Year 2017, Volume , Issue 1, Pages 16 - 21 2017-12-31

Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem
A Simple spectrofluorimetric method to determine Sudan I dye in spices (Full-text language: Turkish)

Osman Can ÇAĞILCI [1] , Abidin GÜMRÜKÇÜOĞLU [2] , Hakan ALP [3] , Elvan VANLI [4] , Ümmühan OCAK [5] , Miraç OCAK [6]


Yasal olmamasına rağmen gıdalarda renklendirme amacıyla kullanıldığı bilinen azo boyar maddesi olan Sudan I’in, kendine has floresans özelliği kullanılarak çeşitli baharatlarda tayini için basit bir spektroflorimetrik yöntem geliştirildi. Önerilen yöntem gerçek numune olarak yerel üreticilerden temin edilen pul biber, sumak ve kimyon numunelerine Sudan I ilavesinden sonra uygulandı. Ekleme-geri kazanım sonuçları ile yöntemin doğruluğu gösterildi. Pul biber, sumak ve kimyon için geri kazanım değerleri %96,6 ile %97,6 arasında bulundu. Ölçümler modifiye edilmiş bir standart ekleme yöntemi kullanılarak gerçekleştirildi. Tespit sınırları pul biber, sumak ve kimyon için sırasıyla; 1,0 mg/L, 0,2 mg/L ve 0,3 mg/L olarak bulundu. Önerilen yöntem, pul biber, sumak ve kimyon gibi baharatlardaki Sudan I miktarını belirlemek için literatürdeki yöntemlere göre basit, çevreci ve düşük maliyetli bir yöntemdir.

A simple spectrofluorimetric method was developed to determine Sudan I, a banned food dye, in various spices by using its intrinsic fluorescence property. The proposed method was used in the determination of red pepper, sumac and cumin samples to which were added Sudan I dye after being supplied from the local sources. The accuracy of method has been shown by the spike and recovery experiments.  The recovery values for red pepper, sumac and cumin found to be acceptable from 96.6% to 97.6%. Measurements were carried out by using the modified standard addition method. Detection limits were 1.0, 0.2 and 0.3 mg/L for red pepper, sumac and cumin, respectively. The presented method is simple, green and cost-effective for determination of Sudan I content of spices.

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Primary Language tr
Subjects Engineering, Chemical
Journal Section Research Article
Authors

Author: Osman Can ÇAĞILCI (Primary Author)
Country: Turkey


Author: Abidin GÜMRÜKÇÜOĞLU
Country: Turkey


Author: Hakan ALP
Country: Turkey


Author: Elvan VANLI
Country: Turkey


Author: Ümmühan OCAK
Country: Turkey


Author: Miraç OCAK

Dates

Publication Date : December 31, 2017

Bibtex @research article { kcst375689, journal = {Karadeniz Chemical Science and Technology}, issn = {}, eissn = {2636-8560}, address = {Karadeniz Chemical Science and Technology (KCST) Journal, Department of Chemistry, Faculty of Science, KTU, 61080, Trabzon, TÜRKİYE}, publisher = {KCST Founding Board}, year = {2017}, volume = {}, pages = {16 - 21}, doi = {}, title = {Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem}, key = {cite}, author = {Çağılcı, Osman Can and Gümrükçüoğlu, Abidin and Alp, Hakan and Vanlı, Elvan and Ocak, Ümmühan and Ocak, Miraç} }
APA Çağılcı, O , Gümrükçüoğlu, A , Alp, H , Vanlı, E , Ocak, Ü , Ocak, M . (2017). Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem . Karadeniz Chemical Science and Technology , (1) , 16-21 . Retrieved from https://dergipark.org.tr/en/pub/kcst/issue/34253/375689
MLA Çağılcı, O , Gümrükçüoğlu, A , Alp, H , Vanlı, E , Ocak, Ü , Ocak, M . "Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem" . Karadeniz Chemical Science and Technology (2017 ): 16-21 <https://dergipark.org.tr/en/pub/kcst/issue/34253/375689>
Chicago Çağılcı, O , Gümrükçüoğlu, A , Alp, H , Vanlı, E , Ocak, Ü , Ocak, M . "Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem". Karadeniz Chemical Science and Technology (2017 ): 16-21
RIS TY - JOUR T1 - Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem AU - Osman Can Çağılcı , Abidin Gümrükçüoğlu , Hakan Alp , Elvan Vanlı , Ümmühan Ocak , Miraç Ocak Y1 - 2017 PY - 2017 N1 - DO - T2 - Karadeniz Chemical Science and Technology JF - Journal JO - JOR SP - 16 EP - 21 VL - IS - 1 SN - -2636-8560 M3 - UR - Y2 - 2018 ER -
EndNote %0 Karadeniz Chemical Science and Technology Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem %A Osman Can Çağılcı , Abidin Gümrükçüoğlu , Hakan Alp , Elvan Vanlı , Ümmühan Ocak , Miraç Ocak %T Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem %D 2017 %J Karadeniz Chemical Science and Technology %P -2636-8560 %V %N 1 %R %U
ISNAD Çağılcı, Osman Can , Gümrükçüoğlu, Abidin , Alp, Hakan , Vanlı, Elvan , Ocak, Ümmühan , Ocak, Miraç . "Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem". Karadeniz Chemical Science and Technology / 1 (December 2017): 16-21 .
AMA Çağılcı O , Gümrükçüoğlu A , Alp H , Vanlı E , Ocak Ü , Ocak M . Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem. Karadeniz Chem. Sci. Tech.. 2017; (1): 16-21.
Vancouver Çağılcı O , Gümrükçüoğlu A , Alp H , Vanlı E , Ocak Ü , Ocak M . Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem. Karadeniz Chemical Science and Technology. 2017; (1): 16-21.
IEEE O. Çağılcı , A. Gümrükçüoğlu , H. Alp , E. Vanlı , Ü. Ocak and M. Ocak , "Baharatlarda Sudan I boyası’nın tayini için basit bir spektroflorimetrik yöntem", Karadeniz Chemical Science and Technology, no. 1, pp. 16-21, Dec. 2018