544, Ara. 2017