Research Article
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Year 2025, Volume: 26 Issue: 3, 379 - 386, 25.09.2025
https://doi.org/10.18038/estubtda.1751355

Abstract

References

  • [1] Kim HJ, Yoon M, Seo B, Lim C. Effects of fatty acid modified epoxy resin on long‐chain epoxy and its physical properties. J Polym Sci 2023; 61: 2194-2202.
  • [2] Kim TH, Kim DY, Lim CS, Seo BK. Studies of the physical properties of cycloaliphatic epoxy resin reacted with anhydride curing agents. Key Engineering Materials 2017; 737: 248-255.
  • [3] Huang R, Gao C, Zhou F, Yu J, Yang H. Mechanical properties analysis of cross-linked epoxy resin. J Phys Conf Ser 2024; 2783: 012054.
  • [4] Sun Y, et al. Development and application of medium-reactivity epoxy infusion resin system in large-scale wind turbine blades. J Phys Conf Ser 2024; 2737: 012001.
  • [5] Zhao C, Zhang G, Sun WM, Shi AH. Study on processing properties of epoxy resin system in VARI. Adv Mater Res 2012; 463-464: 704-708.
  • [6] Zhu Y, Liu J, Qin J, Wang D, Li W, Xu CA, Liang L. Preparation and performance comparison of low‐dielectric epoxy resins cured by naphthalene‐ and phenyl‐based active esters. J Appl Polym Sci 2025; 142: 56437.
  • [7] Bordun I, Szymczykiewicz E. Synthesis and electrochemical properties of Fe3O4/C nanocomposites for symmetric supercapacitors. Appl Sci 2024; 14: 677.
  • [8] Bagheri S, Nejad M. Fully biobased composite made with epoxidized‐lignin, reinforced with bamboo fibers. Polym Compos 2023; 44: 3926-3938.
  • [9] Dhiman A, Sharma AK, Agrawal G. Polymer based engineered materials for sustainable agriculture. ACS Agric Sci Technol 2022; 2: 693-711.
  • [10] Sobti R, Singh MP, Correa FS, Brar M, Kumar DK. Fabrication of biodegradable polymer nanocomposites for sustainable agriculture. E3S Web Conf 2024; 511: 01009.
  • [11] Nyambo C, Mohanty AK, Misra M. Polylactide-based renewable green composites from agricultural residues and their hybrids. Biomacromolecules 2010; 11: 1654-1660.
  • [12] Fernandes Medeiros de Queiroz H, Banea MD, Kawasaki Cavalcanti DK, de Souza e Silva Neto J. The effect of multiscale hybridization on the mechanical properties of natural fiber‐reinforced composites. J Appl Polym Sci 2021; 138: 51213.
  • [13] Pramudita M, Nasikin M, Suresh Babu M, Deva Kumar M. Mechanical characterization of kenaf natural fiber reinforced polymer composite with Terminalia chebula filler. J Phys Conf Ser 2024; 2837: 012024.
  • [14] Alzebdeh KI, Nassar MMA. Surface modification route for date palm fibers-polymer bio-composites towards improved interfacial crosslinking. Mater Sci Forum 2024; 1126: 89-108.
  • [15] Xiao D, Sun X. Mechanism research on the effect of the micro characteristics of filler particles on different bio‐composites formed by RPLA compounded with bio‐polymer fillers. Polym Compos 2025; 46: 4900-4926.
  • [16] Birbilen Y, Karakuş K, Mengeloğlu F. Production of sugar beet pulp/LDPE composites using compression molding method and investigation of some properties. Kastamonu Univ J For Fac 2021; 21: 295-305.
  • [17] Costantine G, Harb E, Bliard C, Maalouf C, Kinab E, Abbès B, Beaumont F, Polidori G. Experimental characterization of starch/beet-pulp bricks for building applications: drying kinetics and mechanical behavior. Constr Build Mater 2020; 264: 120270.
  • [18] Liu LS, Fishman ML, Hicks KB, Liu CK. Biodegradable composites from sugar beet pulp and poly(lactic acid). J Agric Food Chem 2005; 53: 9017-9022.
  • [19] Karpaky H, Maalouf C, Bliard C, Gacoin A, Lachi M, Polidori G. Mechanical and thermal characterization of a beet pulp-starch composite for building applications. E3S Web Conf 2019; 85: 08005.
  • [20] Gökdemir B. Investigation of usability of sugar beet pulp in biocomposite production. MSc, Izmir Katip Çelebi University, Izmir, Turkey, 2020.
  • [21] Baryga A, Ziobro R, Gumul D, Rosicka-Kaczmarek J, Miśkiewicz K. Physicochemical properties and evaluation of antioxidant potential of sugar beet pulp-preliminary analysis for further use (future prospects). Agriculture 2023; 13: 1039.
  • [22] Kopitzky R. Poly(lactic acid)-poly(butylene succinate)-sugar beet pulp composites; part I: mechanics of composites with fine and coarse sugar beet pulp particles. Polymers 2021; 13: 2531.
  • [23] Cárdenas-Fernández M, Hamley-Bennett C, Leak DJ, Lye GJ. Continuous enzymatic hydrolysis of sugar beet pectin and L-arabinose recovery within an integrated biorefinery. Bioresour Technol 2018; 269: 195-202.
  • [24] Sahoo SK, Khandelwal V, Manik G. Influence of epoxidized linseed oil and sisal fibers on structure-property relationship of epoxy biocomposite. Polym Compos 2018; 39: E2595-E2605.
  • [25] Suherman H, Aksa K, Mahyoedin Y, Septe E, Irmayani I. The effect of different fibre lengths on the mechanical properties of biocomposites. Mater Plast 2021; 58: 216-221.
  • [26] Auriga R, Borysiuk P, Latos M, Auriga A, Kwaśny Ł, Walkiewicz J. Impact of sugar beet pulp share on selected physical and mechanical properties of particleboards. Forests 2022; 14: 40.
  • [27] Liu LS, et al. Green composites from sugar beet pulp and poly(lactic acid): structural and mechanical characterization. J Biobased Mater Bioenergy 2007; 1: 323-330.

