Research Article

Droplet-based Microfluidic Device for the Synthesis of Silica Nanoparticles

Volume: 16 Number: 3 September 29, 2020
EN

Droplet-based Microfluidic Device for the Synthesis of Silica Nanoparticles

Abstract

Microfluidic reactors are advantageous for nanomaterial synthesis due to their capability to provide controlled reaction environment. In this work, a droplet based microfluidic reactor is designed for the synthesis of silica nanoparticles. The synthesis is carried out in a very controlled environment and a uniform size and shape distribution is achieved. The classical synthesis protocol for silica nanoparticles is modified to use nonpolar solvents in the reaction so that this platform can later be used for coating hydrophobic nanomaterials. Therefore, this study not only presents a new device but also a new synthesis method. The results are compared with conventional batch wise synthesis methods and the obtained nanoparticles showed better size distribution.

Keywords

Supporting Institution

TÜBİTAK

Project Number

114C092

Thanks

E. Y. Erdem would like to acknowledge the Tübitak 2232 grant that founded this research. She also thanks Mr. Alican Özkan and Mr. Arsalan Nikdoost for their help in laboratory studies.

References

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  3. 3. Wu, KCW, Yamauchi, Y. 2012. Controlling physical features of mesoporoussilica nanoparticles (MSNs) for emergingapplications. Journal of Materials Chemistry; 22:1251-1256.
  4. 4. Mebert, AM, Baglole, CJ, Desimone, MF, Maysinger, Dusica. 2017. Nanoengineered silica: properties, applications and toxicity. Food and Chemical Toxicology; 109(1): 753-770.
  5. 5. Erdem, EY, Cheng, JC, Doyle, FM, Pisano, AP. 2014. Multitemperature zone, droplet-based microreactor for increased temperature control in nanoparticle synthesis. Small; 10(6): 1076-1080.
  6. 6. Phillips, TW, Lignos, IG, Maceiczyk, RM, DeMello, AJ, DeMello, A. 2014. Nanocrystal synthesis in microfluidic reactors: where next?. Lab Chip.; 14(17): 3172-3180,
  7. 7. Chang, CH, Paul, BK, Remcho, VT, Atre, S, Hutchison, JE. 2008. Synthesis and post-processing of nanomaterials using microreaction technology. Journal of Nanoparticle Research; 10: 965-980.
  8. 8. Nightingale, AM, deMello, JC. 2012. Segmented flow reactors for nanocrystal synthesis. Advanced Materials; 25(13): 1813-1821.

Details

Primary Language

English

Subjects

Engineering

Journal Section

Research Article

Publication Date

September 29, 2020

Submission Date

April 29, 2020

Acceptance Date

September 7, 2020

Published in Issue

Year 2020 Volume: 16 Number: 3

APA
Erdem, E. Y. (2020). Droplet-based Microfluidic Device for the Synthesis of Silica Nanoparticles. Celal Bayar University Journal of Science, 16(3), 245-249. https://doi.org/10.18466/cbayarfbe.729586
AMA
1.Erdem EY. Droplet-based Microfluidic Device for the Synthesis of Silica Nanoparticles. CBUJOS. 2020;16(3):245-249. doi:10.18466/cbayarfbe.729586
Chicago
Erdem, Emine Yegan. 2020. “Droplet-Based Microfluidic Device for the Synthesis of Silica Nanoparticles”. Celal Bayar University Journal of Science 16 (3): 245-49. https://doi.org/10.18466/cbayarfbe.729586.
EndNote
Erdem EY (September 1, 2020) Droplet-based Microfluidic Device for the Synthesis of Silica Nanoparticles. Celal Bayar University Journal of Science 16 3 245–249.
IEEE
[1]E. Y. Erdem, “Droplet-based Microfluidic Device for the Synthesis of Silica Nanoparticles”, CBUJOS, vol. 16, no. 3, pp. 245–249, Sept. 2020, doi: 10.18466/cbayarfbe.729586.
ISNAD
Erdem, Emine Yegan. “Droplet-Based Microfluidic Device for the Synthesis of Silica Nanoparticles”. Celal Bayar University Journal of Science 16/3 (September 1, 2020): 245-249. https://doi.org/10.18466/cbayarfbe.729586.
JAMA
1.Erdem EY. Droplet-based Microfluidic Device for the Synthesis of Silica Nanoparticles. CBUJOS. 2020;16:245–249.
MLA
Erdem, Emine Yegan. “Droplet-Based Microfluidic Device for the Synthesis of Silica Nanoparticles”. Celal Bayar University Journal of Science, vol. 16, no. 3, Sept. 2020, pp. 245-9, doi:10.18466/cbayarfbe.729586.
Vancouver
1.Emine Yegan Erdem. Droplet-based Microfluidic Device for the Synthesis of Silica Nanoparticles. CBUJOS. 2020 Sep. 1;16(3):245-9. doi:10.18466/cbayarfbe.729586