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Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering

Yıl 2024, Cilt: 36 Sayı: 1, 33 - 38, 25.03.2024
https://doi.org/10.7240/jeps.1396072

Öz

Although the spark plasma sintering (SPS) method is a very advantageous technque in many aspects, the inability to clearly read the temperature formed on the material during sintering and heterogeneous temperature distributions are the biggest problems of this process. Therefore, it is a common situation that samples taken from different regions of the produced material have different densities and mechanical properties. In this study, the temperature distributions, current density and joule heating effect of the entire setup consisting of the alumina (Al2O3) sample to be sintered, inconel electrodes, graphite dies, punches and spacers, as well as the critical regions in this setup, are modeled by using finite element software. According to the results, the temperature is maximum at the centre of the Al2O3 sample and the temperature gradient along its radius is 22.4°C. The temperature difference between the inner wall of the hole which is opened in the graphite mold to measure the sintering temperature and the centre of the Al2O3 sample is around 40°C. In addition, during the SPS process, Al2O3 is not heated directly by the joule effect and the temperature gradient in the sample occurs due to mold surface radiation.

Kaynakça

  • [1] Laszkiewicz-Łukasik, J., Putyra, P., Klimczyk, P., Podsiadło, M., Bednarczyk, K., (2021). Spark Plasma Sintering/Field Assisted Sintering Technique as a Universal Method for the Synthesis, Densification and Bonding Processes for Metal, Ceramic and Composite Materials. Journal of Applied Materials Engineering. 60(2): 53–69.
  • [2] Cavaliere, P., Sadeghi, B., Shabani, A., (2019). Spark Plasma Sintering: Process Fundamentals. Spark Plasma Sintering of Materials, Cham: Springer International Publishing p. 3–20.
  • [3] Anselmi-Tamburini, U., (2021). Spark Plasma Sintering. Encyclopedia of Materials: Technical Ceramics and Glasses, Elsevier p. 294–310.
  • [4] Bubesh Kumar, D., Selva babu, B., Aravind Jerrin, K.M., Joseph, N., Jiss, A., (2020). Review of Spark Plasma Sintering Process. IOP Conference Series: Materials Science and Engineering. 993(1): 012004.
  • [5] Gok, M.G., (2021). Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites. European Mechanical Science. 5(2): 64–70.
  • [6] Razavi, M., Farajipour, A.R., Zakeri, M., Rahimipour, M.R., Firouzbakht, A.R., (2017). Production of Al2O3–SiC nano-composites by spark plasma sintering. Boletín de La Sociedad Española de Cerámica y Vidrio. 56(4): 186–94.
  • [7] Álvarez, I., Torrecillas, R., Solis, W., Peretyagin, P., Fernández, A., (2016). Microstructural design of Al2O3–SiC nanocomposites by Spark Plasma Sintering. Ceramics International. 42(15): 17248–53.
  • [8] Cetinbag, A., Ormanci, O., Goller, G., (2022). Production of B4C reinforced TZM alloy and boriding its surface in one step by spark plasma sintering (SPS). International Journal of Refractory Metals and Hard Materials. 106: 105860.
  • [9] Danisman, C.B., Goller, G., (2023). Spark plama sintered mn-al (magnets) production and characterization with experimental design. Archives of Metallurgy and Materials. 68(4): 13571367.
  • [10] Kaplan Akarsu, M., Akin, I., Sahin, F., Goller, G., (2022). Comparative study of reactive and nonreactive spark plasma sintering routes for the production of TaB2‐TaC composites. International Journal of Applied Ceramic Technology. 19(1): 332–43.
  • [11] Saheb, N., Iqbal, Z., Khalil, A., Hakeem, A.S., Al Aqeeli, N., Laoui, T., et al., (2012). Spark Plasma Sintering of Metals and Metal Matrix Nanocomposites: A Review. Journal of Nanomaterials. 2012: 1–13.
  • [12] Akin, I., (2010). ZrB2 esaslı kompozitlerin spark plazma sinterleme (SPS) yöntemi ile üretimi ve karakterizasyonu / Production and characterization of ZrB2 based composites prepared by spark plasma sintering. Istanbul Technical University, (2010).
  • [13] Çınar Şahin, F., Mansoor, M., Cengiz, M., Apak, B., Yanmaz, L., Balazsi, K., et al., (2022). B4C Composites with a TiB2-C Core–Shell Microstructure Produced by Self-Propagating High-Temperature Synthesis-Assisted Spark Plasma Sintering. The Journal of Physical Chemistry C. 126(47): 20114–26.
  • [14] Pavia, A., Durand, L., Ajustron, F., Bley, V., Chevallier, G., Peigney, A., et al., (2013). Electro-thermal measurements and finite element method simulations of a spark plasma sintering device. Journal of Materials Processing Technology. 213(8): 1327–36.
  • [15] Sakkaki, M., Sadegh Moghanlou, F., Vajdi, M., Shahedi Asl, M., Mohammadi, M., Shokouhimehr, M., (2020). Numerical simulation of heat transfer during spark plasma sintering of zirconium diboride. Ceramics International. 46(4): 4998–5007.
  • [16] Manière, C., Pavia, A., Durand, L., Chevallier, G., Afanga, K., Estournès, C., (2016). Finite-element modeling of the electro-thermal contacts in the spark plasma sintering process. Journal of the European Ceramic Society. 36(3): 741–8.
  • [17] Molénat, G., Durand, L., Galy, J., Couret, A., (2010). Temperature Control in Spark Plasma Sintering: An FEM Approach. Journal of Metallurgy. 2010: 1–9.
  • [18] Vanmeensel, K., Laptev, A., Hennicke, J., Vleugels, J., Vanderbiest, O., (2005). Modelling of the temperature distribution during field assisted sintering. Acta Materialia. 53(16): 4379–88.

Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering

Yıl 2024, Cilt: 36 Sayı: 1, 33 - 38, 25.03.2024
https://doi.org/10.7240/jeps.1396072

Öz

Although the spark plasma sintering (SPS) method is a very advantageous technque in many aspects, the inability to clearly read the temperature formed on the material during sintering and heterogeneous temperature distributions are the biggest problems of this process. Therefore, it is a common situation that samples taken from different regions of the produced material have different densities and mechanical properties. In this study, the temperature distributions, current density and joule heating effect of the entire setup consisting of the alumina (Al2O3) sample to be sintered, inconel electrodes, graphite dies, punches and spacers, as well as the critical regions in this setup, are modeled by using finite element software. According to the results, the temperature is maximum at the centre of the Al2O3 sample and the temperature gradient along its radius is 22.4°C. The temperature difference between the inner wall of the hole which is opened in the graphite mold to measure the sintering temperature and the centre of the Al2O3 sample is around 40°C. In addition, during the SPS process, Al2O3 is not heated directly by the joule effect and the temperature gradient in the sample occurs due to mold surface radiation.

Kaynakça

  • [1] Laszkiewicz-Łukasik, J., Putyra, P., Klimczyk, P., Podsiadło, M., Bednarczyk, K., (2021). Spark Plasma Sintering/Field Assisted Sintering Technique as a Universal Method for the Synthesis, Densification and Bonding Processes for Metal, Ceramic and Composite Materials. Journal of Applied Materials Engineering. 60(2): 53–69.
  • [2] Cavaliere, P., Sadeghi, B., Shabani, A., (2019). Spark Plasma Sintering: Process Fundamentals. Spark Plasma Sintering of Materials, Cham: Springer International Publishing p. 3–20.
  • [3] Anselmi-Tamburini, U., (2021). Spark Plasma Sintering. Encyclopedia of Materials: Technical Ceramics and Glasses, Elsevier p. 294–310.
  • [4] Bubesh Kumar, D., Selva babu, B., Aravind Jerrin, K.M., Joseph, N., Jiss, A., (2020). Review of Spark Plasma Sintering Process. IOP Conference Series: Materials Science and Engineering. 993(1): 012004.
  • [5] Gok, M.G., (2021). Spark Plasma Sintering of Nano Silicon Carbide Reinforced Alumina Ceramic Composites. European Mechanical Science. 5(2): 64–70.
  • [6] Razavi, M., Farajipour, A.R., Zakeri, M., Rahimipour, M.R., Firouzbakht, A.R., (2017). Production of Al2O3–SiC nano-composites by spark plasma sintering. Boletín de La Sociedad Española de Cerámica y Vidrio. 56(4): 186–94.
  • [7] Álvarez, I., Torrecillas, R., Solis, W., Peretyagin, P., Fernández, A., (2016). Microstructural design of Al2O3–SiC nanocomposites by Spark Plasma Sintering. Ceramics International. 42(15): 17248–53.
  • [8] Cetinbag, A., Ormanci, O., Goller, G., (2022). Production of B4C reinforced TZM alloy and boriding its surface in one step by spark plasma sintering (SPS). International Journal of Refractory Metals and Hard Materials. 106: 105860.
  • [9] Danisman, C.B., Goller, G., (2023). Spark plama sintered mn-al (magnets) production and characterization with experimental design. Archives of Metallurgy and Materials. 68(4): 13571367.
  • [10] Kaplan Akarsu, M., Akin, I., Sahin, F., Goller, G., (2022). Comparative study of reactive and nonreactive spark plasma sintering routes for the production of TaB2‐TaC composites. International Journal of Applied Ceramic Technology. 19(1): 332–43.
  • [11] Saheb, N., Iqbal, Z., Khalil, A., Hakeem, A.S., Al Aqeeli, N., Laoui, T., et al., (2012). Spark Plasma Sintering of Metals and Metal Matrix Nanocomposites: A Review. Journal of Nanomaterials. 2012: 1–13.
