Investigation of the Interaction of Wear Resistance of Hastelloy C-22 Super Alloy with Cryogenic Process for Usability in Machine Construction

Year 2022, , 175 - 188, 01.03.2022

Muhammed Salih Gül , Hasan Gökkaya , Bilgehan Kondul , Muhammet Hüseyin Çetin

https://doi.org/10.36306/konjes.1024523

Abstract

The parts to be used in machine construction must have high wear, fatigue and corrosion resistance. Hastelloy C-22 superalloy draws attention with its high corrosion resistance, but its constructive use is limited due to insufficient wear resistance. In this study, deep and shallow cryogenic treatment was applied to Hastelloy C-22 superalloy to improve wear resistance. Before the wear test, XRD analysis, hardness measurement and microstructure imaging were performed for metallurgical characterization. The cryogenic treated samples were brought to room temperature for 6 hours after being kept at cryogenic treatment application temperatures for 24 hours. The samples brought to room temperature were tempered at 200 ºC for 2 hours. In the hardness measurements made after heat treatment, it was determined that the hardness value of the deep cryogenic treated sample increased by 45%, and the hardness value of the shallow cryogenic treated sample increased by 14%. Wear tests were carried out according to ASTM G133 standard using the ball-on-flat type method that moves back and forth linearly, a force of 10 N, 20 N and 40 N was applied to all samples at a constant sliding speed of 72 mm/s at a total sliding distance of 1000 m. As a result of wear tests, volumetric loss was 24% in shallow cryogenic treatment and 44% in deep cryogenic treatment.

Keywords

Cryogenic treatment, Hastelloy C-22, Hardness, Wear, Microstructure

MAKİNE KONSTRÜKSİYONUNDA KULLANILABİLİRLİK İÇİN HASTELLOY C-22 SÜPER ALAŞIMININ AŞINMA DİRENCİNİN KRİYOJENİK İŞLEM İLE ETKİLEŞİMİNİN İNCELENMESİ

Abstract

Makine konstrüksiyonunda kullanılacak parçaların aşınma, yorulma ve korozyon dirençlerinin yüksek olması önem taşımaktadır. Hastelloy C-22 süperalaşımı yüksek korozyon direnciyle dikkat çekmekte fakat aşınma dayanımının yetersizliği nedeniyle konstrüktif kullanımı sınırlı kalmaktadır. Bu çalışmada, Hastelloy C-22 süper alaşımına, aşınma direncini iyileştirebilmek amacıyla derin ve sığ kriyojenik işlem uygulanmıştır. Aşınma deneyi öncesi metalurjik karakterizasyon amacıyla XRD analizleri, sertlik ölçümü ve mikroyapı görüntülemesi yapılmıştır. Kriyojenik işlem uygulanmış numuneler, kriyojenik işlem uygulama sıcaklıklarında 24’er saat bekletildikten sonra oda sıcaklığına 6 saatlik bir sürede getirilmiştir. Oda sıcaklığına getirilen numunelere 200 ºC ‘de 2 saat süreyle temperleme işlemi uygulanmıştır. Isıl işlem sonrası yapılan sertlik ölçümlerinde, derin kriyojenik işlem uygulanmış numunenin sertlik değerinin %45 oranında, sığ kriyojenik işlem uygulanmış numunenin sertlik değerinin ise %14 oranında arttığı tespit edilmiştir. Aşınma deneyleri ASTM G133 standartına göre doğrusal olarak ileri geri hareket eden pim üzeri plaka (ball-on flat) tipi metoduyla, tüm numunelere 10 N, 20 N ve 40 N kuvvet uygulanarak 72 mm/s sabit kayma hızında toplamda 1000 m kayma mesafesinde gerçekleştirilmiştir. Aşınma deneyleri sonucunda, sığ kriyojenik işlemde %24, derin kriyojenik işlemde ise %44 oranında hacimsel kayıp gerçekleşmiştir.

