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Synthesis, Homopolymerization and Coplymerization of 9-antryl methyl metacrylate and β-naphtyl metacrylate

Year 2015, Volume: 36 Issue: 3, 1657 - 1663, 13.05.2015

Samaneh Hamidizare , Mohammad Hossein Nasir Tabrizi

Abstract

Abstract. 9-antryl methyl metacrylate is synthesized by reaction of 9-anthracene methanol and methcryloyl chloride in the peresence of Et3N in THF as solvent. After characterization of this monomer, by IR and NMR spectroscopic technique, we report the homopolymerization and copolymerization 9-antryl methyl metacrylate using the reaction of styrene in the presence of AIBN as initiator. The structure of all target compounds was characterized by spectral analyses. The thermal behavior of the polymers is studied by TGA.

Keywords

9-anthracene methanol methcryloyl chloride Copolymerization β-naphthol

References

  • Bevinton, J. C., Malpass, B. W. (1965) " Reactivity ratios for the copolymerization of acrylates and methacrylates by nuclear magnetic resonance spectroscopy "European polymer journal, 1, pp.55
  • Coustantinova, T. N., Garbechev, I. K., (1998) polymer International, 43, pp. 49
  • Rouhallah B., Ali-asghar, M. (1998) Synthesis of methyl methacrylate-n-butylacrylate copolymers: Study of the paint properties ""J. Appl. Polym. Sci 70, pp. 367-372
  • Vijayanand P.S, Aron Prasath R., Balaji R., Nanjundan S., (2002) " Synthesis, spectral properties, and thermal properties of homo- and copolymers of 3,5-dimethylphenyl acrylate with glycidyl methacrylate and determination of reactivity ratios "J Appl Polym Sci 85, pp. 2261-2270
  • Ajmal, A., Mideen, A. S., Quraishi, M. A. (1994) " Green seed extract of Tectona grandis as corrosion inhibitor for mild steel in acid medium" Corros. Sci 36, pp. 79
  • Singh, I. (1993) "Synthesis, characterization, and corrosion protection properties of poly(N-(methacryloyloxymethyl) benzotriazole-co-methyl methacrylate) on mild steel " Corrosion, 49, pp. 122
  • Vijayanand, P. S., Sreekuttan Unnithan, C., Penlidis, A., Nanjundan, S. (2007), " Copolymerization of 4-Acetylphenyl Methacrylate with Ethyl Methacrylate: Synthesis, Characterization, Monomer Reactivity Ratios, and Thermal Properties " Journal of macromolecular science, 42, pp. 555-569
  • Mizognchi, K. Hasegawa, E., (1996) "Studies on photocrosslinkable copolymers of 4- methacryloyloxyphenyl-3′,4′-dimethoxystyryl ketone and methyl methacrylate."Polym. Adv. Technol. 7 pp. 471.
  • Patel R. J., Patel Z. H., Patel B. C., Bhavesh P. D. (2013) "Synthesis of acrylic copolymers and their antimicrobial screening" Der Pharma Chemica, 5, pp. 63-72
  • Reis A. V., Cavalcanti O.A., Rubira A. F., Muniz E. C., (2003)," Synthesis and characterization of hydrogels formed from a glycidyl methacrylate derivative of galactomannan " Int J Pharm, 267, pp.13-25
  • Marton, O. R. Varnishes and Lacquers, European Polymer Journal, 1968

