Evaluation of Color Stability in One- and Multi-Shade Composite Resin Materials Polymerized with Different Curing Modes
Year 2025,
Volume: 52 Issue: 1, 34 - 40, 30.04.2025
Leyla Kerimova
,
Ruhsan Müdüroğlu Adıgüzel
,
Bilge Ersöz
,
Meriç Yavuz Çolak
,
Kıvanç Yamanel
Abstract
Purpose: The aim of this in vitro study is to instrumentally compare the color stability of two different one-shade and a multi-shade universal composite resin material after light-cure in soft start (SS) and standard (ST) curing modes.
Materials and Methods: Seventy-eight discs were prepared using two different one-shade composite materials (Omnichroma and Vittra Unique) and A2 shade of a multi-shade universal resin-based composite (Filtek Z250, 3M) when half of them was light-cured in ST and half in SS mode (n=13). The samples were placed in 5 ml of coffee solution and incubated at 37 °C for 30 days for the staining challenge. On the 1st, 7th, and 30th days, the measurements of L*, a*, and b* values were performed with a spectrophotometer and the color change was calculated by using the CIEDE2000 formula (ΔE00).
Results: All materials exhibited significant and clinically unacceptable changes in color over time, regardless of curing mode (p < 0.05) and the maximum staining occurred in the first 24 hours and the first 7 days. Generally, the higher color change observed in the SS groups and Filtek Z250 statistically demonstrated the least staining. However, staining within the first 24 hours was not influenced by curing mode (p > 0.05).
Conclusions: The curing mode and material type used for restoration may affect the amount of material staining caused by coffee consumption.
Supporting Institution
Başkent University
Thanks
Tokuyama Turkey is gratefully acknowledged for providing the composite resin materials used in this project. The authors do not have any financial interest in the companies whose materials are included in this article.
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late Based Resins on the C=C Degree of Conversion, Resid-
ual Monomer Content and Mechanical Properties. Polymers
(Basel). 2021;13(24). doi:10.3390/polym13244415.
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5. Wang WJ, Grymak A, Waddell JN, Choi JJE. The effect of light
curing intensity on bulk-fill composite resins: heat genera-
tion and chemomechanical properties. Biomater Investig Dent.
2021;8(1):137–151. doi:10.1080/26415275.2021.1979981.
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6. Arocha MA, Mayoral JR, Lefever D, Mercade M, Basilio J, Roig M.
Color stability of siloranes versus methacrylate-based compos-
ites after immersion in staining solutions. Clin Oral Investig.
2013;17(6):1481–1487. doi:10.1007/s00784-012-0837-7.
-
7. Reis AF, Vestphal M, Amaral RCD, Rodrigues JA, Roulet JF,
Roscoe MG. Efficiency of polymerization of bulk-fill composite
resins: a systematic review. Braz Oral Res. 2017;31(suppl 1):e59.
doi:10.1590/1807-3107BOR-2017.vol31.0059.
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8. Domingos PA, Garcia PP, Oliveira AL, Palma-Dibb RG. Com-
posite resin color stability: influence of light sources and
immersion media. J Appl Oral Sci. 2011;19(3):204–211.
doi:10.1590/s1678-77572011000300005.
-
9. Aguiar FH, Braceiro A, Lima DA, Ambrosano GM, Lovadino
JR. Effect of light curing modes and light curing time on the
microhardness of a hybrid composite resin. J Contemp Dent
Pract. 2007;8(6):1–8. doi:10.5005/jcdp-8-6-1.
-
10. Ozan G, Sancakli HS, Tiryaki M, Bayrak I. Effect of light
curing modes on the color stability of a nanohybrid compos-
ite immersed in different beverages. Odovtos-Int J Dent Sc.
2020;22(2):71–81. doi:10.15517/ijds.2020.38726.
-
11. Selivany BJ. The Effect of Different Immersion Media, Poly-
merization Modes, and Brushing on the Color Stability of Dif-
ferent Composite Resins. Int J Periodontics Restorative Dent.