Keywords

Kriyojenik işlem, Hastelloy C-22, Sertlik, Aşınma, Mikroyapı

References

• Abdullah, T.K., Petitjean, C., Panteix, PJ., Rapin, C., Vilasi, M., Hussain Z., ve Rahim, AA., 2013, “Dissolution Equilibrium of Chromium Oxide in a Soda Lime Silicate Melt Exposed to Oxidizing and Reducing Atmospheres”, Materials Chemistry and Physics, Cilt 142, Sayı 2–3, ss. 572–79.
• Abu Kassim S., Thor, JA., Abu Seman, A., ve Abdullah TK., 2020, “High Temperature Corrosion of Hastelloy C22 in Molten Alkali Salts: The Effect of Pre-Oxidation Treatment”, Corrosion Science, Cilt 173, ss. 108761.
• Akhbarizadeh, A., Shafyei, A., ve Golozar MA., 2009, “Effects of Cryogenic Treatment on Wear Behavior of D6 Tool Steel”, Materials and Design, Cilt 30, Sayı 8, ss. 3259–3264.
• Baldissera, P., ve Delprete, C., 2008, “Deep Cryogenic Treatment: A Bibliographic Review”, The Open Mechanical Engineering Journal, Cilt 2, Sayı 1, ss. 1–11.
• Barron, RF., 1982, “Cryogenic Treatment To Improve Wear Resistance of Steel By the ‘Cryotough’ Process”, Cryogenics, Cilt 22, Sayı 8, ss. 409–13.
• Barron, RF., ve Mulhern CR., 1980, “Cryogenic Treatment of Aisi-T8 and Ci045 Steels”, Advances In Cryogenic Engineering Materials, Cilt 26, ss. 171–79.
• Bensely, A., Prabhakaran, A., Mohan Lal, D., ve Nagarajan, G., 2005, “Enhancing the Wear Resistance of Case Carburized Steel (En 353) by Cryogenic Treatment”, Cryogenics, Cilt 45, Sayı 12, ss. 747–54.
• Candane, D., Alagumurthi, N., ve Palaniradja, K., 2013, “Effect of Cryogenic Treatment on Microstructure and Wear Characteristics of AISI M35 HSS”, International Journal of Materials Science and Applications, Cilt 2, Sayı 2, ss. 56-65.
• Dixit, Swadesh S., Nimbalkar, SR., ve Kharde, RR., 2013, “Dry Sliding Wear Analysis of D5 Tool Steel at Different Heat Treatments”, The International Journal Of Engineering And Science (IJES), Cilt 2, Sayı 5, ss. 16–26.
• Erdoğan, A., 2019, “Investigation of High Temperature Dry Sliding Behavior of Borided H13 Hot Work Tool Steel with Nanoboron Powder”, Surface and Coatings Technology, Cilt 357, Sayı September 2018, ss. 886–95.
• Firouzdor, V., Nejati, E., ve Khomamizadeh, F., 2008, “Effect of Deep Cryogenic Treatment on Wear Resistance and Tool Life of M2 HSS Drill”, Journal of Materials Processing Technology, Cilt 206, Sayı 1–3, ss. 467–72.
• Firouzdor, V., Sridharan, K., Cao, G., Anderson, M., ve Allen, TR., 2013, “Corrosion of a Stainless Steel and Nickel-Based Alloys in High Temperature Supercritical Carbon Dioxide Environment”, Corrosion Science, Cilt 69, ss. 281–91.
• Gül, MS., 2019, Kriyojenik Isıl İşlemin Hastelloy C-22 Süper Alaşımının Aşınma Davranışına Olan Etkisinin Araştırılması, Yüksek Lisans Tezi, Karabük Üniversitesi, Fen Bilimleri Enstitüsü, Karabük.
• Hashim, AA., Hammood, AS., ve Hammadi, NJ., 2015, “Evaluation of High-Temperature Oxidation Behavior of Inconel 600 and Hastelloy C-22”, Arabian Journal for Science and Engineering, Cilt 40, Sayı 9, ss. 2739–46.
• He, X., Xiao, H., Ozaydin, MF., Balzuweit, K., ve Liang, H., 2015, " Low-Temperature Boriding of High-Carbon Steel Xingliang", Surface and Coatings Technology, Cilt 263, ss. 21-26.
• He, Y.,Yang, J., Chen, S., ve Gao, Z., 2016, “Influence of Simulated Heat-Affected Zone Thermal Cycle Treatment on Mechanical Performances and Microstructural Stability of Ni-17Mo-7Cr Based Superalloy”, Vacuum, Cilt 125, ss. 26–35.
• Kalsi, NS., Sehgal, R., ve Sharma, VS., 2014, “Effect of Tempering after Cryogenic Treatment of Tungsten Carbide-Cobalt Bounded Inserts”, Bulletin of Materials Science, Cilt 37, Sayı 2, ss. 327–35.
