The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate

Volume: 11 Number: 3 December 23, 2015
EN

The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate

Abstract

MSU-x (MSU represents Michigan State University) materials are a family of ordered mesoporous silica obtained by using nonionic poly(ethylene oxide)-based surfactants [1]. MSU materials have many application areas due to their mesoporous structure, high mass oil cracking activity and high thermal stability [2]. In recent years MSU mesoporous materials were used in adsorption, catalytic applications, separation process, and drug delivery system [2-6].

In this study, MSU mesoporous silica materials were synthesized from sodium metasilicate pentahydrate (SMP) which is more cost-effective than the tetraethyl orthosilicate (TEOS) as a silica source and Pluronic 123 as a nonionic structure-directing triblock copolymer surfactant in an acidic medium. The synthesized materials were characterized by X-ray diffraction (XRD) and Fourier transform infrared spectroscopy (FTIR) analyses. The obtained results showed that the MSU-x was successfully synthesized. 

Keywords

References

  1. C. Boissie`re, A. Larbot, E. Prouzet, Chemistry of Materials 2000, 12, 1937-1940.
  2. K S. Triantafyllidis, E. F. Iliopoulou, E. V. Antonakou, A. A. Lappas, H. Wang, T. J. Pinnavaia, Microporous and Mesoporous Materials, 2007, 99, 132-139.
  3. Y. Jung, S. Kim, S. J. Park, J. M. Kim, Colloids and Surfaces A: Physicochem. Eng. Aspects, 2008, 313-314, 162-166.
  4. H. Liu, Z. Wang, H. Hu, Y. Liang, M. Wang, Journal of Solid State Chemistry, 2009, 182, 1726-1732.
  5. E. Prouzet, C. Boissiere, C. R. Chimie, 2005, 8, 579-596.
  6. M. Kruk, M. Jaroniec, J. Phys. Chem. 2001, 105, 7663-7670.
  7. P.S. Liu, G.F. Chen, ‘Porous Materials’, Chapter 9, Tsinghua University Press Limited. Published by Elsevier Inc. , 2014.
  8. P.S. Liu, G.F. Chen, ‘Porous Materials’, Chapter 3, Tsinghua University Press Limited. Published by Elsevier Inc. , 2014.

Details

Primary Language

English

Subjects

-

Journal Section

-

Authors

Nervin Mermer This is me

Sevil Karakaş This is me

Publication Date

December 23, 2015

Submission Date

December 23, 2015

Acceptance Date

-

Published in Issue

Year 2015 Volume: 11 Number: 3

APA
Mermer, N., Karakaş, S., & Yılmaz, M. (2015). The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate. Celal Bayar University Journal of Science, 11(3). https://doi.org/10.18466/cbujos.55665
AMA
1.Mermer N, Karakaş S, Yılmaz M. The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate. CBUJOS. 2015;11(3). doi:10.18466/cbujos.55665
Chicago
Mermer, Nervin, Sevil Karakaş, and Müge Yılmaz. 2015. “The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate”. Celal Bayar University Journal of Science 11 (3). https://doi.org/10.18466/cbujos.55665.
EndNote
Mermer N, Karakaş S, Yılmaz M (December 1, 2015) The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate. Celal Bayar University Journal of Science 11 3
IEEE
[1]N. Mermer, S. Karakaş, and M. Yılmaz, “The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate”, CBUJOS, vol. 11, no. 3, Dec. 2015, doi: 10.18466/cbujos.55665.
ISNAD
Mermer, Nervin - Karakaş, Sevil - Yılmaz, Müge. “The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate”. Celal Bayar University Journal of Science 11/3 (December 1, 2015). https://doi.org/10.18466/cbujos.55665.
JAMA
1.Mermer N, Karakaş S, Yılmaz M. The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate. CBUJOS. 2015;11. doi:10.18466/cbujos.55665.
MLA
Mermer, Nervin, et al. “The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate”. Celal Bayar University Journal of Science, vol. 11, no. 3, Dec. 2015, doi:10.18466/cbujos.55665.
Vancouver
1.Nervin Mermer, Sevil Karakaş, Müge Yılmaz. The Synthesis of MSU-X Mesoporous Materials from Sodium Silicate. CBUJOS. 2015 Dec. 1;11(3). doi:10.18466/cbujos.55665