MECHANICAL CHARACTERIZATION OF EPOXY RESIN COMPOSITES REINFORCED WITH SUGAR BEET PULP FOR SUSTAINABLE MATERIAL APPLICATIONS

Year 2025, Volume: 26 Issue: 3, 379 - 386, 25.09.2025
https://doi.org/10.18038/estubtda.1751355

Abstract

In this study, the mechanical behavior of epoxy resin composites reinforced with 0%, 5%, 10%, and 20% beet pulp (BP) was systematically investigated. The specimens were prepared by casting into silicone molds and subjected to tensile and hardness tests. The results showed that increasing BP content led to a decrease in tensile strength from 36.5 ± 1.6 MPa (neat epoxy) to 23.1 ± 0.5 MPa, and a reduction in Vickers hardness from 9.8 HV to 8.8 HV. SEM analyses revealed that higher BP content caused weak interfacial bonding and pull-out voids, explaining the deterioration in mechanical performance. Although beet pulp has been studied in PLA, LDPE, PP, and starch-based matrices, its direct incorporation into epoxy resin without chemical treatment has not been reported. This study addresses this gap by systematically preparing and characterizing BP-reinforced epoxy composites and evaluating their tensile, hardness, and fracture surface behavior. The findings suggest that such composites may be considered for low-load applications, particularly in furniture panels, decorative coatings, and automotive interior trim components.

