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SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES

Year 2018, Volume: 6 Issue: 2, 250 - 256, 01.06.2018

Muhammet Ceylan Beyza Nur Tepekıran

Abstract

This work related to fabrication of platinum nano particles, reveals considerably outstanding catalytic and electrical properties and preparation of Pt- PS nano composite. For this study Pt nano particles were synthesized by wet chemical method. Pt particles with 0.25%, 0.5%, 1% and 2% concentration amounts were added into the polystyrene solution, acquired by recycled PS. Three different composites which possess a distinct percentage of platinum were produced. Fibers were fabricated by electro spinning method afterward. Pt particles which were produced by wet chemical method and fibers were analyzed by SEM-EDS. There were various test and measurement methods performed to determine the characteristics of the platinum nano composite.

Keywords

platinum nanocomposites electro spinning fibers

References

  • Bonet, F., Tekaia-Elhsissen, K., & Sarathy, K. V. (2000). Study of interaction of ethylene glycol/PVP phase on noble metal powders prepared by polyol process. Bulletin of Materials Science, 23(3), 165-168.
  • Wang, C. D. (2007). Synthesis of Monodisperse Pt Nanocubes and Their Enhanced Catalysis for Oxygen Reduction. J. Am. Chem. Soc. 129.
  • Ahmadi, T. S., Wang, Z. L., Green, T. C., Henglein, A., & El-Sayed, M. A. (1996). Shape-controlled synthesis of colloidal platinum nanoparticles. Science, 272(5270), 1924-1925.
  • Greeley, J., Stephens, I. E. L., Bondarenko, A. S., Johansson, T. P., Hansen, H. A., Jaramillo, T. F., ... & Nørskov, J. K. (2009). Alloys of platinum and early transition metals as oxygen reduction electrocatalysts. Nature chemistry, 1(7), 552.
  • Murphy, S. E. (2009). Synthesis and Characterization of Silver–Platinum Bimetallic Nanowires and Platinum Nanotubes. Springer.
  • Jana, N. R., Gearheart, L., & Murphy, C. J. (2001). Wet chemical synthesis of high aspect ratio cylindrical gold nanorods. The Journal of Physical Chemistry B, 105(19), 4065-4067.
  • Herricks, T., Chen, J., & Xia, Y. (2004). Polyol synthesis of platinum nanoparticles: control of morphology with sodium nitrate. Nano Letters, 4(12), 2367-2371.
  • Chen, J. F., Wang, Y. H., Guo, F., Wang, X. M., & Zheng, C. (2000). Synthesis of nanoparticles with novel technology: high-gravity reactive precipitation. Industrial & engineering chemistry research, 39(4), 948-954.
  • Agarwal, S., Burgard, M., Greiner, A., & Wendorff, J. (2016). Electrospinning: A Practical Guide to Nanofibers. Walter de Gruyter GmbH & Co KG.
  • Nuraje, N., Khan, W. S., Lei, Y., Ceylan, M., & Asmatulu, R. (2013). Superhydrophobic electrospun nanofibers. Journal of Materials Chemistry A, 1(6), 1929-1946. [11] Khan, W. S., Asmatulu, R., Ceylan, M., & Jabbarnia, A. (2013). Recent progress on conventional and non-conventional electrospinning processes. Fibers and Polymers, 14(8), 1235-1247.
  • Huang, Z. M., Zhang, Y. Z., Kotaki, M., & Ramakrishna, S. (2003). A review on polymer nanofibers by electrospinning and their applications in nanocomposites. Composites science and technology, 63(15), 2223-2253.
  • Khan, W. S., Ceylan, M., Jabbarnia, A., Saeednia, L., Asmatulu, R., (2017), Chemical And Thermal Investigations Of Electrospun Polyacrylonitrile Nanofibers Incorporated With Various Nanoscale Inclusions, Journal of Thermal Engineering, 3(4), 1375-1390