2023;43(2):246–255. doi:10.11607/prd.6427.
-
12. Paolone G, Formiga S, De Palma F, Abbruzzese L, Chirico L,
Scolavino S, et al. Color stability of resin-based composites:
Staining procedures with liquids-A narrative review. J Esthet
Restor Dent. 2022;34(6):865–887. doi:10.1111/jerd.12912.
-
13. Gomez-Polo C, Portillo Munoz M, Lorenzo Luengo MC, Vicente
P, Galindo P, Martin Casado AM. Comparison of the CIELab
and CIEDE2000 color difference formulas. J Prosthet Dent.
2016;115(1):65–70. doi:10.1016/j.prosdent.2015.07.001.
-
14. Lang-Salas MG, Villarreal-Romero LA, Domínguez-Monreal
JA, Cuevas-González JC, Donohué-Cornejo A, Reyes-López SY,
et al. Evaluation of adhesion of total etch adhesive systems on
bovine dental enamel using a deproteinizing agent: an in vitro
study. Revista ADM. 2020;77(1):22–27. doi:10.35366/OD201E.
-
15. Paravina RD, Ghinea R, Herrera LJ, Bona AD, Igiel C, Linninger
M, et al. Color difference thresholds in dentistry. J Esthet Restor
Dent. 2015;27 Suppl 1:S1–9. doi:10.1111/jerd.12149.
-
16. Ernst CP, Brand N, Frommator U, Rippin G, Willershausen B.
Reduction of polymerization shrinkage stress and marginal
microleakage using soft-start polymerization. J Esthet Restor
Dent. 2003;15(2):93–103; discussion 104. doi:10.1111/j.1708-
8240.2003.tb00323.x.
-
17. Munchow EA, Meereis CTW, de Oliveira da Rosa WL, da Silva AF,
Piva E. Polymerization shrinkage stress of resin-based dental
materials: A systematic review and meta-analyses of technique
protocol and photo-activation strategies. J Mech Behav Biomed
Mater. 2018;82:77–86. doi:10.1016/j.jmbbm.2018.03.004.
-
18. Lu H, Stansbury JW, Bowman CN. Impact of curing protocol on
conversion and shrinkage stress. J Dent Res. 2005;84(9):822–
826. doi:10.1177/154405910508400908.
-
19. Taubock TT, Feilzer AJ, Buchalla W, Kleverlaan CJ, Krejci I, Attin
T. Effect of modulated photo-activation on polymerization
shrinkage behavior of dental restorative resin composites. Eur
J Oral Sci. 2014;122(4):293–302. doi:10.1111/eos.12139.
-
20. Zanchi CH, de Carvalho RV, Rodrigues Junior SA, Demarco
FF, Burnett Junior LH. Shrinkage stress of three compos-
ites under different polymerization methods. Braz Oral Res.
2006;20(2):137–142. doi:10.1590/s1806-83242006000200009.
-
21. Ilie N, Jelen E, Hickel R. Is the soft-start polymerisation con-
cept still relevant for modern curing units? Clin Oral Investig.
2011;15:21–29. doi:10.1007/s00784-009-0354-5.
-
22. Checchi V, Forabosco E, Della Casa G, Kaleci S, Giannetti L, Gen-
erali L, et al. Color Stability Assessment of Single- and Multi-
Shade Composites Following Immersion in Staining Food Sub-
stances. Dent J (Basel). 2024;12(9). doi:10.3390/dj12090285.
-
23. Kobayashi S, Nakajima M, Furusawa K, Tichy A, Hosaka K,
Tagami J. Color adjustment potential of single-shade resin
composite to various-shade human teeth: Effect of struc-
tural color phenomenon. Dent Mater J. 2021;40(4):1033–1040.
doi:10.4012/dmj.2020-364.
-
24. Ertas E, Guler AU, Yucel AC, Koprulu H, Guler E. Color stability
of resin composites after immersion in different drinks. Dent
Mater J. 2006;25(2):371–6. doi:10.4012/dmj.25.371.
