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Year 2012, Volume: 1 Issue: 1, 1 - 4, 01.01.2012

Derya Celik Ahmet Tutar Ramazan Erenler

Abstract

Short and Selective Synthesis of 3,5-dibromoinden-1-one

Year 2012, Volume: 1 Issue: 1, 1 - 4, 01.01.2012

Derya Celik Ahmet Tutar Ramazan Erenler

Abstract

Brominations of hydrocarbons are important processes in synthetic chemistry. Bromoindanes and bromoindenones are key intermediate for medicinally valuable compounds. Short and efficient synthesis of 3,5-dibromoinden-1-one is presented. 5-bromoindane-1-one 1 was treated with ethylene glycol to mask the ketone functional group to yield the cyclic ketal 2. Bromination of bromoindanecyclic ketal 2 with bromine in photochemical reaction apparatus while being irradiated with a projector lamp afforded the product which was treated with silica gel directly to remove the protective group afforded the corresponding 3,5-dibromoinden-1-one 3

Keywords

Photobromination 5-bromoindanone ethylene ketal 3 5-dibromoinden-1-one protecting group radical mechanism

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Details

Primary Language English
Journal Section Articles
Authors

Derya Celik This is me

Ahmet Tutar This is me

Ramazan Erenler This is me

Publication Date January 1, 2012
Published in Issue Year 2012 Volume: 1 Issue: 1

Cite

APA Celik, D., Tutar, A., & Erenler, R. (2012). Short and Selective Synthesis of 3,5-dibromoinden-1-one. Journal of New Results in Science, 1(1), 1-4.
AMA Celik D, Tutar A, Erenler R. Short and Selective Synthesis of 3,5-dibromoinden-1-one. JNRS. January 2012;1(1):1-4.
Chicago Celik, Derya, Ahmet Tutar, and Ramazan Erenler. “Short and Selective Synthesis of 3,5-Dibromoinden-1-One”. Journal of New Results in Science 1, no. 1 (January 2012): 1-4.
EndNote Celik D, Tutar A, Erenler R (January 1, 2012) Short and Selective Synthesis of 3,5-dibromoinden-1-one. Journal of New Results in Science 1 1 1–4.
IEEE D. Celik, A. Tutar, and R. Erenler, “Short and Selective Synthesis of 3,5-dibromoinden-1-one”, JNRS, vol. 1, no. 1, pp. 1–4, 2012.
ISNAD Celik, Derya et al. “Short and Selective Synthesis of 3,5-Dibromoinden-1-One”. Journal of New Results in Science 1/1 (January 2012), 1-4.
JAMA Celik D, Tutar A, Erenler R. Short and Selective Synthesis of 3,5-dibromoinden-1-one. JNRS. 2012;1:1–4.
MLA Celik, Derya et al. “Short and Selective Synthesis of 3,5-Dibromoinden-1-One”. Journal of New Results in Science, vol. 1, no. 1, 2012, pp. 1-4.
Vancouver Celik D, Tutar A, Erenler R. Short and Selective Synthesis of 3,5-dibromoinden-1-one. JNRS. 2012;1(1):1-4.


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