Year 2018, Volume: 6 Issue: 2, 250 - 256, 01.06.2018

Muhammet Ceylan Beyza Nur Tepekıran

Abstract

References

  • Bonet, F., Tekaia-Elhsissen, K., & Sarathy, K. V. (2000). Study of interaction of ethylene glycol/PVP phase on noble metal powders prepared by polyol process. Bulletin of Materials Science, 23(3), 165-168.
  • Wang, C. D. (2007). Synthesis of Monodisperse Pt Nanocubes and Their Enhanced Catalysis for Oxygen Reduction. J. Am. Chem. Soc. 129.
  • Ahmadi, T. S., Wang, Z. L., Green, T. C., Henglein, A., & El-Sayed, M. A. (1996). Shape-controlled synthesis of colloidal platinum nanoparticles. Science, 272(5270), 1924-1925.
  • Greeley, J., Stephens, I. E. L., Bondarenko, A. S., Johansson, T. P., Hansen, H. A., Jaramillo, T. F., ... & Nørskov, J. K. (2009). Alloys of platinum and early transition metals as oxygen reduction electrocatalysts. Nature chemistry, 1(7), 552.
  • Murphy, S. E. (2009). Synthesis and Characterization of Silver–Platinum Bimetallic Nanowires and Platinum Nanotubes. Springer.
  • Jana, N. R., Gearheart, L., & Murphy, C. J. (2001). Wet chemical synthesis of high aspect ratio cylindrical gold nanorods. The Journal of Physical Chemistry B, 105(19), 4065-4067.
  • Herricks, T., Chen, J., & Xia, Y. (2004). Polyol synthesis of platinum nanoparticles: control of morphology with sodium nitrate. Nano Letters, 4(12), 2367-2371.
  • Chen, J. F., Wang, Y. H., Guo, F., Wang, X. M., & Zheng, C. (2000). Synthesis of nanoparticles with novel technology: high-gravity reactive precipitation. Industrial & engineering chemistry research, 39(4), 948-954.
  • Agarwal, S., Burgard, M., Greiner, A., & Wendorff, J. (2016). Electrospinning: A Practical Guide to Nanofibers. Walter de Gruyter GmbH & Co KG.
  • Nuraje, N., Khan, W. S., Lei, Y., Ceylan, M., & Asmatulu, R. (2013). Superhydrophobic electrospun nanofibers. Journal of Materials Chemistry A, 1(6), 1929-1946. [11] Khan, W. S., Asmatulu, R., Ceylan, M., & Jabbarnia, A. (2013). Recent progress on conventional and non-conventional electrospinning processes. Fibers and Polymers, 14(8), 1235-1247.
  • Huang, Z. M., Zhang, Y. Z., Kotaki, M., & Ramakrishna, S. (2003). A review on polymer nanofibers by electrospinning and their applications in nanocomposites. Composites science and technology, 63(15), 2223-2253.
  • Khan, W. S., Ceylan, M., Jabbarnia, A., Saeednia, L., Asmatulu, R., (2017), Chemical And Thermal Investigations Of Electrospun Polyacrylonitrile Nanofibers Incorporated With Various Nanoscale Inclusions, Journal of Thermal Engineering, 3(4), 1375-1390
There are 12 citations in total.

Details

Journal Section Articles
Authors

Muhammet Ceylan This is me

Beyza Nur Tepekıran This is me

Publication Date June 1, 2018
Published in Issue Year 2018 Volume: 6 Issue: 2

Cite

APA Ceylan, M., & Tepekıran, B. N. (2018). SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES. Eskişehir Teknik Üniversitesi Bilim Ve Teknoloji Dergisi B - Teorik Bilimler, 6(2), 250-256.
AMA Ceylan M, Tepekıran BN. SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES. Eskişehir Teknik Üniversitesi Bilim ve Teknoloji Dergisi B - Teorik Bilimler. June 2018;6(2):250-256.
Chicago Ceylan, Muhammet, and Beyza Nur Tepekıran. “SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES”. Eskişehir Teknik Üniversitesi Bilim Ve Teknoloji Dergisi B - Teorik Bilimler 6, no. 2 (June 2018): 250-56.
EndNote Ceylan M, Tepekıran BN (June 1, 2018) SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES. Eskişehir Teknik Üniversitesi Bilim ve Teknoloji Dergisi B - Teorik Bilimler 6 2 250–256.
IEEE M. Ceylan and B. N. Tepekıran, “SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES”, Eskişehir Teknik Üniversitesi Bilim ve Teknoloji Dergisi B - Teorik Bilimler, vol. 6, no. 2, pp. 250–256, 2018.
ISNAD Ceylan, Muhammet - Tepekıran, Beyza Nur. “SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES”. Eskişehir Teknik Üniversitesi Bilim ve Teknoloji Dergisi B - Teorik Bilimler 6/2 (June 2018), 250-256.
JAMA Ceylan M, Tepekıran BN. SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES. Eskişehir Teknik Üniversitesi Bilim ve Teknoloji Dergisi B - Teorik Bilimler. 2018;6:250–256.
MLA Ceylan, Muhammet and Beyza Nur Tepekıran. “SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES”. Eskişehir Teknik Üniversitesi Bilim Ve Teknoloji Dergisi B - Teorik Bilimler, vol. 6, no. 2, 2018, pp. 250-6.
Vancouver Ceylan M, Tepekıran BN. SYNTHESIS AND CHARACTERIZATION OF PLATINUM NANOCOMPOSITES. Eskişehir Teknik Üniversitesi Bilim ve Teknoloji Dergisi B - Teorik Bilimler. 2018;6(2):250-6.