Year 2015, Volume: 36 Issue: 3, 1657 - 1663, 13.05.2015

Samaneh Hamidizare , Mohammad Hossein Nasir Tabrizi

Abstract

References

  • Bevinton, J. C., Malpass, B. W. (1965) " Reactivity ratios for the copolymerization of acrylates and methacrylates by nuclear magnetic resonance spectroscopy "European polymer journal, 1, pp.55
  • Coustantinova, T. N., Garbechev, I. K., (1998) polymer International, 43, pp. 49
  • Rouhallah B., Ali-asghar, M. (1998) Synthesis of methyl methacrylate-n-butylacrylate copolymers: Study of the paint properties ""J. Appl. Polym. Sci 70, pp. 367-372
  • Vijayanand P.S, Aron Prasath R., Balaji R., Nanjundan S., (2002) " Synthesis, spectral properties, and thermal properties of homo- and copolymers of 3,5-dimethylphenyl acrylate with glycidyl methacrylate and determination of reactivity ratios "J Appl Polym Sci 85, pp. 2261-2270
  • Ajmal, A., Mideen, A. S., Quraishi, M. A. (1994) " Green seed extract of Tectona grandis as corrosion inhibitor for mild steel in acid medium" Corros. Sci 36, pp. 79
  • Singh, I. (1993) "Synthesis, characterization, and corrosion protection properties of poly(N-(methacryloyloxymethyl) benzotriazole-co-methyl methacrylate) on mild steel " Corrosion, 49, pp. 122
  • Vijayanand, P. S., Sreekuttan Unnithan, C., Penlidis, A., Nanjundan, S. (2007), " Copolymerization of 4-Acetylphenyl Methacrylate with Ethyl Methacrylate: Synthesis, Characterization, Monomer Reactivity Ratios, and Thermal Properties " Journal of macromolecular science, 42, pp. 555-569
  • Mizognchi, K. Hasegawa, E., (1996) "Studies on photocrosslinkable copolymers of 4- methacryloyloxyphenyl-3′,4′-dimethoxystyryl ketone and methyl methacrylate."Polym. Adv. Technol. 7 pp. 471.
  • Patel R. J., Patel Z. H., Patel B. C., Bhavesh P. D. (2013) "Synthesis of acrylic copolymers and their antimicrobial screening" Der Pharma Chemica, 5, pp. 63-72
  • Reis A. V., Cavalcanti O.A., Rubira A. F., Muniz E. C., (2003)," Synthesis and characterization of hydrogels formed from a glycidyl methacrylate derivative of galactomannan " Int J Pharm, 267, pp.13-25
  • Marton, O. R. Varnishes and Lacquers, European Polymer Journal, 1968
There are 11 citations in total.

Details

Journal Section Special
Authors

Samaneh Hamidizare

Mohammad Hossein Nasir Tabrizi This is me

Publication Date May 13, 2015
Published in Issue Year 2015 Volume: 36 Issue: 3

Cite

APA Hamidizare, S., & Nasir Tabrizi, M. H. (2015). Synthesis, Homopolymerization and Coplymerization of 9-antryl methyl metacrylate and β-naphtyl metacrylate. Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi, 36(3), 1657-1663.
AMA Hamidizare S, Nasir Tabrizi MH. Synthesis, Homopolymerization and Coplymerization of 9-antryl methyl metacrylate and β-naphtyl metacrylate. Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi. May 2015;36(3):1657-1663.
Chicago Hamidizare, Samaneh, and Mohammad Hossein Nasir Tabrizi. “Synthesis, Homopolymerization and Coplymerization of 9-Antryl Methyl Metacrylate and β-Naphtyl Metacrylate”. Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi 36, no. 3 (May 2015): 1657-63.
EndNote Hamidizare S, Nasir Tabrizi MH (May 1, 2015) Synthesis, Homopolymerization and Coplymerization of 9-antryl methyl metacrylate and β-naphtyl metacrylate. Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi 36 3 1657–1663.
IEEE S. Hamidizare and M. H. Nasir Tabrizi, “Synthesis, Homopolymerization and Coplymerization of 9-antryl methyl metacrylate and β-naphtyl metacrylate”, Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi, vol. 36, no. 3, pp. 1657–1663, 2015.
ISNAD Hamidizare, Samaneh - Nasir Tabrizi, Mohammad Hossein. “Synthesis, Homopolymerization and Coplymerization of 9-Antryl Methyl Metacrylate and β-Naphtyl Metacrylate”. Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi 36/3 (May 2015), 1657-1663.
JAMA Hamidizare S, Nasir Tabrizi MH. Synthesis, Homopolymerization and Coplymerization of 9-antryl methyl metacrylate and β-naphtyl metacrylate. Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi. 2015;36:1657–1663.
MLA Hamidizare, Samaneh and Mohammad Hossein Nasir Tabrizi. “Synthesis, Homopolymerization and Coplymerization of 9-Antryl Methyl Metacrylate and β-Naphtyl Metacrylate”. Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi, vol. 36, no. 3, 2015, pp. 1657-63.
Vancouver Hamidizare S, Nasir Tabrizi MH. Synthesis, Homopolymerization and Coplymerization of 9-antryl methyl metacrylate and β-naphtyl metacrylate. Cumhuriyet Üniversitesi Fen Edebiyat Fakültesi Fen Bilimleri Dergisi. 2015;36(3):1657-63.