-
25. Topcu FT, Sahinkesen G, Yamanel K, Erdemir U, Oktay EA,
Ersahan S. Influence of different drinks on the colour stabil-
ity of dental resin composites. Eur J Dent. 2009;3(1):50–56.
doi:10.1055/s-0039-1697405.
-
26. Alex A, Venkatesh V. Comparative Evaluation of Surface
Roughness and Color Stability Between Single-Shade Com-
posite and Multi-Shade Composite: An In Vitro Study. Cureus.
2024;16(7):e65396. doi:10.7759/cureus.65396.
-
27. Chen S, Zhu J, Yu M, Jin C, Huang C. Effect of aging and bleach-
ing on the color stability and surface roughness of a recently in-
troduced single-shade composite resin. J Dent. 2024;143:104917.
doi:10.1016/j.jdent.2024.104917.
-
28. Ersoz B, Karaoglanoglu S, Oktay EA, Aydin N. of Single-shade Composites to Discoloration. Resistance
Oper Dent.
2022;47(6):686–692. doi:10.2341/21-156-L.
-
29. Cumhur A, Özkoçak BBC. Evaluation of the Color Stability and
Surface Roughness of a Novel Single-Shade Composite Resin:
A Smart Chromatic Technology. Evaluation. 2024;9(1):28–35.
doi:10.4274/cjms.2023.2023-37.
-
30. Fidan M, Yagci O. Effect of aging and fiber-reinforcement
on color stability, translucency, and microhardness of single-
shade resin composites versus multi-shade resin composite. J
Esthet Restor Dent. 2024;36(4):632–642. doi:10.1111/jerd.13125.
-
31. Tepe H, Çeliksöz O, Biçer Z, Yaman B. Evaluating the effects of
bleaching on color stability and surface roughness in single-
shade and multi-shade resin composites. ACMJ. 2024;6(6):372–
381. doi:10.38053/acmj.1543644.
-
32. Bilgili Can D, Ozarslan M. Evaluation of color stability and
microhardness of contemporary bulk-fill composite resins
with different polymerization properties. J Esthet Restor Dent.
2022;34(6):924–932. doi:10.1111/jerd.12879.
Year 2025,
Volume: 52 Issue: 1, 34 - 40, 30.04.2025
Leyla Kerimova
,
Ruhsan Müdüroğlu Adıgüzel
,
Bilge Ersöz
,
Meriç Yavuz Çolak
,
Kıvanç Yamanel
References
-
AlHamdan EM, Bashiri A, Alnashmi F, Al-Saleh S, Al-Shahrani
K, Al-Shahrani S, et al. Evaluation of smart chromatic technol-
ogy for a single-shade dental polymer resin: an in vitro study.
Applied Sciences. 2021;11(21):10108. doi:10.3390/app112110108.
-
Shamszadeh S, Sheikh-Al-Eslamian SM, Hasani E, Abrand-
abadi AN, Panahandeh N. Color Stability of the Bulk-Fill
Composite Resins with Different Thickness in Response to
Coffee/Water Immersion. Int J Dent. 2016;2016:7186140.
doi:10.1155/2016/7186140.
-
3. Yilmaz Atali P, Dogu Kaya B, Manav Ozen A, Tarcin B, Senol
AA, Tuter Bayraktar E, et al. Assessment of Micro-Hardness,
Degree of Conversion, and Flexural Strength for Single-Shade
Universal Resin Composites. Polymers (Basel). 2022;14(22).
doi:10.3390/polym14224987.
-
4. Sarosi C, Moldovan M, Soanca A, Roman A, Gherman T, Trifoi A,
et al. Effects of Monomer Composition of Urethane Methacry-
late Based Resins on the C=C Degree of Conversion, Resid-
ual Monomer Content and Mechanical Properties. Polymers
(Basel). 2021;13(24). doi:10.3390/polym13244415.
-
5. Wang WJ, Grymak A, Waddell JN, Choi JJE. The effect of light
curing intensity on bulk-fill composite resins: heat genera-
tion and chemomechanical properties. Biomater Investig Dent.