References

  • [1] Kim HJ, Yoon M, Seo B, Lim C. Effects of fatty acid modified epoxy resin on long‐chain epoxy and its physical properties. J Polym Sci 2023; 61: 2194-2202.
  • [2] Kim TH, Kim DY, Lim CS, Seo BK. Studies of the physical properties of cycloaliphatic epoxy resin reacted with anhydride curing agents. Key Engineering Materials 2017; 737: 248-255.
  • [3] Huang R, Gao C, Zhou F, Yu J, Yang H. Mechanical properties analysis of cross-linked epoxy resin. J Phys Conf Ser 2024; 2783: 012054.
  • [4] Sun Y, et al. Development and application of medium-reactivity epoxy infusion resin system in large-scale wind turbine blades. J Phys Conf Ser 2024; 2737: 012001.
  • [5] Zhao C, Zhang G, Sun WM, Shi AH. Study on processing properties of epoxy resin system in VARI. Adv Mater Res 2012; 463-464: 704-708.
  • [6] Zhu Y, Liu J, Qin J, Wang D, Li W, Xu CA, Liang L. Preparation and performance comparison of low‐dielectric epoxy resins cured by naphthalene‐ and phenyl‐based active esters. J Appl Polym Sci 2025; 142: 56437.
  • [7] Bordun I, Szymczykiewicz E. Synthesis and electrochemical properties of Fe3O4/C nanocomposites for symmetric supercapacitors. Appl Sci 2024; 14: 677.
  • [8] Bagheri S, Nejad M. Fully biobased composite made with epoxidized‐lignin, reinforced with bamboo fibers. Polym Compos 2023; 44: 3926-3938.
  • [9] Dhiman A, Sharma AK, Agrawal G. Polymer based engineered materials for sustainable agriculture. ACS Agric Sci Technol 2022; 2: 693-711.
  • [10] Sobti R, Singh MP, Correa FS, Brar M, Kumar DK. Fabrication of biodegradable polymer nanocomposites for sustainable agriculture. E3S Web Conf 2024; 511: 01009.
  • [11] Nyambo C, Mohanty AK, Misra M. Polylactide-based renewable green composites from agricultural residues and their hybrids. Biomacromolecules 2010; 11: 1654-1660.
  • [12] Fernandes Medeiros de Queiroz H, Banea MD, Kawasaki Cavalcanti DK, de Souza e Silva Neto J. The effect of multiscale hybridization on the mechanical properties of natural fiber‐reinforced composites. J Appl Polym Sci 2021; 138: 51213.
  • [13] Pramudita M, Nasikin M, Suresh Babu M, Deva Kumar M. Mechanical characterization of kenaf natural fiber reinforced polymer composite with Terminalia chebula filler. J Phys Conf Ser 2024; 2837: 012024.
  • [14] Alzebdeh KI, Nassar MMA. Surface modification route for date palm fibers-polymer bio-composites towards improved interfacial crosslinking. Mater Sci Forum 2024; 1126: 89-108.
  • [15] Xiao D, Sun X. Mechanism research on the effect of the micro characteristics of filler particles on different bio‐composites formed by RPLA compounded with bio‐polymer fillers. Polym Compos 2025; 46: 4900-4926.
  • [16] Birbilen Y, Karakuş K, Mengeloğlu F. Production of sugar beet pulp/LDPE composites using compression molding method and investigation of some properties. Kastamonu Univ J For Fac 2021; 21: 295-305.
  • [17] Costantine G, Harb E, Bliard C, Maalouf C, Kinab E, Abbès B, Beaumont F, Polidori G. Experimental characterization of starch/beet-pulp bricks for building applications: drying kinetics and mechanical behavior. Constr Build Mater 2020; 264: 120270.
  • [18] Liu LS, Fishman ML, Hicks KB, Liu CK. Biodegradable composites from sugar beet pulp and poly(lactic acid). J Agric Food Chem 2005; 53: 9017-9022.
  • [19] Karpaky H, Maalouf C, Bliard C, Gacoin A, Lachi M, Polidori G. Mechanical and thermal characterization of a beet pulp-starch composite for building applications. E3S Web Conf 2019; 85: 08005.
  • [20] Gökdemir B. Investigation of usability of sugar beet pulp in biocomposite production. MSc, Izmir Katip Çelebi University, Izmir, Turkey, 2020.
  • [21] Baryga A, Ziobro R, Gumul D, Rosicka-Kaczmarek J, Miśkiewicz K. Physicochemical properties and evaluation of antioxidant potential of sugar beet pulp-preliminary analysis for further use (future prospects). Agriculture 2023; 13: 1039.
  • [22] Kopitzky R. Poly(lactic acid)-poly(butylene succinate)-sugar beet pulp composites; part I: mechanics of composites with fine and coarse sugar beet pulp particles. Polymers 2021; 13: 2531.
  • [23] Cárdenas-Fernández M, Hamley-Bennett C, Leak DJ, Lye GJ. Continuous enzymatic hydrolysis of sugar beet pectin and L-arabinose recovery within an integrated biorefinery. Bioresour Technol 2018; 269: 195-202.
  • [24] Sahoo SK, Khandelwal V, Manik G. Influence of epoxidized linseed oil and sisal fibers on structure-property relationship of epoxy biocomposite. Polym Compos 2018; 39: E2595-E2605.
  • [25] Suherman H, Aksa K, Mahyoedin Y, Septe E, Irmayani I. The effect of different fibre lengths on the mechanical properties of biocomposites. Mater Plast 2021; 58: 216-221.
  • [26] Auriga R, Borysiuk P, Latos M, Auriga A, Kwaśny Ł, Walkiewicz J. Impact of sugar beet pulp share on selected physical and mechanical properties of particleboards. Forests 2022; 14: 40.
  • [27] Liu LS, et al. Green composites from sugar beet pulp and poly(lactic acid): structural and mechanical characterization. J Biobased Mater Bioenergy 2007; 1: 323-330.
There are 27 citations in total.

Details

Primary Language English
Subjects Composite and Hybrid Materials
Journal Section Articles
Authors

Muhammet Mevlüt Karaca 0000-0001-9644-3663

Mustafa Buğday 0000-0003-4413-509X

Publication Date September 25, 2025
Submission Date July 25, 2025
Acceptance Date September 14, 2025
Published in Issue Year 2025 Volume: 26 Issue: 3

Cite

AMA Karaca MM, Buğday M. MECHANICAL CHARACTERIZATION OF EPOXY RESIN COMPOSITES REINFORCED WITH SUGAR BEET PULP FOR SUSTAINABLE MATERIAL APPLICATIONS. Estuscience - Se. September 2025;26(3):379-386. doi:10.18038/estubtda.1751355