Determination of aflatoxin and some trace element contents in black pepper samples

Fevzi Kılıçel; Hacer Sibel Karapinar

doi:10.32571/ijct.464189

Research Article

Determination of aflatoxin and some trace element contents in black pepper samples

Year 2018, Volume: 2 Issue: 2, 153 - 160, 28.12.2018

Fevzi Kılıçel Hacer Sibel Karapinar

https://doi.org/10.32571/ijct.464189

Abstract

Concentrations
of the total aflatoxin (AF), aflatoxin G1 (AFG1), aflatoxin G2 (AFG2),
aflatoxin B1 (AFB1), aflatoxin B2 (AFB2) and some trace elements such as lead,
cobalt, nickel, arsenic, copper, zinc, manganese, magnesium, iron, calcium and
chromium in black pepper samples were determined. Four black pepper samples were
collected from markets in Karaman/Turkey. Detection of toxins were performed
using HPLC instruments after pre-separation using immunoaffinity columns
working through a solid phase extraction. The heavy metal contents in black
peppers were determined by flame atomic adsorption methods. Also, quantities of
trace elements were determined in 4 samples collected during summer and winter
months. The total AF was determined below the maximum limits in pepper samples.
Quantities of Co, Ni, Cr, Cu, Zn, Pb, Mn, Fe, Mg and Ca were detected in the samples.
When the results were evaluated, the values found for Cu, Zn and Mg were seen
to be at normal levels. Co, Ni, Cr, Pb, Mn, Fe, Ca trace element concentrations
were obtained above the normal limit but Co, Pb and Mn were found below the
toxic limits.

Keywords

Aflatoxins, Heavy metals, Black pepper, HPLC

References

1. D'Mello, J. P. F. Food safety: Contaminants and toxins. 2003, pp 65.
2. Kwiatkowski, A.; De Faria Alves, A. P. SaBios-Revista de Saúde e Biologia. 2007, 2(2).
3. Creppy, E. E. Toxicol. Lett. 2002, 127(1-3), 19-28.
4. Solis-Sánchez, L. O.; Castañeda-Miranda, R.; García-Escalante, J. J.; Torres-Pacheco, I.; Guevara-González, R. G.; Castañeda-Miranda, C. L.; Alaniz-Lumbreras, P. D. Comput. Eelectron. Agric. 2011, 75(1), 92-99.
5. Strosnider, H.; Azziz-Baumgartner, E.; Banziger, M.; Bhat, R. V., Breiman, R.; Brune, M. N.; Henry, S. H. Environ. Health Persp. 2006, 114(12), 1898.
6. Razzaghi-Abyaneh, M.; Shams-Ghahfarokhi, M.; Peng-Kuang, C. Aflatoxins: Mechanism of inhibition by antagonistic plants and bacteria; Eds., www. Intechopen. com/boks. 2010; pp 586-304.
7. Merian, E.; Clarkson, T. W. Metals and their compounds in the environment, 1991. http://agris.fao.org/agris-search/index.do (accessed May 10, 2017).
8. Hongxing, Z.; Yu-Kui, R. J. Chem. 2011, 8(2), 782-786.
9. Singh, A.; Sharma, R. K.; Agrawal, M.; Marshall, F. M. Food Chem. Toxicol. 2010, 48(2), 611-619.
10. Macrae. R.; Robinson, R.K.; Sadler, M.J. Encyclopaedia of Food Science. Food Technology and Nutrition, Academic Press INC, San Diego, 1993, pp 3126 -3131.
11. Guide, E. A laboratory guide to method validation and related topics, LGC, Teddington, Middlesex, UK, 1998.
12. Stanojkovic-Sebic, A.; Pivic, R..; Josic, D.; Dinic, Z.; Stanojkovic, A. Tarım Bilimleri Dergisi. 2015, 21(3), 317-325 (in Turkish).
13. Kilicel, F.; Karapinar, H. S.; Cimen, A. Science J. Anal. Chem. 2017, 5(6), 90.