2021;8(1):137–151. doi:10.1080/26415275.2021.1979981.
-
6. Arocha MA, Mayoral JR, Lefever D, Mercade M, Basilio J, Roig M.
Color stability of siloranes versus methacrylate-based compos-
ites after immersion in staining solutions. Clin Oral Investig.
2013;17(6):1481–1487. doi:10.1007/s00784-012-0837-7.
-
7. Reis AF, Vestphal M, Amaral RCD, Rodrigues JA, Roulet JF,
Roscoe MG. Efficiency of polymerization of bulk-fill composite
resins: a systematic review. Braz Oral Res. 2017;31(suppl 1):e59.
doi:10.1590/1807-3107BOR-2017.vol31.0059.
-
8. Domingos PA, Garcia PP, Oliveira AL, Palma-Dibb RG. Com-
posite resin color stability: influence of light sources and
immersion media. J Appl Oral Sci. 2011;19(3):204–211.
doi:10.1590/s1678-77572011000300005.
-
9. Aguiar FH, Braceiro A, Lima DA, Ambrosano GM, Lovadino
JR. Effect of light curing modes and light curing time on the
microhardness of a hybrid composite resin. J Contemp Dent
Pract. 2007;8(6):1–8. doi:10.5005/jcdp-8-6-1.
-
10. Ozan G, Sancakli HS, Tiryaki M, Bayrak I. Effect of light
curing modes on the color stability of a nanohybrid compos-
ite immersed in different beverages. Odovtos-Int J Dent Sc.
2020;22(2):71–81. doi:10.15517/ijds.2020.38726.
-
11. Selivany BJ. The Effect of Different Immersion Media, Poly-
merization Modes, and Brushing on the Color Stability of Dif-
ferent Composite Resins. Int J Periodontics Restorative Dent.
2023;43(2):246–255. doi:10.11607/prd.6427.
-
12. Paolone G, Formiga S, De Palma F, Abbruzzese L, Chirico L,
Scolavino S, et al. Color stability of resin-based composites:
Staining procedures with liquids-A narrative review. J Esthet
Restor Dent. 2022;34(6):865–887. doi:10.1111/jerd.12912.
-
13. Gomez-Polo C, Portillo Munoz M, Lorenzo Luengo MC, Vicente
P, Galindo P, Martin Casado AM. Comparison of the CIELab
and CIEDE2000 color difference formulas. J Prosthet Dent.
2016;115(1):65–70. doi:10.1016/j.prosdent.2015.07.001.
-
14. Lang-Salas MG, Villarreal-Romero LA, Domínguez-Monreal
JA, Cuevas-González JC, Donohué-Cornejo A, Reyes-López SY,
et al. Evaluation of adhesion of total etch adhesive systems on
bovine dental enamel using a deproteinizing agent: an in vitro
study. Revista ADM. 2020;77(1):22–27. doi:10.35366/OD201E.
-
15. Paravina RD, Ghinea R, Herrera LJ, Bona AD, Igiel C, Linninger
M, et al. Color difference thresholds in dentistry. J Esthet Restor
Dent. 2015;27 Suppl 1:S1–9. doi:10.1111/jerd.12149.
-
16. Ernst CP, Brand N, Frommator U, Rippin G, Willershausen B.
Reduction of polymerization shrinkage stress and marginal
microleakage using soft-start polymerization. J Esthet Restor
Dent. 2003;15(2):93–103; discussion 104. doi:10.1111/j.1708-
8240.2003.tb00323.x.
-
17. Munchow EA, Meereis CTW, de Oliveira da Rosa WL, da Silva AF,
Piva E. Polymerization shrinkage stress of resin-based dental
materials: A systematic review and meta-analyses of technique
protocol and photo-activation strategies. J Mech Behav Biomed
Mater. 2018;82:77–86. doi:10.1016/j.jmbbm.2018.03.004.