• Khakbaz, F., ve Kazeminezhad, M., 2012, “Work Hardening and Mechanical Properties of Severely Deformed AA3003 by Constrained Groove Pressing”, Journal of Manufacturing Processes, Cilt 14, Sayı 1, ss. 20–25.
• Kondul, B., ve Çetin MH., 2022, " Increasing The Wear Resistance of Railway Switches With Boron Coating And Analysis of Tribological Performance by ANOVA Method", Wear, Cilt 488-489, Sayı Eylül 2021, ss. 204132.
• Kumar, S., Chattopadhyay, K., ve Singh V., 2016, “Effect of Surface Nanostructuring on Corrosion Behavior of Ti–6Al–4V Alloy”, Materials Characterization, Cilt 121, ss.23–30.
• Leskovšek, V., Kalin, M., ve Vižintin J., 2006, “Influence of Deep-Cryogenic Treatment on Wear Resistance of Vacuum Heat-Treated HSS”, Vacuum, Cilt 80, Sayı 6, ss. 507–18.
• Maleki, E., ve Unal, O., 2018, “Roles of Surface Coverage Increase and Re-Peening on Properties of AISI 1045 Carbon Steel in Conventional and Severe Shot Peening Processes", Surfaces and Interfaces, Cilt 11, Sayı March 2018, ss. 82–90.
• Mohan Lal, D., Renganarayanan, S., ve Kalanidhi A., 2001, “Cryogenic Treatment to Augment Wear Resistance of Tool and Die Steels”, Cryogenics, Cilt 41, Sayı 3, ss. 149–55.
• Moore, K., ve Collins DN., 1993, “Cryogenic Treatment of Three Heat-Treated Tool Steels”, Key Engineering Materials, Cilt 86–87, ss. 47–54.
• Patil, PI., ve Tated RG., 2012, “Comparison of Effects of Cryogenic Treatment on Different Types of Steels: A Review”, IJCA Proceedings on International Conference in Computional Intelligence, Sayı 9, ss. 10–29.
• Podgornik, B., Leskovsek, V., ve Vizintin, J.,2009, " Influence of Deep-Cryogenic Treatment on Tribological Properties of P/M High-Speed Steel", Materials and Manufacturing Processes, Cilt 24, Sayı 7-8, ss. 734-738.
• Reitz, W., ve Pendray J., 2001, “Cryoprocessing of Materials: A Review of Current Status”, Materials and Manufacturing Processes, Cilt 16, Sayı 6, ss. 829–40.
• Senthilkumar, D., ve Rajendran, I., 2011, " Influence of Shallow and Deep Cryogenic Treatment on Tribological Behavior of En 19 Steel", Cilt 18, Sayı 9, ss. 53-59.
• Sharma, S., Taiwade, RV., Yadav, A., ve Vashishtha, H., 2019, “Influence of Fillers and Welding Processes on the Microstructural Evolution, Mechanical Properties and Corrosion Behavior of Dissimilar Hastelloy C-22/AISI 321 Joints”, Materials Research Express, Cilt 6, Sayı 9.
• Slatter, T., Lewis, R., ve Jones AH., 2011, “The Influence of Cryogenic Processing on Wear on the Impact Wear Resistance of Low Carbon Steel and Lamellar Graphite Cast Iron”, Wear, Cilt 271, Sayı 9–10, ss.1481–89.
• Thakur, D., Ramamoorthy, B., ve Vijayaraghavan, L., 2008, “Influence of Different Post Treatments on Tungsten Carbide-Cobalt Inserts”, Materials Letters, Cilt 62, Sayı 28, ss. 4403–4406.
• Turan, ME., Sun, Y., ve Akgul, Y., 2018, “Improved Wear Properties of Magnesium Matrix Composite with the Addition of Fullerene Using Semi Powder Metallurgy”, Fullerenes Nanotubes and Carbon Nanostructures, Cilt 26, Sayı 2, ss. 130–36.
• Vimal, AJ., Bensely, A., Lal, DM., ve Srinivasan, K., 2008, “Deep Cryogenic Treatment Improves Wear Resistance of En 31 Steel”, Materials and Manufacturing Processes, Cilt 23, Sayı 4, ss. 369–76.
• Zhirafar, S., Rezaeian, A., ve Pugh, M., 2007, “Effect of Cryogenic Treatment on the Mechanical Properties of 4340 Steel”, Journal of Materials Processing Technology, Cilt 186, Sayı 1–3, ss. 298–303.
• Zhisheng, W., Ping, S., Jinrui, L., ve Shengsun H., 2003, “Effect of Deep Cryogenic Treatment on Electrode Life and Microstructure for Spot Welding Hot Dip Galvanized Steel”, Materials and Design, Cilt 24, Sayı 8, ss. 687–92.