Investigation of value-added compounds derived from oak wood using hydrothermal processing techniques and comprehensive analytical approaches (HPLC, GC-MS, FT-IR, and NMR)

Yunus Başar; Fatih Gül; Mehmet Salih Nas; Mehmet Hakkı Alma; Mehmet Harbi Çalımlı

doi:10.32571/ijct.1365592

EN

Investigation of value-added compounds derived from oak wood using hydrothermal processing techniques and comprehensive analytical approaches (HPLC, GC-MS, FT-IR, and NMR)

Abstract

In this study, slow pyrolysis of oak woods was carried out in a fixed bed tube reactor at four different temperatures ranging from 100 °C to 400 °C and at 5 °C/min speed time intervals. The compositions of the produced bio-tar and bio-oils were determined in detail using FT-IR, GC-MS, HPLC, and NMR devices. Several pyrolysis parameters were carried out to reveal the distribution of pyrolytic products under different pyrolysis temperatures (100–400 °C) and times (1–4 h). During the slow pyrolysis process, oak wood started to decompose to form organic volatile products at a set temperature of 100 °C and reached a maximum yield of volatile products at around 400 °C. GC-MS analyses revealed that different valuable components such as furans, phenolic compounds, carbonyls, linear, aromatic compounds, acids, and hydrocarbons have been formed. Based on the experimental results of the pyrolysis, it has been detected that the temperature and time interval are very effective parameters in the conversion of oak wood to the amount of liquid product.

Keywords

References

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Details

Primary Language

English

Subjects

Chemical Engineering (Other)

Journal Section

Research Article

Authors

Yunus Başar
0000-0002-7785-3242
Türkiye

Fatih Gül
0000-0002-4297-786X
Türkiye

Mehmet Salih Nas
0000-0003-1092-5237
Türkiye

Mehmet Hakkı Alma
0000-0001-7011-3965
Türkiye

Mehmet Harbi Çalımlı ^*
0000-0001-9756-191X
Türkiye

Early Pub Date

April 6, 2024

Publication Date

June 5, 2024

Submission Date

September 24, 2023

Acceptance Date

December 1, 2023

Published in Issue

Year 2024 Volume: 8 Number: 1

DOI

https://doi.org/10.32571/ijct.1365592

IZ

https://izlik.org/JA92AE78MF

Cite

RIS / Bibtex

APA

Başar, Y., Gül, F., Nas, M. S., Alma, M. H., & Çalımlı, M. H. (2024). Investigation of value-added compounds derived from oak wood using hydrothermal processing techniques and comprehensive analytical approaches (HPLC, GC-MS, FT-IR, and NMR). International Journal of Chemistry and Technology, 8(1), 51-59. https://doi.org/10.32571/ijct.1365592

AMA

1.Başar Y, Gül F, Nas MS, Alma MH, Çalımlı MH. Investigation of value-added compounds derived from oak wood using hydrothermal processing techniques and comprehensive analytical approaches (HPLC, GC-MS, FT-IR, and NMR). Int. J. Chem. Technol. 2024;8(1):51-59. doi:10.32571/ijct.1365592

Chicago

Başar, Yunus, Fatih Gül, Mehmet Salih Nas, Mehmet Hakkı Alma, and Mehmet Harbi Çalımlı. 2024. “Investigation of Value-Added Compounds Derived from Oak Wood Using Hydrothermal Processing Techniques and Comprehensive Analytical Approaches (HPLC, GC-MS, FT-IR, and NMR)”. International Journal of Chemistry and Technology 8 (1): 51-59. https://doi.org/10.32571/ijct.1365592.

EndNote

Başar Y, Gül F, Nas MS, Alma MH, Çalımlı MH (June 1, 2024) Investigation of value-added compounds derived from oak wood using hydrothermal processing techniques and comprehensive analytical approaches (HPLC, GC-MS, FT-IR, and NMR). International Journal of Chemistry and Technology 8 1 51–59.

IEEE

[1]Y. Başar, F. Gül, M. S. Nas, M. H. Alma, and M. H. Çalımlı, “Investigation of value-added compounds derived from oak wood using hydrothermal processing techniques and comprehensive analytical approaches (HPLC, GC-MS, FT-IR, and NMR)”, Int. J. Chem. Technol., vol. 8, no. 1, pp. 51–59, June 2024, doi: 10.32571/ijct.1365592.

ISNAD

Başar, Yunus - Gül, Fatih - Nas, Mehmet Salih - Alma, Mehmet Hakkı - Çalımlı, Mehmet Harbi. “Investigation of Value-Added Compounds Derived from Oak Wood Using Hydrothermal Processing Techniques and Comprehensive Analytical Approaches (HPLC, GC-MS, FT-IR, and NMR)”. International Journal of Chemistry and Technology 8/1 (June 1, 2024): 51-59. https://doi.org/10.32571/ijct.1365592.

JAMA

1.Başar Y, Gül F, Nas MS, Alma MH, Çalımlı MH. Investigation of value-added compounds derived from oak wood using hydrothermal processing techniques and comprehensive analytical approaches (HPLC, GC-MS, FT-IR, and NMR). Int. J. Chem. Technol. 2024;8:51–59.

MLA

Başar, Yunus, et al. “Investigation of Value-Added Compounds Derived from Oak Wood Using Hydrothermal Processing Techniques and Comprehensive Analytical Approaches (HPLC, GC-MS, FT-IR, and NMR)”. International Journal of Chemistry and Technology, vol. 8, no. 1, June 2024, pp. 51-59, doi:10.32571/ijct.1365592.

Vancouver

1.Yunus Başar, Fatih Gül, Mehmet Salih Nas, Mehmet Hakkı Alma, Mehmet Harbi Çalımlı. Investigation of value-added compounds derived from oak wood using hydrothermal processing techniques and comprehensive analytical approaches (HPLC, GC-MS, FT-IR, and NMR). Int. J. Chem. Technol. 2024 Jun. 1;8(1):51-9. doi:10.32571/ijct.1365592