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KARBAMAT GRUBU PESTİSİTLERLE DENEYSEL ZEHİRLENMELERDE ZEHİRİN İÇ ORGANLARDAN EKSTRAKSİYONU, İDENTİFİKASYONU VE TAYİNİ ÜZERİNDE KİMYASAL ARAŞTIRMALAR

Year 1985, Volume: 1 Issue: 1, 43 - 56, 01.03.1985

H. Ahmet Acet.

Abstract

Ülkemizde, entansif tarım yapıldığı bölgelerde, tarımsal ilaçların özellikle pestisidlerin bilinçsiz bir şekilde kullanıldığı bir gerçektir.
Bunlardan karbamat pestisidlerinin laboratuvarımız koşullarında tesbitine çalışıldı.
İnce- tabaka kromatografi ile karbamat pestisidlerin karbaril, baygon, mesurol, metomil, matasil, primikarb ve promikarb'ın teşhisi yapıldı.
Uygulama yapılmış plakalar on değişik solvan sistemi ile develope edildi. Dibromokinonklorimid, ninhidrin, rodamin B, rodamin B-AgN03:
bromin- fluoressein ayıraçları ve kısa dalga (254) UV ışığı, develope edilmiş plakalardaki lekeleri tayin etmek için kullanıldı. Bu ayıraçlarla ayrıca yedi çeşit karbamat pestisidin duyarlık sınırları ve renk reaksiyonları saptandı.
On tavşan ve üç köpeğe ağız yoluyla karbaril, baygon ve karbaril+
baygon karışımı LD50 dozda verildi. Hayvanların tümünün ilaç verildikten sonra öldüğü görüldü. Bu hayvanların mide - barsak, karaciğer, böbrek ve dalakları alındı. Araştırmada bu organlarda yukarıda belirtilen
maddeler saptandı. Bu, laboratuvar koşullarında doku örneklerinde dibromokinonklorimid
ayıracı ile karbamat pestisidleri 0,5 ug veya daha fazla düzeylerde tesbit edildi.

Chemical investigations for extraction, identification and determination of the poisons from animals' vicera that poisoned experimentally with carbamate groubs pecticides

Year 1985, Volume: 1 Issue: 1, 43 - 56, 01.03.1985

H. Ahmet Acet.

Abstract

It is fact that agricultural drugs, especially pesticides:
have been used unconsciously in the regions where intensive agriculture
is made in this country. Carbamate pecticides of these were studied to
determine under our laboratory conditions.
The identifications of carbaryl, baygon, mesurol, methomyl, matacil,
primicarbe and promecarbe of carbamate pecticides were made with
thin-layer chromatograms.
The spoted layers were developed with ten different solvent systems.
Dibromoquinonchlorimide, ninhydrin, rhodamin B, rhodamin B- AgN03,
bromin- fluorescein reagents and UV light with short wave (254 nm)
were used to determine the spots on the developed layers. The sensitivitiy
limits and the color reactions of seven various carbamate pecticides were
also determined with the aid of this reagents.
Carbaryl, baygon and carbaryl+ baygon mixture were given orally
to ten rabbits and three dogs in LD50 doses. After administering of the
drugs was seen that all animals were died. Stomach intestine, liver, kidney and spleen of these animals were removed. After the results of our
research was determinde the above stated chemical compounds in this
organs. Carbamate pecticides were determinde at the levels of 0,5 ug or
more with the aid of dibromoquinonchlorimid in this tissues samples on
this laboratory conditions.

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Details

Other ID JA74MZ64FF
Journal Section Research
Authors

H. Ahmet Acet. This is me

Publication Date March 1, 1985
Published in Issue Year 1985 Volume: 1 Issue: 1

Cite

APA Acet., H. A. (1985). Chemical investigations for extraction, identification and determination of the poisons from animals’ vicera that poisoned experimentally with carbamate groubs pecticides. Eurasian Journal of Veterinary Sciences, 1(1), 43-56.
AMA Acet. HA. Chemical investigations for extraction, identification and determination of the poisons from animals’ vicera that poisoned experimentally with carbamate groubs pecticides. Eurasian J Vet Sci. March 1985;1(1):43-56.
Chicago Acet., H. Ahmet. “Chemical Investigations for Extraction, Identification and Determination of the Poisons from animals’ Vicera That Poisoned Experimentally With Carbamate Groubs Pecticides”. Eurasian Journal of Veterinary Sciences 1, no. 1 (March 1985): 43-56.
EndNote Acet. HA (March 1, 1985) Chemical investigations for extraction, identification and determination of the poisons from animals’ vicera that poisoned experimentally with carbamate groubs pecticides. Eurasian Journal of Veterinary Sciences 1 1 43–56.
IEEE H. A. Acet., “Chemical investigations for extraction, identification and determination of the poisons from animals’ vicera that poisoned experimentally with carbamate groubs pecticides”, Eurasian J Vet Sci, vol. 1, no. 1, pp. 43–56, 1985.
ISNAD Acet., H. Ahmet. “Chemical Investigations for Extraction, Identification and Determination of the Poisons from animals’ Vicera That Poisoned Experimentally With Carbamate Groubs Pecticides”. Eurasian Journal of Veterinary Sciences 1/1 (March 1985), 43-56.
JAMA Acet. HA. Chemical investigations for extraction, identification and determination of the poisons from animals’ vicera that poisoned experimentally with carbamate groubs pecticides. Eurasian J Vet Sci. 1985;1:43–56.
MLA Acet., H. Ahmet. “Chemical Investigations for Extraction, Identification and Determination of the Poisons from animals’ Vicera That Poisoned Experimentally With Carbamate Groubs Pecticides”. Eurasian Journal of Veterinary Sciences, vol. 1, no. 1, 1985, pp. 43-56.
Vancouver Acet. HA. Chemical investigations for extraction, identification and determination of the poisons from animals’ vicera that poisoned experimentally with carbamate groubs pecticides. Eurasian J Vet Sci. 1985;1(1):43-56.