-
18. Lu H, Stansbury JW, Bowman CN. Impact of curing protocol on
conversion and shrinkage stress. J Dent Res. 2005;84(9):822–
826. doi:10.1177/154405910508400908.
-
19. Taubock TT, Feilzer AJ, Buchalla W, Kleverlaan CJ, Krejci I, Attin
T. Effect of modulated photo-activation on polymerization
shrinkage behavior of dental restorative resin composites. Eur
J Oral Sci. 2014;122(4):293–302. doi:10.1111/eos.12139.
-
20. Zanchi CH, de Carvalho RV, Rodrigues Junior SA, Demarco
FF, Burnett Junior LH. Shrinkage stress of three compos-
ites under different polymerization methods. Braz Oral Res.
2006;20(2):137–142. doi:10.1590/s1806-83242006000200009.
-
21. Ilie N, Jelen E, Hickel R. Is the soft-start polymerisation con-
cept still relevant for modern curing units? Clin Oral Investig.
2011;15:21–29. doi:10.1007/s00784-009-0354-5.
-
22. Checchi V, Forabosco E, Della Casa G, Kaleci S, Giannetti L, Gen-
erali L, et al. Color Stability Assessment of Single- and Multi-
Shade Composites Following Immersion in Staining Food Sub-
stances. Dent J (Basel). 2024;12(9). doi:10.3390/dj12090285.
-
23. Kobayashi S, Nakajima M, Furusawa K, Tichy A, Hosaka K,
Tagami J. Color adjustment potential of single-shade resin
composite to various-shade human teeth: Effect of struc-
tural color phenomenon. Dent Mater J. 2021;40(4):1033–1040.
doi:10.4012/dmj.2020-364.
-
24. Ertas E, Guler AU, Yucel AC, Koprulu H, Guler E. Color stability
of resin composites after immersion in different drinks. Dent
Mater J. 2006;25(2):371–6. doi:10.4012/dmj.25.371.
-
25. Topcu FT, Sahinkesen G, Yamanel K, Erdemir U, Oktay EA,
Ersahan S. Influence of different drinks on the colour stabil-
ity of dental resin composites. Eur J Dent. 2009;3(1):50–56.
doi:10.1055/s-0039-1697405.
-
26. Alex A, Venkatesh V. Comparative Evaluation of Surface
Roughness and Color Stability Between Single-Shade Com-
posite and Multi-Shade Composite: An In Vitro Study. Cureus.
2024;16(7):e65396. doi:10.7759/cureus.65396.
-
27. Chen S, Zhu J, Yu M, Jin C, Huang C. Effect of aging and bleach-
ing on the color stability and surface roughness of a recently in-
troduced single-shade composite resin. J Dent. 2024;143:104917.
doi:10.1016/j.jdent.2024.104917.
-
28. Ersoz B, Karaoglanoglu S, Oktay EA, Aydin N. of Single-shade Composites to Discoloration. Resistance
Oper Dent.
2022;47(6):686–692. doi:10.2341/21-156-L.
-
29. Cumhur A, Özkoçak BBC. Evaluation of the Color Stability and
Surface Roughness of a Novel Single-Shade Composite Resin:
A Smart Chromatic Technology. Evaluation. 2024;9(1):28–35.
doi:10.4274/cjms.2023.2023-37.
-
30. Fidan M, Yagci O. Effect of aging and fiber-reinforcement
on color stability, translucency, and microhardness of single-
shade resin composites versus multi-shade resin composite. J
Esthet Restor Dent. 2024;36(4):632–642. doi:10.1111/jerd.13125.
-
31. Tepe H, Çeliksöz O, Biçer Z, Yaman B. Evaluating the effects of
bleaching on color stability and surface roughness in single-
shade and multi-shade resin composites. ACMJ. 2024;6(6):372–
381. doi:10.38053/acmj.1543644.
-
32. Bilgili Can D, Ozarslan M. Evaluation of color stability and
microhardness of contemporary bulk-fill composite resins
with different polymerization properties. J Esthet Restor Dent.
2022;34(6):924–932. doi:10.1111/jerd.12879.