  • [12] Akin, I., (2010). ZrB2 esaslı kompozitlerin spark plazma sinterleme (SPS) yöntemi ile üretimi ve karakterizasyonu / Production and characterization of ZrB2 based composites prepared by spark plasma sintering. Istanbul Technical University, (2010).
  • [13] Çınar Şahin, F., Mansoor, M., Cengiz, M., Apak, B., Yanmaz, L., Balazsi, K., et al., (2022). B4C Composites with a TiB2-C Core–Shell Microstructure Produced by Self-Propagating High-Temperature Synthesis-Assisted Spark Plasma Sintering. The Journal of Physical Chemistry C. 126(47): 20114–26.
  • [14] Pavia, A., Durand, L., Ajustron, F., Bley, V., Chevallier, G., Peigney, A., et al., (2013). Electro-thermal measurements and finite element method simulations of a spark plasma sintering device. Journal of Materials Processing Technology. 213(8): 1327–36.
  • [15] Sakkaki, M., Sadegh Moghanlou, F., Vajdi, M., Shahedi Asl, M., Mohammadi, M., Shokouhimehr, M., (2020). Numerical simulation of heat transfer during spark plasma sintering of zirconium diboride. Ceramics International. 46(4): 4998–5007.
  • [16] Manière, C., Pavia, A., Durand, L., Chevallier, G., Afanga, K., Estournès, C., (2016). Finite-element modeling of the electro-thermal contacts in the spark plasma sintering process. Journal of the European Ceramic Society. 36(3): 741–8.
  • [17] Molénat, G., Durand, L., Galy, J., Couret, A., (2010). Temperature Control in Spark Plasma Sintering: An FEM Approach. Journal of Metallurgy. 2010: 1–9.
  • [18] Vanmeensel, K., Laptev, A., Hennicke, J., Vleugels, J., Vanderbiest, O., (2005). Modelling of the temperature distribution during field assisted sintering. Acta Materialia. 53(16): 4379–88.
Toplam 18 adet kaynakça vardır.

Ayrıntılar

Birincil Dil İngilizce
Konular Malzeme Üretim Teknolojileri, Toz Metalurjisi
Bölüm Araştırma Makaleleri
Yazarlar

Mustafa Güven Gök 0000-0002-5959-0549

Erken Görünüm Tarihi 18 Mart 2024
Yayımlanma Tarihi 25 Mart 2024
Gönderilme Tarihi 25 Kasım 2023
Kabul Tarihi 7 Şubat 2024
Yayımlandığı Sayı Yıl 2024 Cilt: 36 Sayı: 1

Kaynak Göster

APA Gök, M. G. (2024). Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering. International Journal of Advances in Engineering and Pure Sciences, 36(1), 33-38. https://doi.org/10.7240/jeps.1396072
AMA Gök MG. Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering. JEPS. Mart 2024;36(1):33-38. doi:10.7240/jeps.1396072
Chicago Gök, Mustafa Güven. “Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering”. International Journal of Advances in Engineering and Pure Sciences 36, sy. 1 (Mart 2024): 33-38. https://doi.org/10.7240/jeps.1396072.
EndNote Gök MG (01 Mart 2024) Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering. International Journal of Advances in Engineering and Pure Sciences 36 1 33–38.
IEEE M. G. Gök, “Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering”, JEPS, c. 36, sy. 1, ss. 33–38, 2024, doi: 10.7240/jeps.1396072.
ISNAD Gök, Mustafa Güven. “Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering”. International Journal of Advances in Engineering and Pure Sciences 36/1 (Mart 2024), 33-38. https://doi.org/10.7240/jeps.1396072.
JAMA Gök MG. Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering. JEPS. 2024;36:33–38.
MLA Gök, Mustafa Güven. “Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering”. International Journal of Advances in Engineering and Pure Sciences, c. 36, sy. 1, 2024, ss. 33-38, doi:10.7240/jeps.1396072.
Vancouver Gök MG. Electrothermal Simulation of the Production of Alumina by Spark Plasma Sintering. JEPS. 2024;36(1):33-8.