Year 2018, Volume: 2 Issue: 2, 153 - 160, 28.12.2018

Fevzi Kılıçel Hacer Sibel Karapinar

https://doi.org/10.32571/ijct.464189

Abstract

References

1. D'Mello, J. P. F. Food safety: Contaminants and toxins. 2003, pp 65.
2. Kwiatkowski, A.; De Faria Alves, A. P. SaBios-Revista de Saúde e Biologia. 2007, 2(2).
3. Creppy, E. E. Toxicol. Lett. 2002, 127(1-3), 19-28.
4. Solis-Sánchez, L. O.; Castañeda-Miranda, R.; García-Escalante, J. J.; Torres-Pacheco, I.; Guevara-González, R. G.; Castañeda-Miranda, C. L.; Alaniz-Lumbreras, P. D. Comput. Eelectron. Agric. 2011, 75(1), 92-99.
5. Strosnider, H.; Azziz-Baumgartner, E.; Banziger, M.; Bhat, R. V., Breiman, R.; Brune, M. N.; Henry, S. H. Environ. Health Persp. 2006, 114(12), 1898.
6. Razzaghi-Abyaneh, M.; Shams-Ghahfarokhi, M.; Peng-Kuang, C. Aflatoxins: Mechanism of inhibition by antagonistic plants and bacteria; Eds., www. Intechopen. com/boks. 2010; pp 586-304.
7. Merian, E.; Clarkson, T. W. Metals and their compounds in the environment, 1991. http://agris.fao.org/agris-search/index.do (accessed May 10, 2017).
8. Hongxing, Z.; Yu-Kui, R. J. Chem. 2011, 8(2), 782-786.
9. Singh, A.; Sharma, R. K.; Agrawal, M.; Marshall, F. M. Food Chem. Toxicol. 2010, 48(2), 611-619.
10. Macrae. R.; Robinson, R.K.; Sadler, M.J. Encyclopaedia of Food Science. Food Technology and Nutrition, Academic Press INC, San Diego, 1993, pp 3126 -3131.
11. Guide, E. A laboratory guide to method validation and related topics, LGC, Teddington, Middlesex, UK, 1998.
12. Stanojkovic-Sebic, A.; Pivic, R..; Josic, D.; Dinic, Z.; Stanojkovic, A. Tarım Bilimleri Dergisi. 2015, 21(3), 317-325 (in Turkish).
13. Kilicel, F.; Karapinar, H. S.; Cimen, A. Science J. Anal. Chem. 2017, 5(6), 90.

There are 13 citations in total.

Details

Primary Language	English
Subjects	Chemical Engineering
Journal Section	Research Articles
Authors	Fevzi Kılıçel 0000-0002-5454-5597 Hacer Sibel Karapinar 0000-0002-0123-3901
Publication Date	December 28, 2018
Published in Issue	Year 2018 Volume: 2 Issue: 2

Cite

APA	Kılıçel, F., & Karapinar, H. S. (2018). Determination of aflatoxin and some trace element contents in black pepper samples. International Journal of Chemistry and Technology, 2(2), 153-160. https://doi.org/10.32571/ijct.464189
AMA	Kılıçel F, Karapinar HS. Determination of aflatoxin and some trace element contents in black pepper samples. Int. J. Chem. Technol. December 2018;2(2):153-160. doi:10.32571/ijct.464189
Chicago	Kılıçel, Fevzi, and Hacer Sibel Karapinar. “Determination of Aflatoxin and Some Trace Element Contents in Black Pepper Samples”. International Journal of Chemistry and Technology 2, no. 2 (December 2018): 153-60. https://doi.org/10.32571/ijct.464189.
EndNote	Kılıçel F, Karapinar HS (December 1, 2018) Determination of aflatoxin and some trace element contents in black pepper samples. International Journal of Chemistry and Technology 2 2 153–160.
IEEE	F. Kılıçel and H. S. Karapinar, “Determination of aflatoxin and some trace element contents in black pepper samples”, Int. J. Chem. Technol., vol. 2, no. 2, pp. 153–160, 2018, doi: 10.32571/ijct.464189.
ISNAD	Kılıçel, Fevzi - Karapinar, Hacer Sibel. “Determination of Aflatoxin and Some Trace Element Contents in Black Pepper Samples”. International Journal of Chemistry and Technology 2/2 (December 2018), 153-160. https://doi.org/10.32571/ijct.464189.
JAMA	Kılıçel F, Karapinar HS. Determination of aflatoxin and some trace element contents in black pepper samples. Int. J. Chem. Technol. 2018;2:153–160.
MLA	Kılıçel, Fevzi and Hacer Sibel Karapinar. “Determination of Aflatoxin and Some Trace Element Contents in Black Pepper Samples”. International Journal of Chemistry and Technology, vol. 2, no. 2, 2018, pp. 153-60, doi:10.32571/ijct.464189.
Vancouver	Kılıçel F, Karapinar HS. Determination of aflatoxin and some trace element contents in black pepper samples. Int. J. Chem. Technol. 2018;2(2):153-60.