DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS

Borys Varynskyı

doi:10.1501/Eczfak_0000000586

TR EN

KÜMES HAYVANLARI YUMURTALARINDAKİ PİPERİDİN-1-YUM {[5-(2-FURİL)-4- FENİL-4H-1,2,4-TRİAZOL-3-İL]TİYO}ASETAT ARTIKLARININ BELİRLENMESİ İÇİN BİR LC-ESI-MS YÖNTEMİNİN GELİŞTİRİLMESİ VE VALİDASYONU

Abstract

ESI-MS yöntemi tasarlanmıştır. Numuneler ultrasonik banyoda dimetil sülfoksit ile ekstre edilmiş, 15.000 g'da santrifüjlenmiş, ultrafiltre ile süzülmüş ve HPLC sistemine enjekte edilmiştir. Suda %0,1 (h/h) formik asit (A) ve asetonitrilde %0,1 (h/h) formik asit (B) içeren mobil faz ile izokratik elüsyon yapılmıştır. Mobil fazın bileşimi, 0,4 mL. dak-1 akış hızında, A/B (%70: %30, h/h)dır. Toplam çalışma süresi 5 dakikadır. Kütle spektrometrik koşullar, SIM modu (m/z 302,1), pozitif polaritedir. Doğruluk %0,2887-7,204 dır. Kesinlik, %1,564-5,636 dır. Yöntem, kümes hayvanları yumurtalarındaki Trifuzol kalıntısı kantitatif tayininde kullanılabilir.

Keywords

kümes hayvanları yumurtası, kütle spektrometrisi, triazoller, trifuzol, yüksek basınçlı sıvı kromatografisi

Details

Primary Language

English

Subjects

-

Journal Section

-

Authors

Borys Varynskyı This is me

Publication Date

December 1, 2016

Submission Date

December 1, 2016

Acceptance Date

-

Published in Issue

Year 2016 Volume: 40 Number: 3

DOI

https://doi.org/10.1501/Eczfak_0000000586

IZ

https://izlik.org/JA29TC44TK

Cite

RIS / Bibtex

APA

Varynskyı, B. (2016). DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS. Journal of Faculty of Pharmacy of Ankara University, 40(3), 29-40. https://doi.org/10.1501/Eczfak_0000000586

AMA

1.Varynskyı B. DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS. J. Fac. Pharm. Ankara. 2016;40(3):29-40. doi:10.1501/Eczfak_0000000586

Chicago

Varynskyı, Borys. 2016. “DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS”. Journal of Faculty of Pharmacy of Ankara University 40 (3): 29-40. https://doi.org/10.1501/Eczfak_0000000586.

EndNote

Varynskyı B (December 1, 2016) DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS. Journal of Faculty of Pharmacy of Ankara University 40 3 29–40.

IEEE

[1]B. Varynskyı, “DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS”, J. Fac. Pharm. Ankara, vol. 40, no. 3, pp. 29–40, Dec. 2016, doi: 10.1501/Eczfak_0000000586.

ISNAD

Varynskyı, Borys. “DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS”. Journal of Faculty of Pharmacy of Ankara University 40/3 (December 1, 2016): 29-40. https://doi.org/10.1501/Eczfak_0000000586.

JAMA

1.Varynskyı B. DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS. J. Fac. Pharm. Ankara. 2016;40:29–40.

MLA

Varynskyı, Borys. “DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS”. Journal of Faculty of Pharmacy of Ankara University, vol. 40, no. 3, Dec. 2016, pp. 29-40, doi:10.1501/Eczfak_0000000586.

Vancouver

1.Borys Varynskyı. DEVELOPMENT AND VALIDATION OF A LC-ESI-MS METHOD FOR DETECTION OF PIPERIDIN-1-IUM {[5-(2-FURYL)-4-PHENYL-4H- 1,2,4-TRIAZOL-3-YL] THIO}ACETATE RESIDUES IN POULTRY EGGS. J. Fac. Pharm. Ankara. 2016 Dec. 1;40(3):29-40. doi:10.1501/Eczfak_0000000586

KÜMES HAYVANLARI YUMURTALARINDAKİ PİPERİDİN-1-YUM {[5-(2-FURİL)-4- FENİL-4H-1,2,4-TRİAZOL-3-İL]TİYO}ASETAT ARTIKLARININ BELİRLENMESİ İÇİN BİR LC-ESI-MS YÖNTEMİNİN GELİŞTİRİLMESİ VE VALİDASYONU

Abstract

Keywords