Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate

Celâl Tüzün

Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate

Abstract

4-Amino-N-ethyl-N-ı8~hydroxyethylaniline hemi-sulfate hydrate was synthesized by nitrosation of N-ethyl-N-p-hydroxyethylaniline, then reduced with zinc powder/ hydrochloric acid, without isolating of the nitroso compound. The amine salt so formed was basified with ammonia, then extracted with chloroform and the free base converted its hemi-sulfate hydrate directly, by adding a sufficient amount of sulfuric acid in ethanol.

Keywords

Synthesis, Hydrate, Hemi-Sulfate

References

Ankara Üniversitesi Communications, Series B: Chemistry and Chemical Engineering

Details

Primary Language

English

Subjects

Chemical Engineering

Journal Section

Research Article

Authors

Celâl Tüzün This is me
Türkiye

Publication Date

January 1, 1968

Submission Date

January 1, 1968

Acceptance Date

-

Published in Issue

Year 1968 Volume: 15

IZ

https://izlik.org/JA95PT26LG

APA

Tüzün, C. (1968). Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate. Communications Faculty of Sciences University of Ankara Series B Chemistry and Chemical Engineering, 15. https://izlik.org/JA95PT26LG

AMA

1.Tüzün C. Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate. Commun. Fac. Sci. Univ. Ank. Ser. B. 1968;15. https://izlik.org/JA95PT26LG

Chicago

Tüzün, Celâl. 1968. “Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate”. Communications Faculty of Sciences University of Ankara Series B Chemistry and Chemical Engineering 15 (January). https://izlik.org/JA95PT26LG.

EndNote

Tüzün C (January 1, 1968) Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate. Communications Faculty of Sciences University of Ankara Series B Chemistry and Chemical Engineering 15

IEEE

[1]C. Tüzün, “Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate”, Commun. Fac. Sci. Univ. Ank. Ser. B, vol. 15, Jan. 1968, [Online]. Available: https://izlik.org/JA95PT26LG

ISNAD

Tüzün, Celâl. “Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate”. Communications Faculty of Sciences University of Ankara Series B Chemistry and Chemical Engineering 15 (January 1, 1968). https://izlik.org/JA95PT26LG.

JAMA

1.Tüzün C. Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate. Commun. Fac. Sci. Univ. Ank. Ser. B. 1968;15. Available at https://izlik.org/JA95PT26LG.

MLA

Tüzün, Celâl. “Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate”. Communications Faculty of Sciences University of Ankara Series B Chemistry and Chemical Engineering, vol. 15, Jan. 1968, https://izlik.org/JA95PT26LG.

Vancouver

1.Celâl Tüzün. Synthesis of 4-Amino-N-Ethyl-N-P-HydroxyethyIanilin Hemi-Sulfate Hydrate. Commun. Fac. Sci. Univ. Ank. Ser. B [Internet]. 1968 Jan. 1;15. Available from: https://izlik.org/JA95PT26LG

Communications Faculty of Sciences University of Ankara Series B Chemistry and Chemical Engineering

This work is licensed under a Creative Commons Attribution 4.0 International License.