Year 2017, Volume 18, Issue 5, Pages 1107 - 1117 2017-12-18

COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe)

Emine Sert [1] , Esra Yılmaz [2] , Ferhan Sami Atalay [3]

203 757

Iron based MIL-53 (Fe) was synthesized by solvothermal and ionothermal methods. Then the synthesized materials were sulfated to increase the acidic property. Characterization of synthesized and sulfated materials were performed by FT-IR, BET, XRD and TGA methods. The sulfated materials were used in esterification reaction of acetic acid to test the catalytic activity. The effect of synthesis method on the structure of MIL-53 (Fe) and also effects of temperature, time and sulfation of samples on the conversion of acetic acid were studied. Also reusability of sulfated samples was achieved by washing with pure water. In ionothermal synthesis of iron based metal organic framework, deep eutectic solvent formed by choline chloride and dimethyl urea was used as solvent.

MOF, MIL-53(Fe), ionothermal, solvothermal
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Subjects Engineering
Journal Section Articles
Authors

Author: Emine Sert
Country: Turkey


Author: Esra Yılmaz
Country: Turkey


Author: Ferhan Sami Atalay

Dates

Publication Date: December 18, 2017

Bibtex @research article { aubtda328791, journal = {ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering}, issn = {1302-3160}, eissn = {2146-0205}, address = {Eskişehir Teknik Üniversitesi}, year = {2017}, volume = {18}, pages = {1107 - 1117}, doi = {10.18038/aubtda.328791}, title = {COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe)}, key = {cite}, author = {Sert, Emine and Yılmaz, Esra and Atalay, Ferhan Sami} }
APA Sert, E , Yılmaz, E , Atalay, F . (2017). COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe). ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering, 18 (5), 1107-1117. DOI: 10.18038/aubtda.328791
MLA Sert, E , Yılmaz, E , Atalay, F . "COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe)". ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering 18 (2017): 1107-1117 <http://dergipark.org.tr/aubtda/issue/31308/328791>
Chicago Sert, E , Yılmaz, E , Atalay, F . "COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe)". ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering 18 (2017): 1107-1117
RIS TY - JOUR T1 - COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe) AU - Emine Sert , Esra Yılmaz , Ferhan Sami Atalay Y1 - 2017 PY - 2017 N1 - doi: 10.18038/aubtda.328791 DO - 10.18038/aubtda.328791 T2 - ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering JF - Journal JO - JOR SP - 1107 EP - 1117 VL - 18 IS - 5 SN - 1302-3160-2146-0205 M3 - doi: 10.18038/aubtda.328791 UR - https://doi.org/10.18038/aubtda.328791 Y2 - 2017 ER -
EndNote %0 ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe) %A Emine Sert , Esra Yılmaz , Ferhan Sami Atalay %T COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe) %D 2017 %J ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering %P 1302-3160-2146-0205 %V 18 %N 5 %R doi: 10.18038/aubtda.328791 %U 10.18038/aubtda.328791
ISNAD Sert, Emine , Yılmaz, Esra , Atalay, Ferhan Sami . "COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe)". ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering 18 / 5 (December 2017): 1107-1117. https://doi.org/10.18038/aubtda.328791
AMA Sert E , Yılmaz E , Atalay F . COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe). AUJST-A. 2017; 18(5): 1107-1117.
Vancouver Sert E , Yılmaz E , Atalay F . COMPARISON OF SOLVOTHERMAL AND IONOTHERMAL METHODS ON CATALYTIC ACTIVITY OF MIL-53 (Fe). ANADOLU UNIVERSITY JOURNAL OF SCIENCE AND TECHNOLOGY A - Applied Sciences and Engineering. 2017; 18(5): 1117-1107.