Synchrotron-based techniques for elemental analysis in soil-plant system under polluted environment

Year 2024, , 89 - 100, 29.03.2024

Mikhail Kirichkov Marina Burachevskaya Saglara Mandzhieva Tatiana Minkina Vishnu D. Rajput Dina Nevidomskaya Sudhir S. Shende Victoria Tsitsuashvili Aleksey Maksimov Svetlana Sushkova Coşkun Gülser , Rıdvan Kızılkaya

https://doi.org/10.18393/ejss.1401145

Cited By: 1

Abstract

Analytical techniques for elemental analysis in the soil-plant system have significance importance, especially emerging techniques such as synchrotron radiation (SR). Improved techniques allow samples to be examined in a non-invasive manner at high speed and resolution, resulting in better sample data. By applying various analytical techniques based on SR, it is possible to gather different information about the structure of the studied samples. In mining ecology, such techniques are widely used in assessing heavy metal-polluted sites, i.e., overburden dumps and areas around operating and mothballed mines. The present review elaborated insights into different analytical techniques for applying SR in plant-soil samples. The review also compared traditional research techniques with SR-based emerging and improved techniques. The need to use SR techniques for the complex diagnostics of sample structures to study their elemental and phase composition is substantiated. Using an integrated approach with SR, we can study the dynamics and speciation of HMs with carrier phases and uncover the mechanisms underlying the interactions between the adsorption centers of minerals, organic components, and heavy metals. It also improves the efficiency and accuracy of analysis and broadens the range of information obtained, which could lead to a more precise analysis of samples.

Keywords

Synchrotron radiation (SR), heavy metals, ore, spectroscopy, XRD, XAFS, FTIR, SRμCT

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