An Innovative Synthesis of Nano-ZSM-5 Zeolite Through Interrupted Ultrasound

Pirzada Afridi; Farrukh Arsalan Siddiqui; Sergio Gonzalez-cortes; Liam France

An Innovative Synthesis of Nano-ZSM-5 Zeolite Through Interrupted Ultrasound

Abstract

NanoZSM-5 was synthesized with crystal size ≤30 nm by using an interrupted ultrasound crystallization process. In his process, the hydrothermal treatment was interrupted with ultrasound and without ultrasound at 170 oC for 24 hours. The nanoZSM-5 crystallinity was confirmed by X-ray diffraction. The crystallite size and morphology were determined by TEM and SEM. The textural properties were investigated by N2 physisorption. 29Si MAS NMR confirmed the framework composition and presence of silanol group at the surface of the nanoZSM-5.

Keywords

References

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Details

Primary Language

English

Subjects

Chemical Engineering

Journal Section

Research Article

Authors

Pirzada Afridi This is me
United Kingdom

Farrukh Arsalan Siddiqui ^* This is me
Pakistan

Sergio Gonzalez-cortes This is me
United Kingdom

Liam France This is me
United Kingdom

Publication Date

May 7, 2022

Submission Date

October 12, 2021

Acceptance Date

-

Published in Issue

Year 2022 Volume: 6 Number: 1

IZ

https://izlik.org/JA52FB43CG

Cite

RIS / Bibtex